Document text
SCIENTIFIC
Operating Instructions
Thermo Scientific Barnstead GenPure
Water Purification System
with xCAD
50131281 Stand: 11.12 Rights to technical changes reserved
Thermo Thermo Scientific Barnstead GenPure with xCAD
te ere Ultrapure water system
EC-Declaration of Conformity
in accordance with the EEC machine directive 2006/42/EC, appendix Il A
We hereby certify that the following described machine in its conception and form put by us into
circulation is in accordance with all the relevant essential health and safety requirements of the
EC machinery directive 2006/42/EC as amended and the national laws and regulations adopt-
ing this directive.
This declaration is no longer valid if the machine is modified without our consent.
Manufacturer: Thermo Electron LED GmbH
Robert-Bosch-Strake 1
D-63505 Langenselbold
Description of the machine:
function: Ultrapure water system
type: GenPure with xCAD, GenPure UF with xCAD, GenPure UV with xCAD,
GenPure UV/UF with xCAD, GenPure UV-TOC with xCAD, GenPure UV-
TOC/UF with xCAD
article number: bench version: 50131286, 50131250, 50131254, 50131252, 50131296,
50131298
wall version: 50131300, 50131302, 50131317, 50131315, 50131321,
50131323
The agreement with further valid guidelines/regulations following for the product is ex-
plained:
EMC Directive (2004/108/EC)
Reference to the harmonised standards:
DIN EN ISO 12100-1 Safety of machinery, Part 1: Basic terminology
DIN EN ISO 12100-2 Safety of machinery, Part 2: Technical principles
DIN EN ISO 14121-1 Safety of machinery, Part 1: Risk assessment
DIN EN 61326-1
Authorized person for the technical documentation:
Detlef Opp
Stockland3
D-56412 Niederelbert
Niederelbert, 1. April 2010
Detlef Opp, Head of Technical documentation
Signature
Thermo Thermo Scientific Barnstead GenPure with xCAD
a Ultrapure water system
Preface
Dear Sir or Madam,
In deciding to purchase a high-purity water system of type GenPure with xCAD you have se-
lected a high-quality product.
Thank you for the confidence you have placed in us.
Before you start to install and operate your pure water system, please carefully read the infor-
mation given in these Operating Instructions on how to correctly carry out installation and how
to properly operate the system.
This is particularly important, as we, the manufacturer, cannot accept liability for any damage
occurring as a result of improper operation of this system, or from use of it for other than the
intended purpose.
Niederelbert, 20.03.2008
Thermo Thermo Scientific Barnstead GenPure with xCAD
iad ns Ultrapure water system
1. Contents
1- Greg) (=) 6) Scere ener eee oe eee nt A ne ee E te meres erent eer 4
2. Explanatory notes on the operating instructions ................:::eceeeeesseeeeeeees 6
3. Transport and packaging vcvcssiccccinecstsnonsaresturcrnceeonesesn vecsuitenzenvcriueduedéces T7
3.1 Examination On reCeipt ...........cccccecccecccecccceecceeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeettes 7
3.2- COMPLAINS sensensa a a a a Ea avin e E RE EENE 7
3.3 Packaging and return SHIDMENE: .xccicsrtaloacecsccte: steeesteteatedsatean sdanteetictdetnaucsassDibestcendidesaseans Bene 7
4. Safety precautions axcsariiisssccitessscuceswsdartadenkadissanccdalawicdestemcuctanGiiveaiantdens 8
5. Intended purpose ecpiiecsctccccpaneddd ainetatausenievecdvanewsaenreid anesiebioreeecsdenuecdndans 10
5:1 Application areas iiron ds ain in ee aie i es 10
6. Extent of delivery so iiccccomntonwuerecetaasematorntwcaiubinidecsdeddemeconemuccameatumnedes 11
7. Technical specifications ice siiciecsnevsicianieabisidesanclucietumeciaeeneeas 13
8. Description of how the systems fUNCTION...............ccccceeeeeeeeeeeeeeeaeeeeeeeeees 17
8.1 Flow chart, GenPure Standard with xCAD o.oo... ccc cccccceeesceeceseeceeeeeeeeeeeseeeeeeeaseeeeeeenanes 18
8.2 Flow chart , GenPure UV with XCAD..... ccc cccccccsceeceeseeeeeeeeeeseeeueeeeeeeeeueeeaeeenens 19
8.3 Flow chart, GenPure UF with xCAD ....... ccc ccc ccesceceseeeeseeeesseeueeseceeeeeeeeeeeseueueeeaseenaess 20
8.4 Flow chart, GenPure UV/UF with XCAD uu... ccc cc ceccce esse ecseeeceeeeeeseeeseeeseueaeeeeeeeenegs 21
8.5 Flow chart, GenPure UV-TOC with XCAD uo. ccc ccccccccsseeceseeceeeeueeeeeeseeeeseeeeeueeneenaees 22
8.6 Flow chart, GenPure UV-TOC/UF with XCAD o.oo ccc cccceceecsseeceseeseeeeeeseeeeeseeueeeeseeeanes 23
9. Setting up the system ccc sanceesccceassilenndernanetincciaccewessceassuectenouberetietoaeedios: 24
9.1 Installation Area cccncccacacensveaasntccareauareesarauadehenencgansay aattnnastdedanavasxacaounntessabeaseeacnareoneecesmuaeonts 24
9.2 OS Ui a aerarii ee a ea A eaa e A E a S ete 25
9.3 General setting up of the system / bench version XCAD ...........c:ccceeeeeeeeeeeeeeeeeeeeeeeeeeeeeaaas 26
9.4 Setting up the system / wall version XCAD.............::::::ccceeeeeeeeeeseeeeeeeeeeeseeeeseeeeeeeeeeneeeeences 27
9.5 Wall mounting GenPure system asa scetassinteetiincencostscigeeddecacheualeidsesiaeateiecastegetiavsadanuncdeaeatvatdee 30
9.6 Mounting the power pack (voltage supply)........eessssssssereesseseerirrrerrreeesirrrrrnnnsssrnnnnnrnsssseene 31
9.7 Examples of system Set-UDS ...............ccceeeeeeeeeeee eect eeee cece eeeeeegeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeeneeeees 32
10. Putting the system into OperatiOn.................cccccecseeeeeeeeeeaeeeeeeeeeeeeneeeeeees 34
11. Operating SClOMISIIS vessss a sacceveviieaverwctccrsicevdiinsssnuicbdusawevesteytcem andiddsaatetee 35
12: System control oecite ie e rE EERE AEE E EREE EERE 36
TZA MENU ise aa cai a E E E E eects aad te cor eagaane 37
12.1.1 Feedwater conductivity: .2der0tdcedencotendtlenstienstacestaelsidadastnedeasdsagbtenticcns peoelaedesveldsdnecere? 37
12.1.2 Ultra pure water limiting value: ncsucredincicttiobndnsetinaatmretdccunetdbasattetatieanehetnetsiealderendss 37
12.1.3 UV-Lamp operating time and intensity: ............ccccceeseeeeenceeeeeeeeeeneeeeeeeeeeeeeeeneseeeeeeees 38
12.1.4 Filter cartridge operating time counter: ..............:ccccceeceeenceeeeeeeeeeeeeeeeeeeeeeeneneeneeeeeeees 38
12:14:95 RINSING arnncmntcedssteaanscecmebicantesnneenacancatenxantteds aldo aa Aaa ARARAT T ANNESSA 38
12.1.0 [DISIMPOCUON sccdictsnsacnicxerecvariiis stcunlnccaddicbadue sa cecita ie daeesunka dana CaA Eaa EEA EAEE NENEA 39
Thermo Thermo Scientific Barnstead GenPure with xCAD
SCIENTIFIC Ultrapure water system
12.1:-7 Display of TAGE SIC AGS sain es ca saci tee ttccendcteadaeedededeicanas tenier ii eiki 40
12.1280 PCIE OU sssri taan aE EEA Ra ea 41
12.1.9 Unlocking the system ..........ssssesssseeeeesseesesirirttttetttrrrritttteeeertrinttnsssstttnnnnnnnnnatenennnnnnat 41
12-2 QEM MENU cag ttacgeetenacttaieh tacts cceamiah eerie aed ta vesen enti dati cleoet EAEan aain 43
12.2.1 Setting the maximum operating temperature: .......... eee eeeeeeeee cette eeeeeeeeeeeeeeeeeeeeeeaaae 43
12.2.2 Setting the rinsing TMG igccsisicasss cetnvecdcepeas nebaetucverks cana eabocebhiceebeavansayuantnedeseccaanaanevedte 44
12.2.3 Changing the disinfection time: scccccccv.cirs.0sse-seceeeneav.ssanduc tes bicanadede udanendecndedes duane stones 44
12.2.4 Setting the interval pump tiMe?............... ccc cceceeeneeeeeeeaeeeaeeaaeeeaeeaaeeaaeeaaaeaaaeaaeeaaasaaaeees 44
12.2.5 Setting the interval rinse LIMO! as stviccctrctetniincincaredcteatdsieatsneeientasteeardsuonseteeaebidaanncendbs 45
12.2.6 Setting the real-time clock: ....ussssssiseeesesesesssessssorosrrrrnnnnnrrrrnnnunnunuonnnnnnnnnuenaaeeeeeneeeee 45
12.2.7 Setting the sending interval: caisscecscccccevsanaisacttecertataraecanedeoseschanavehduk us tedeeerevxarkieasminetss 45
12.2.8 Selecting the lANQUAGE fiiccicciassidcancccnseneanunnd stdecebaeian Gans scuiebinantexaion santnmdeneetanaviamicents 46
12:29. SWwitehing WING inini ian a anehe ee Rani daad iani aaa A aana a S4ecicitcaaddgacatenrs 46
12.2.10 Switching temperature compensation on or Off: .............::ccccceseeeeeeeeeeeeeeeeeeeeeeeeaeeees 46
12.2.11 Entering the system type and serial NUMDE-?.............ccccceeeeeeeeeeeeeeteeeeeeeeeteeeeenaaaeees 47
12.2.12 Water dispensing via volume control ............:cccceeeeseeeeneeceeeeseeeeeseeeeceeeeseeneseenenseeees 47
12.3 Printer output.. s-ren cece cece cece cece cece cece eect eee dane aan EE EE EEE EEEEEEEE EEE EEE NE EA TERE A Eanan i Ra nina EEA 48
‘12st. Standard (MESSAGES: cre. kaencstasnsscisncdceatiderathanaeumedtaateaag deena tictudtetahdealegteinedeteetaadanactyinens 48
12.3:2 Code messages a cat Sica i neta ssc a heeds alps decedent eal 48
12:3-3 Fault IIMS SAS eenia N EE a O E 49
13; TEMAS ANG -srra n aaa boc oo aia EE aE EE entiey 50
13.1 Maintenance intervals .............nnsnssssrnssesrnrnnrnnsssussnenrsnneeesocoosssarnstrrrrnrrrnnnnnneurnnnnnunaauseeeenee 51
13.2 Replacing the filter CANN Ss icsetictcticstinceids cabipecdddsvalaiademeatlatnots tnesssouelesaaldesendioacubacetstes 52
13:3: DISINTSCHUO Negrie ieee tees eecwte see dea secect cece es eas neous mada E E 53
14: Waste disposal css ssa ic nieri ea eae e aa AEEA aE EEEa 55
15. Trouble shooting..............esseoenenneeonnnnneernnnnneernnnnnternnnnrrennnnnerennnnennnnnn nne 56
16. Replacement parts and consumables ................ccccseeeeeeeeeeeeeeeeeeeaaeeees 58
16:1 GenPU Gins aa aaa aa aeaa ora a aa i aAa nee meee 58
16 2- XSAD ee a ene ee era rer ee ree ee rere eer ree 59
17. Consumables and accessories .........ccceeee cece eeeeeeeeeeeeeeeeeeeeeeeeeaaaaeeeeeeees 60
18. Terminal ASSIGNING sis i12s orrtaerencinrnscadeetednnecincemernetatedadiauenetcotss 62
19. Maintenance (ECON cso eectteasetcce ianamprge seeds ate Gaakie cence tetherewncie 63
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
2. Explanatory notes on the operating instructions
d:
(SA
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EU Mark of Conformity
CSA - admission
Important operating and/or maintenance instructions! Read the oper-
ating instructions with due care.
Risk of electric shock! Electrical work on the system is only to be car-
ried out by qualified personnel.
General information! Particularly important notes are marked with this
information sign.
Protective conductor connection
Connect the power supply to an electrical socket with a protective
connection.
The information provided in these operating instructions is only valid for the system which has
the serial number which is to be entered on the front page.
Please enter the serial number* of your GenPure with xCAD
system in the space provided on the front page.
* Read the serial number of your ultra pure water system from the type plate.
For quick and correct service, please include the following information on all inquiries and re-
placement parts orders which relate to your system:
- The serial number
- The article number
Thermo Thermo Scientific Barnstead GenPure with xCAD
SETE Ultrapure water system
3. Transport and packaging
Ultra pure water systems are carefully checked and packed prior to shipment but, despite this,
there is always a possibility that damage could occur to them during shipment.
3.1 Examination on receipt
> Check the completeness of the delivery against the shipping papers.
Is the packaging damaged?
> Check the system for damage.
3.2 Complaints
Should the system have been damaged during transport:
> Immediately contact the post office, railway or forwarding agent*.
> Keep the packaging, including the outer cardboard box, for a possible inspection
and/or return shipment.
3.3 Packaging and return shipment
Whenever possible use the original packaging and packing materials.
Should these no longer be available:
> Pack the system in packing film and then in a strong cardboard box so that it is held
shock-proof.
* Complaints are only valid for 6 days (after receipt of the goods).
After this time, the right to claim for damages expires.
Thermo Thermo Scientific Barnstead GenPure with xCAD
ee ee Ultrapure water system
4. Safety precautions
For your own safety, please observe the above safety precautions!
> GenPure series systems are modern ultra pure water systems that are intended ex-
clusively for the purification of tap water of drinking quality that has been previously
treated by reverse osmosis, ion exchange or distillation.
> Do not install the system and operate it until you have read through the appropriate in-
formation that is given in these Operating Instructions.
> Lifting and carrying the ultra pure water system, e.g. to the installation location, should
be carried out by two people. To lift it, each takes hold of it under the base plate at two
corners.
> — The CE-Mark becomes invalidated when constructional changes are made to the sys-
tem or when products of other manufacturers are installed in it.
> Protect the system from frost.The temperature at the installation area must be at least
+2°C.
> Observe all general requirements and regulations, including current accident preven-
tion regulations, that are applicable at the ultra pure water system installation area.
> The feedwater pressure must be at least 0.1 bar and at most 6 bar. Should the feed-
water pressure be higher, then an additional pressure reducer must be installed.
> Water purification systems must have a safety device acc. to DIN EN 1717 to protect
the tap water from contamination.
> A grounded 100 - 240V/ 50/60Hz socket must be available.
> The installation area must be equipped with a floor drain with at least DN 50 pipe (40
mm o.d.).
> When the system is to be wall-mounted, first check the statics of the wall. It must have
sufficient load-bearing capacity (for weights, see the technical specifications).
> The maximum operating temperature is +40°C.
> When the system will be at a standstill for a longer period (e.g.or during long holidays),
proceed as follows:
— Switch the system off.
— Close the supply of feedwater to the ultrapure water system.
Damage to the pump will occur should the supply of feedwater be turned off with the
system still on. The manufacturer does not accept liability should such damage occur.
> — When planning the installation of the system, ensure that there will be sufficient work-
ing room for convenient operation of the system and for maintenance such as chang-
ing the filter cartridge and opening, breaking and checking connections.
Thermo Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
> The term of the guarantee is12 months!
> — Never look directly at a switched-on UV-lamp, because UV light endangers eyesight!
Never switch the UV-lamp on when is has been taken out of the metal cylinder!
> Only authorized personnel are to carry out UV-lamp replacement.
Thermo Thermo Scientific Barnstead GenPure with xCAD
Se Ultrapure water system
5. Intended purpose
The continuous increase in ultra pure water quality requirements, technologies that are increas-
ingly more sophisticated, lowered detection limits in laboratories and the need of for user-
friendly systems and complete solutions were the basic for the development of the novel ultra
pure water systems that we call GenPure with xCAD.
GenPure with xCAD has been specifically developed for the production of salts-free, organically
pure, particle-free and sterile filtered ultra pure water.
To ensure long service lives of the high-quality purification media, this type of ultra pure water
system must be fed with water from upstream pre-purification steps (reverse osmosis, ion ex-
change, distillation).
5.1 Application areas
- Analytical techniques in laboratories:
- HPLC ( High Performance Liquid Chromatograhy )
-IC ( lon Chromatography )
- ICP ( Inductive Coupled Argon Plasma )
- AAS ( Atomic Absorption Spectrophotometry )
- TOC-Analysis ( Total Organic Carbon )
- DNA-Research
- etc.
- Preparation of reagents and solutions:
- Cell culture media
- Tissue culture media
- Make-up water for reagents for
online automatic analyzers
- Ultra pure water for demanding laboratory rinsing processes
10
Thermo Thermo Scientific Barnstead GenPure with xCAD
SEEE Ultrapure water system
6. Extent of delivery
The GenPure with xCAD ultra pure water system is available in the following versions:
GenPure Standard, article no. 50131286 (Basic system) with xCAD, bench version
GenPure Standard, article no. 50131300 (Basic system) with xCAD, wall version
GenPure UF, article no. 50131250 (Basic system + Ultrafiltration module) with xCAD,
bench version
GenPure UF, article no. 50131302 (Basic system + Ultrafiltration module) with xCAD,
wall version
GenPure UV, article no. 50131254 (Basic system + UV-photooxidation) with xCAD,
bench version
GenPure UV, article no. 50131317 (Basic system + UV-photooxidation) with xCAD,
wall version
GenPure UV/UF, article no. 50131252 (Basic system + UV-photooxidation + Ultrafiltration
module) with xCAD, bench version
GenPure UV/UF, article no. 50131315 (Basic system + UV-photooxidation + Ultrafiltration
module) with xCAD, wall version
GenPure UV-TOC, article no. 50131296 (Basic system + UV-photooxidation and TOC meas-
urement) with xCAD, bench version
GenPure UV-TOC, article no. 50131321 (Basic system + UV-photooxidation and TOC meas-
urement) with xCAD, wall version
GenPure UV-TOC/UF, article no.50131298 (Basic system + UV-photooxidation and TOC meas-
urement + ultrafiltration) with xCAD, bench version
GenPure UV-TOC/UF, article no.50131323 (Basic system + UV-photooxidation and TOC meas-
urement + ultrafiltration) with xCAD, wall version
(Please check your version against the article number given on the delivery note)
1x GenPure with xCAD (acc. to the version) Article no. 5013xx
incl. Assembly kit for bench and wall version,
consisting of: Article no. 50131283
(bench version)
Article no. 50131380
(wall version)
Filter cartridge for the ultra pure water system Article no. 09.2005
Sterile filter capsule, 0.2 um Article no. 09.1003
PE-Hose 8 x 1mm, 2 m Article no. 18.0036
PE-Hose 6 x 1mm, 5m Article no. 18.0047
PE-Hose 4 x 1mm, 5m Article no. 18.0053
SUB-D Extension cable, 25-pin, 5 m, 2x Article no. 16.0375
Screw, 4 x 40 mm (only wall version version) Article no. 21.0001
Plug, 2 x S8 Article no. 21.0035
Screw hook 2 x 5,2 x 50 mm Article no. 21.0057
Plug 4 x S6 (only wall version) Article no. 21.0002
Operating Instructions Article no. 50131281
Tabletop power pack, 24V DC Article no. 50134196
Universal adapter Article no. 21.1006
Universal holder Article no. 21.1007
Connecting cord (rubber connector to nema plug connector) Article no. 50132200
Connecting cord (rubber connector to british ST plug connector) Article no. 50132203
Connecting cord (rubber connector to euro plug connector) Article no. 50132215
11
Thermo Thermo Scientific Barnstead GenPure with xCAD
ile kali Ultrapure water system
Feedwater connector kit Article no. 25.0075
consisting of:
Union nut, R 3/4“ Article no. 14.0003
Insert, R 1/4“ Article no. 14.0189
Screwed connector, R 1/4“ Article no. 14.0075
Gasket, R 3/4" Article no. 21.5008
PE-Hose, 8 mm o.d., 2m Article no. 18.0036
Dirt-trap sieve for union nut, R 3/4“ Article no. 14.0390
12
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
7. Technical specifications
| Demands on the feedwater |
Source
Tap water pretreated by reverse osmosis, ion ex-
change or distillation.
Silt density index (SDI)
max. 1 for all versions. For water that is not pretreated
by reverse osmosis, a prefilter with a 1 um membrane
is recommended.
Feedwater resistance >0.5 MOxcm
Free chlorine max. 0.05 ppm
TOC max. 50 ppb
Bacteria count < 100 CFU/ml
Turbidity <1.0 NTU
Carbon dioxide (CO2) max. 30 ppm
Silicate max. 2 ppm
Particles Filtration to 0.2 um is recommended to protect the in-
ternal filter and, if appropriate, the final filter.
Temperature 2-35°C
Pressure 0.1 - 6 bar
Product water quality
Standard
UV-
UN UF TOC/UF
Resistance
(Reference
temperature
25°C)
18.2
TOC
Bacteria
<1 <1 <1
Bacterial En-
dotoxines
< 0.001*| <0.001* < 0.001*
Particles
Flow rate
L/min**
< 1/ml < 1/ml < 1/ml
Flow rate with
L/min
volume control
* Depending on feedwater and appropriate disinfection
** Depending on feedwater pressure
Dimensions, GenPure
Height
615 mm
Width
372 mm
Depth
330 mm
Weight:
GenPure Standard
GenPure UF
GenPure UV
GenPure UV/UF
GenPure UV-TOC
GenPure UV-TOC/UF
13
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
Dimensions, xCAD (bench version)
approx. 725 mm
260 mm
approx. 530 mm
12 kg
approx
Dimensions, xCAD (wall version)
approx. 655 mm
260 mm
approx. 530 mm
Weight
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14
Thermo Thermo Scientific Barnstead GenPure with xCAD
AAEE Ultrapure water system
Cell constants, measuring cells
Conductivity, feedwater 0.16 cm“
Conductivity, after UV-photooxidation 0.01 cm“
Conductivity, ultra pure water 0.01 cm“
Connectors for water genpure
Feedwater Hose, 8 mm o.d.
Rinse water Hose, 8 mm o.d.
Ultra pure water/outlet Hose, 6 mm o.d.
Ultra pure water/recirculation Hose, 4 mm o.d.
Connectors for water, xCAD
Ultra pure water/inlet Hose, 6 mm o.d.
Ultra pure water/recirculation Hose, 4 mm o.d.
Ultra pure water/outlet R 1/4"
Sterile filter outlet Hose, 8 - 10 mm o.d.
Electrical connections / external switched mode power supply
Input voltage AC 100 — 240 V, 50 — 60 Hz, 5 - 3.8 A
Output voltage DC 24 V, 3,8 A
System connection DC 24 V, 80 W
Serial interface RS 232
Protection Class Class II (external SMPS certified as Class I)
Electrical connections, xCAD
2x SUB-D socket 25 pin
Airborne sound emission
Sound-pressure level 49 db(A)
Ambient conditions (DIN EN 61010-1 (VDE 0411-1):2011-02)
Usage Indoor rooms
Height Up to 2000 m
Temperature range From 5° C to 40° C
Relative humidity Maximum relative humidity 80 % at temperatures of
up to 31° C, linearly decreasing to 50 % relative hu-
midity at 40° C
Line-voltage variation Not more than + 10 % of the line voltage
Transient overvoltages As usually occur in the supply network (overvoltage
category II acc. to IEC 60364-4-443).
Note: The rated level of transient overvoltage is the
withstand impulse voltage acc. to overvoltage cate-
Il of IEC 60364-4-443
Ventilation requirements There are no special requirements with regard to ven-
tilation.
Degree of pollution 2
15
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
Materials of parts that contact water
Pressure reducer
NBR
Pump head
Nylon with glass fibre
UV-Lamp
High purity quartz
UV-Housing
Stainless steel
Filter cartridge
PP
UF-Housing
Polycarbonate
Rinsing solenoid valve
Dispensing valve
Conductivity measuring cell
POM, stainless steel
Distributor block
POM
Connections
POM
Hoses
Gaskets
16
PE
Thermo Thermo Scientific Barnstead GenPure with xCAD
SETE Ultrapure water system
8. Description of how the systems function
GenPure versions: Standard, UV, UF, UV/UF with xCAD
Tap water that has been pretreated upstream by reverse osmosis, ion exchange or distillation
passes through a pressure reducer and into the GenPure ultra pure water system, where the
conductivity is monitored. A pump forces this feedwater through UV-photooxidation (only with
GenPure UV and GenPure UV/UF) and the filter cartridge, from where it flows through an ul-
trafiltration module (only with GenPure UF and GenPure UV/UF), after which the conductivity is
measured by a special conductivity measuring cell (with temperature compensation).
When ultra pure water is taken from the system, it flows through a sterile filter before reaching
the dispensing outlet. During interval operation, the water is circulated around an internal circuit
at regular intervals.
GenPure versions: UV-TOC, UV-TOC/UF with xCAD
Tap water that has been pretreated upstream by reverse osmosis, ion exchange or distillation
passes through a pressure reducer and into the GenPure ultra pure water system, where the
conductivity is monitored. A pump forces this feedwater through UV-photooxidation, after which
the conductivity is again measured to determine the TOC-value. The water then flows through
the filter cartridge and an ultrafiltration module (only with GenPure UF-TOC/UF), after which the
conductivity of it is measured by a special conductivity measuring cell (with temperature com-
pensation).
The TOC value is calculated by taking the difference between the values measured by the
measuring cells QIA300 and QI302.
The measurement range is 0 - 30 ppb.
When this measurement range is exceeded, the number 99 is shown in the display instead of
the measured value.
In Stand-by operation, "___" is shown instead of the measured value.
When ultra pure water is taken from the system, it flows through a sterile filter before reaching
the dispensing outlet. During interval operation, the water is circulated around an internal circuit
at regular intervals.
17
8.1 Flow chart, GenPure Standard with xCAD
peisewasser
Eingan
Feedwater inlet `
A-F1
A-F2
A-P1
FIS400
QIA 300
QIA 301
TIA 500
18
GenPore Standard
Abfl
rain
TIL
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
Filter cartridge
Sterile filter
Circulation pump
Digital flowmeter
Conductivity, feedwater
Conductivity, ultra pure water
Temperature sensor
Pressure reducer
Check valve
Solenoid valve
Rinsing solenoid valve
Check valve 1 bar
8.2 Flow chart , GenPure UV with xCAD
peisewasser
Ein si i m>
Feedwater inlet
A-F1
A-F2
A-P1
A-UV1
FIS400
QIA 300
QIA 301
TIA 500
GenPore
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
z
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=
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Filter cartridge
Sterile filter
Circulation pump
UV-Photooxidation
Digital flowmeter
Conductivity feedwater
Conductivity, ultra pure water
Temperature sensor
Pressure reducer
Check valve
Solenoid valve
Rinsing solenoid valve
Check valve 1 bar
19
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
8.3 Flow chart, GenPure UF with xCAD
peisewasser
Eingar
Feed
ater inle
A-F1
A-F2
A-F3
A-P1
FIS400
QIA 300
QIA 301
TIA 500
20
Lh
GenPure LF
=
i
1
=o
|
© o Z -F
Filter cartridge
Sterile filter
Ultrafiltration module
Circulation pump
Digital flowmeter
Conductivity, feedwater
Conductivity, ultra pure water
Temperature sensor
Pressure reducer
Check valve
Solenoid valve
Rinsing solenoid valve
Check valve 1 bar
KZ
Reinstwasser
Itrapure water
rain
Thermo Thermo Scientific Barnstead GenPure with xCAD
SETE Ultrapure water system
8.4 Flow chart, GenPure UV/UF with xCAD
GenPure F
ala L EIS í ` AF3 QIA YTIA
peisewasser 3 1 ak ou) N v3
Eingan D ec | L . } X
I \
Feedwater inle v ” i LX
po A-F Ke
pa
Reinstwasser
ltrapure water
rain
A-F1 Filter cartridge
A-F2 Sterile filter
A-F3 Ultrafiltration module
A-P1 Circulation pump
A-UV1 UV-Photooxidation
FIS 400 Digital flowmeter
QIA 300 Conductivity, feedwater
QIA 301 Conductivity, ultra pure water
TIA 500 Temperature sensor
V1 Pressure reducer
V2 Check valve
V3 Solenoid valve
V4 Rinsing solenoid valve
V5 Check valve 1 bar
21
peisewasser
Eincan
Feedwater inle
A-F1
A-F2
A-P1
A-UV1
FIS400
QIA 300
QIA 301
QI 302
QIA 303
TIA 500
22
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
Filter cartridge
Sterile filter
Circulation pump
UV-Photooxidation
Digital flowmeter
Conductivity, feedwater
UV-Intensity
Conductivity, TOC measurement
Conductivity, ultra pure water
Temperature sensor
Pressure reducer
Check valve
Solenoid valve
Rinsing solenoid valve
Check valve 1 bar
Reinstwa
Itrapure
arer
Eingan
eedwater inle
2 m
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
A-F1
A-F2
A-F3
A-P1
A-UV1
FIS400
QIA 300
QIA 301
QI 302
QIA 303
TIA 500
ala \TIA
Filter cartridge
Sterile filter
Ultrafiltration module
Circulation pump
UV-Photooxidation
Digital flowmeter
Conductivity, feedwater
UV-Intensity
Conductivity, TOC measurement
Conductivity, ultra pure water
Temperature sensor
Pressure reducer
Check valve
Solenoid valve
Rinsing solenoid valve
Check valve 1 bar
Reinstwasser
ltrapure water
23
Thermo Thermo Scientific Barnstead GenPure with xCAD
Se re Ultrapure water system
9. Setting up the system
9.1
Installation area
Take the following criteria into consideration when selecting the installation area:
24
Vv
Feedwater pressure at least 0,1 bar, at most 6 bar
Lowest temperature +2°C
Level standing surface
When the system is to be wall-mounted: A smooth wall is required. Check the statics
of the wall, it must be sufficiently loadable (for weight, see Technical specifications)
Floor drain, DN 50
Free gravity fall to drain.
Should no such floor drain be available, then, for safety reasons, a water watcher (ar-
ticle no. 16.0129) must be installed!
Free gravity fall to drain must be ensured !
Safety socket, 100 - 240V, 50/60Hz
Sufficient working space around the system (filter replacement, etc.)
It must be easy to operate and monitor the system
R 3/4" Tap water connector
9.2 Connectors
Genk
re
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
Connectors, GenPure:
Connector for 25 pin sockets (system control)
Connector for 25 pin sockets (system control)
Feedwater connector, 8 mm o.d.
Rinse water connector, 8 mm o.d.
Ultra pure water connector, 6 mm o.d. (to xCAD)
Ultra pure water connector, 4 mm o.d. (to xCAD)
Connector for optional printer (art. no.: 09.2207)
Mains plug/100 - 240V, 50/60Hz power supply
Connectors, xCAD:
Connector for 25 pin sockets (system control)
Connector for 25 pin sockets (system control)
Ultra pure water connector, 6 mm o.d. (to GenPure)
Ultra pure water connector, 4 mm o.d (to GenPure)
Dispensing valve outlet, R 1/4” female thread
Sterile filter 0,2 um
20
Thermo Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
9.3 General setting up of the system / bench version xCAD
1)
2)
3)
4)
5)
6)
26
Proceed as follows to set your GenPure with xCAD (bench version) ultra pure water
system up ready for use:
Stand the GenPure system with the xCAD where it is to be installed.
Remove the cartidge cover from the GenPure system.
Take the plugs off from the filter cartridge and save them.
Push the filter cartridge in the guide in the system, plug the quick-connect connectors on so
that they audibly click into position and put the cartridge cover back on.
Connect the 8 mm o.d. hose that is provided in the connector kit to feedwater connector (3)
of the GenPure system.
Now make a pressureless connection between the 8 mm o.d. hose (4) and the drain.
The drain to the sewer must be max. Are 1m above the rinsing water connector of the Unit.
Plug each of the extension cable cables with 25 pin socket in the sockets (1) and (2) of the
GenPure System and screw them tight.
Then connect the tubing (4 mm and 6 mm) by plugging the connectors (5) and (6) of the
system.
Thermo Thermo Scientific Barnstead GenPure with xCAD
SAE Ultrapure water system
7) Lead the 25 pin plugs/extension cables and 4 mm and 6 mm o.d. hoses through the wall
and connect the 25 pin plug (1) from the GenPure with the socket (1) on the xCAD and the
25 pin plug (2) from the GenPure with the socket (2) on the xCAD.
Caution: Do not interchanging the connections of the 25 pin connector, otherwise no ab-
straction of water possible!
8) Fix the 6 mm und 4 mm o.d. hoses in the hose connectors (5) and 6) of the xCAD.
9) If you intend to use the sterile filter (10) that is standardly supplied, screw it in the R 1/4"
female thread outlet of the dispensing valve (9) of the xCAD.
10) Connect the mains plug (8) of the voltage supply to an earthed 100-240V/50/60Hz socket.
11) Open the feedwater supply.
12) Check all connections for leaks.
9.4 Setting up the system / wall version xCAD
Proceed as follows to set your GenPure with xCAD (wall version) ultra pure water
system up ready for use:
View from below/front
xCAD mit montiertem Wandhalter
xCAD with mounted wall mount Wandhalter
wall mount
- E
N Schrauben 4x12 mm
7 screws 4x12 mm
132
_ 12, | 10
N o 2h 8h
d4
p 5 f
Ne = a
Ol 0O
1) Release the four screws (4x12 mm) marked above from the xCAD underside and
remove the wall mount from it.
27
Thermo Thermo Scientific Barnstead GenPure with xCAD
2)
3)
4)
5)
6)
7)
8)
28
Ultrapure water system
Installing the wall mount
Caution: The included screws and dowels are only intended to fix the wall mount
to a concrete wall or a solid masonry!
The two 25 pin plugs/extension cables and the 4 mm o.d. and 6 mm o.d. hoses can be led
laterally down the wall or be led out through the wall at the back. There are three possibili-
ties for cut-outs for the cable and hoses (see the next diagram).
Note: Only one of these cut-outs is required.
Hold the wall mount at the wanted position on the wall and mark the four boreholes
for the fixing of the wall mount.
Wand
wall
Yypyy min.18
_ YXGF rT
ZZ *
ZZ Z l
Uy Uy,
AY Ao “Yi
Yd AY
VK Ay wo
AN Wij, O
yf VI
Vi VAY
Za:
U :
Wandhalter moglicher Ausschnitt in der Wand, für Kabel-
und Schlauchdurchführung nach hinten
wall mount
possible wall cut- outs for cable
and hose taken out at the back
Bore the holes for the 6 mm plugs and make the necessary cut-out.
Fix the wall mount in position with the plugs and screws provided.
Lead the 25 pin plugs/extension cables and 4 mm and 6 mm o.d. hoses through the wall
to the wall mount and connect the 25 pin plug (1) from the GenPure with the socket (1) on
the xCAD and the 25 pin plug (2) from the GenPure with the socket (2) on the xCAD.
Caution: Do not interchanging the connections of the 25-pin connector, otherwise no ab-
straction of water possible!
Fix the 6 mm und 4 mm o.d. hoses in the hose connectors (5) and (6) of the xCAD.
Now carefully position the xCAD on the wall mount and screw it tight to the wall
mount using the four 4x12 mm screws.
Place the GenPure system at the planned position.
Thermo Thermo Scientific Barnstead GenPure with xCAD
AAEE Ultrapure water system
9) Take the cartridge cover off of the GenPure system
10) Take the plugs off from the filter cartridge and save them.
11) Push the filter cartridge in the guide in the system, plug the quick-connect connectors on so
that they audibly click into position and put the cartridge cover back on.
12) Connect the 8 mm o.d. hose that is provided in the connector kit to the feedwater connector
(3) of the GenPure system.
13) Now use the 8 mm o.d. hose to make a pressureless connection between the system
(connector 4) and the drain. The drain to the sewer must be max. Are 1m
above the rinsing water connector of the Unit.
14) Plug the two extension cables with 25 pin plugs in the sockets (1) and (2) of the GenPure
system and screw them tight.
15) If you intend to use the sterile filter (10) that is standardly supplied, screw it in the R 1/4"
female thread outlet of the dispensing valve (9) of the xCAD.
16) Open the feedwater supply.
17) Check all connections for leaks.
29
Thermo Thermo Scientific Barnstead GenPure with xCAD
eee Ultrapure water system
9.5 Wall mounting GenPure system
Ansicht von hinten
Le acl ide
=
|
ohruncen für
andmontace
J Holes for wall
mountin
ii
Proceed as follows to mount your GenPure system to a wall:
> Use a twist frill (8 mm or 5/16 inch) to make the two holes in the wall that are required as
shown in the diagram above.
> Plug the nylon S8 dowels that are supplied in the assembly kit in the holes. Screw the
5.2 x 50 mm screw hooks that are also supplied in the assembly kit in the dowels.
> Lift the GenPure system (2 people are required for this) and hang the back side of it on
the screw hooks.
30
Thermo Thermo Scientific Barnstead GenPure with xCAD
SIETE Ultrapure water system
9.6 Mounting the power pack (voltage supply)
ack view power supp niversal adapter
> Whenever possible, mount the power pack on the wall to the left or right of the ultra
pure water system where it is freely accessible.
> Stick the universal holder which is supplied in the assembly kit to the back of the
power pack as shown in the above Figure.
> Stick the universal adapter to a smooth wall surface or screw it to the wall using the
dowels and screws supplied in the assembly kit.
> When the universal holder and universal adapter have been fitted, hang the power
pack in.
> Plug the connecting cable (appliance cable) in the power pack socket.
> Connect the power pack to the ultra pure water system (Connectors, GenPure, 4-pin
power supply connector, pos. 8) and to an earthed 100 - 240V, 50/60Hz socket.
> The system is now ready for use.
31
Thermo Scientific Barnstead GenPure with xCAD
Thermo
Ultrapure water system
9.7 Examples of system set-ups
Connection to a pretreatment:
lonenaustuscher DI 1
nicht im Lieferumfang enthalten
lon exchanger Il
not included in extent of delivery
a
i
S
Connecting hose
Connection to a Pacific TII system with storage tank:
Pacific TIITII mit Tank und Vorbehandlun
nicht im Lieferumfang enthalten
Pacific TH/TI with tank and pretreatment
not included in extent of deliver
ag
Anschlussschlauch
Connecting hose —
T
il
rain
32
Thermo Thermo Scientific Barnstead GenPure with xCAD
SETENE Ultrapure water system
Connection to a storage tank:
orratstank nicht im
Lieferumfang enthalten
Storrage tank not included
in extent of deliver
Anschl chlauch
Connecting hose i -
Caution: When connected to a storage tank, the system must be switched to
“nonstop“ operation for ultra pure water dispensing.
33
Thermo Thermo Scientific Barnstead GenPure with xCAD
i lists Ultrapure water system
10. Putting the system into operation
Allow the system to warm up to, or to cool down to, room temperature
before starting it up for the first time.
Check that all hose connections have been made as specified in the
"Setting up the system" section.
I Switch the system on by pressing this button. After a compulsory rinse the sys-
tem switches to the last operating mode.
To vent air from the system, switch the system 3 times successively to
"Rinsing" in the menu and collect and discard approx. 5 litres of water
each time. The ultra pure water limiting value can be gone below during
this procedure.
MONSIG Use this “NONSTOP“-key to switch the system to the “Nonstop“ operating
dlià mode.
You can set the system back to “Interval“ operation when the system has
brought the ultra pure water to the quality you require.
INTERVAL
34
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
11. Operating elements
Intervall — ppb
18,2 MOxcm
18,5°C UV/TC
NONSTOP
Entei
Menu,
INTERVAL
Switches the system on or off
Switches "Nonstop" operation on or, in the menu,
increases a value on display
Confirms the value shown in a menu
point
Switches the menu to the next menu
point
Switches "Interval" operation on or, in the menu,
decreases a value on display
Switches the UV-lamp on or, in the menu,
allows you to select the position in a number
that you wish to change
35
Thermo Thermo Scientific Barnstead GenPure with xCAD
i kali Ultrapure water system
12. System control
General information
A press on the ON/OFF-key causes the system to run in the /nterval operating mode (see Inter-
val mode).
Interval operation then runs automatically every 0.5 hours for the set length of time to ensure
the ultra pure water quality.
When the UV-lamp is on, then the "UV" text message is displayed. When temperature compen-
sation of measured values is active, then the "TC" message is displayed. In addition, the meas-
ured values for the ultra pure water conductivity and the temperature are displayed.
Should a fault exist, then a fault message is given out across the potential-free output and is
shown in line 4 of the display. Should several faults occur simultaneously, then they are alter-
nately displayed.
When the Nonstop-key is now pressed, the system switches to the Nonstop mode, the pump is
started and the solenoid rinsing valve opens for the set rinsing time. Nonstop operation can be
stopped by pressing the Interval-key. After a wait of 2 hours, the system switches itself back to
the Interval mode.
A press on the UV-key brings "UV" to display. The UV-lamp is only switched on when the sys-
tem is in the Nonstop mode, however. The UV-lamp switches itself off when the Nonstop mode
is ended (2 h). When Nonstop operation is manually stopped by a press on the Interval-key,
then the UV-lamp is not switched off until it has been burning for 0.5 hours.
During the time that the UV-lamp is burning, the intensity of the UV-light in monitored. The dis-
play of the UV-intensity is made in the menu. The TOC-value is also displayed.
User-menu
All of the measured values, operating times and limiting values that are relevant for the user can
be set and read in this menu.
A press on the menu-key brings you into this menu. Each further press on the menu-key moves
you on from one menu prompt to the next.
Settings can be changed with the arrow keys. When you confirm a value by pressing the Enter-
key, you are taken to the next menu prompt. Settings can only be made when the system con-
trol has been previously unlocked (see section12.1.8).
To simplify changing settings, a press on the UV-key allows you to select a certain number in
the numerical value that you wish to change. The arrow-keys can then be used to enter the
wanted number from 0 to 9 at the selected position.
With all three measuring cells for conductivity and with the temperature sensor, a minimum and
a maximum measured value are fixed in the programme. Should measured values be below or
above these values respectively, then it must be assumed that there is a cable break. In such a
case, the appropriate fault message "Measuring cell LF1", "Measuring cell LF2", "Measuring cell
LF3" or "Measuring cell Temp." is displayed in line 4.
36
Thermo Thermo Scientific Barnstead GenPure with xCAD
SIETE Ultrapure water system
12.1 Menu
12.1.1 Feedwater conductivity:
A single press on the menu-key allows the feedwater conductivity to be read and the limit-
ing value of the feedwater conductivity to be set. The fault message that flashes in the
fourth line of the display when the feedwater limiting value is exceeded is "Limit value
feed".
Measuring range, feedwater: 10.0- 0.010 MOxcm
Setting range, limiting value: 0.1- 50.0 pS/cm
Basic setting: 0.5 MOxcm
With settings above 50 uS/cm, the limiting value is switched off and the word "Off" is
shown in the display.
The display shows:
Feedwater
1.25 MOxcm
Limit value feed
2.0 uS/cm
12.1.2 Ultra pure water limiting value:
Two presses on the menu-key in this menu allow the fault display for the pure water limit-
ing value and the pure water limiting value to be set. As soon as the fault display is
switched on, the fault will be displayed both in Stand-by mode and in Production mode.
When the fault display is switched off, the fault is only displayed in Production mode.
The “Lim. val.pure w.” message is displayed when the limiting value is exceeded.
Ultrapure water measuring range: 0.100 MQxcm
Limiting value setting range: 0.055- 5.000 pS/cm
Basic setting: 10.0 MOxcm
Basic setting, fault suppression: On
With settings above 5.000 uS/cm, the limiting value is switched off and the word "Off" is
shown in the display.
The display shows:
Fault message
Stand- by On
Lim. val.pure w.
0.100 uS/cm
37
Thermo Thermo Scientific Barnstead GenPure with xCAD
i ir kali les Ultrapure water system
12.1.3 UV-Lamp operating time and intensity:
In this menu, the operating hours of the UV-lamp are displayed and the input for the UV-
sensor is evaluated.
When the maximum operating time is reached, then the "UV-time" fault message is trig-
gered. The UV-sensor measures the actual intensity of the UV-lamp. The display shows
the % of this compared to the maximum value.
The display shows:
UV Time
0000 h
UV intensity
90%
12.1.4 Filter cartridge operating time counter:
The operating time counter for the filter cartridge is set in this menu by a fourth press on
the menu-key and the entry of a valid serial number for the filter cartridge..
The display shows:
Ser. No.:
Cartridge
Press Enter
omer
12.1.5 Rinsing
38
A fifth press on the menu key in this menu allows rinsing to be carried out if this is neces-
sary. Triggering is made by confirming the requirement with a press on the Enter-key. The
pump is started and the rinsing solenoid valve is opened for the rinsing time period set in
the OEM-menu. During rinsing, the count-down of the rinsing time is displayed
When rinsing has finished, the system returns to the last operating mode (Interval or Non-
stop).
The display shows:
Rinse ?
Press enter
Thermo Thermo Scientific Barnstead GenPure with xCAD
TaS Ultrapure water system
During Rinsing the display shows:
Rinse
30 sec.
12.1.6 Disinfection
A sixth press on the menu-key gives you the possibility of carrying out disinfection. When
this menu-prompt is confirmed with Enter, the command Disinfection cartidge. Install one“
is shown. After confirming this with Enter, disinfection is carried out. The pump runs for the
disinfection time that has been set in the OEM-menu. When the half of the disinfection
time has passed, the rinsing solenoid valve opens and stays open up to the end of the dis-
infection process. The "New filter cartridge. Install one" message is given when the disin-
fection process has finished
On confirming this with Enter, the system returns to the last operating mode.
During disinfection, the count-down of the disinfection time is shown in the display
The display shows:
Disinfection
Press enter
After confirnation with Enter, the display shows:
Disinfection
cartridge!
Install one
Press enter
During disinfection, the display shows:
Disinfection
25 min.
39
Thermo Thermo Scientific Barnstead GenPure with xCAD
ee ee Ultrapure water system
After disinfection, the display shows:
New
filterset
Press enter
12.1.7 Display of fault storage:
A seventh press on the menu-key calls the fault storage. Confirmation with Enter allows
you to look through the faults in the fault storage.
Should several faults have occured, then two faults, each with date and time, are shown in
the display. Appropriate pressing of the arrow-keys brings previous and subsequent faults
to display.
A press on the menu-key or the Enter-key returns the display to the last operating mode.
The display shows:
Error history
Press enter
Show of faults in the fault storage:
14.03.04 14.30
Limit value feed
14.03.04 15.30
Lim. val.pure w.
40
Thermo Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
12.1.8 Print-out
A eight press on the menu-key bring you to a menu in which you can hand-request a print-
out.
The display shows:
Print out?
Press enter
0000
12.1.9 Unlocking the system
A nine press on the menu-key in this menu brings you to the “Code” menu. To prevent un-
authorized access to the settings in the system control, changes to the settings can only
be carried out when a correct code from the Assignment Table that follows is entered and
confirmed with the Enter-key.
The unlocking remains active for 5 minutes.
Each access via the code is issued to the printer (RS 232) complete with date, time and
abbreviated code number (“Code 0001” corresponds to code 150, “Code 0002” to code
250 etc.).
The display shows:
Code
Press enter
0000
Code numbers can be assigned to individual persons in the Assignment Table on
the following page.
Please remove this page from the Operating Instructions and store it where it is
safe from unauthorized viewing.
41
Thermo Thermo Scientific Barnstead GenPure with xCAD
42
Ultrapure water system
Assignment Table for code numbers
that allow the system to be unlocked
Printer
Code no. Person
output
150 0001
250 0002
350 0003
450 0004
550 0005
650 0006
750 0007
850 0008
| 950 0009 |
Thermo Thermo Scientific Barnstead GenPure with xCAD
SIETA Ultrapure water system
12.2 OEM-Menu:
Basic settings and limiting values can be changed in this menu.
To make changes in the OEM menu, the system control must previously be unlocked (see
section “Menu” Unlocking the system).
Calling the OEM menu:
Simultaneous pressing of the Interval-key and the Nonstop-key calls the OEM menu. Fol-
lowing this, the prompt "OEM menu Press Enter" appears. When this is confirmed with the
Enter-key, the first menu prompt can be worked on. To simplify changing settings, press
the UV-key to select the number in a numerical value which you want to change. Now use
the arrow keys to enter the wanted number from 0 to 9 at that selected position.
A press on the menu-key takes you to the next menu prompt.
The OEM menu call display shows:
OEM Menu
12.2.1 Setting the maximum operating temperature:
The maximum temperature which the system is to be allowed to reach can be set in this
menu. When this temperature is exceeded, the "max. Temperature" fault message is trig-
gered.
It is shown in the 4th line of the display.
Basic setting: 50 °C
Setting range: 1-50°C
The display shows:
OEM Menu
Max. temp.
35 °C
43
Thermo Thermo Scientific Barnstead GenPure with xCAD
AAEN EEES Ultrapure water system
12.2.2 Setting the rinsing time:
Basic setting: 30 sec.
Setting range: 10 - 60 sec.
The display shows:
OEM Menu
Rinse time
30 sec.
12.2.3 Changing the disinfection time:
Basic setting: 30 min.
Setting range: 15 -90 min.
The display shows:
OEM Menu
Disinfect. time
30 min.
12.2.4 Setting the interval pump time:
Basic setting: 5 min.
Setting range: 1 -30 min.
The display shows:
OEM Menu
Pump interval
05 min.
44
Thermo Thermo Scientific Barnstead GenPure with xCAD
SETE Ultrapure water system
12.2.5 Setting the interval rinse time:
Basic setting: 0.5 sec.
Setting range: 0.1 - 2 sec.
The display shows:
OEM Menu
Rinse interval
0.5 sek.
12.2.6 Setting the real-time clock:
Basic setting: The actual date
Setting range: 1 -12 Month, 1 - 31 day, 0 - 24 h, 0 - 60 min.
The display shows:
OEM Menu
Day 30 Month 12
Year 2008
Hour 12 Min.30
12.2.7 Setting the sending interval:
In this menu, the sending interval is set for transmissions of measured values and fault
messages to the RS 232 interface.
Basic setting: 1 hour
Setting range: 0.5 - 12 hours
The display shows:
OEM Menu
Send interval
08:00 h : min
45
Thermo Thermo Scientific Barnstead GenPure with xCAD
i rials Ultrapure water system
12.2.8 Selecting the language:
Basic setting: English
Setting range: Englisch, French, German
The display shows:
OEM Menu
Language
English
12.2.9 Switching units:
Basic setting: Resistance MOxcm
Setting range: Resistance MOxcm,
Specific electrical resistance MO cm
The display shows:
OEM Menu
uS/cm - MO cm
MOxcm
12.2.10 Switching temperature compensation on or off:
Basic setting: on
Setting range: on, off
The display shows:
OEM Menu
Temp. comp.
On
46
Thermo Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
12.2.11 Entering the system type and serial number:
This menu prompt is for the entry of the system type and the serial number of it. Both en-
tries are given in the headline of each print-out. Settings are made with the arrow keys.
The system type and the serial number can also be briefly seen when the on/off-key is
pressed (on booting).
The serial number has six characters including a slash and can be entered with the arrow
keys just as all other entries.
The display shows:
OEM Menu
Genpure UV UF
S.No.: 9999/08
12.2.12 Water dispensing via volume control
As soon as the Nonstop-mode is selected, then a litre volume is shown in line 2 of the dis-
play. This is the volume of ultra pure water that was last dispensed.
A single press on the push button on the grip allows the litre volume to be changed within
the range from 0.01 bis 65.5 litres by means of the arrow-keys. The UV-key can be used
to position the cursor at a particular number that you wish to change.
A second press on the push button causes dispensing of the volume of water that has
been set. The litre volume shown in the display is the actual volume that has been dis-
pensed. Dispensing stops as soon as the set volume has been reached.
Dispensing can be stopped at any time by a further press on the press button.
Manual dispensing can also be made of any volumes within the set volume by two
presses on the press button to start dispensing and a further press to stop it.
The display shows:
Nonstop 5 ppb
18.2 MOxcm 1.00L
21.3°C UV/TC
47
Thermo Thermo Scientific Barnstead GenPure with xCAD
eee eee Ultrapure water system
12.3 Printer output
Various parameters are recorded by the printer. A differentiation is made between three types of
messages:
- Standard messages
- Code messages
- Fault messages
12.3.1 Standard messages:
Here a record of all measured values is printed out in dependence on the sending interval.
A complete data set is also printed out during NONSTOP-operation.
Print-out:
e.g.: 03.04.08 15:15
GenPure Standard
S.No. 3988/08
Interv. TC on UV off
LF1= 18.2 MOxcm
LF2= 10.0 MOxcm
LF3= 0.000 MOxcm
Temp.= 16.8 °C
TOC= 0 ppb
UV Intens.= 0%
The standard record includes all measured values. With systems that are not equipped
with TOC measurement and UV-intensity measurement, 0 is given as measured value!
12.3.2 Code messages:
Whenever a code number is entered in the system control and confirmed with the Enter-key,
then the code input is immediately printed out.
For code identification refer to the “Assignment Table for code numbers that allow the sys-
tem to be unlocked”.
Print-out:
e.g.: 03.04.08 15:17
GenPure Standard
S.No. 3988/08
Code 0002
48
Thermo Thermo Scientific Barnstead GenPure with xCAD
SETE Ultrapure water system
12.3.3 Fault messages:
When a fault message is shown in the display, e.g. for the ultra pure water limiting value,
then the fault message is printed out at the end of the sending interval.
Print-out:
e.g.: 03.04.08 17:09
GenPure Standard
S.No. 3988/08
Lim val.pure w.
49
Thermo Thermo Scientific Barnstead GenPure with xCAD
See S Ultrapure water system
13. Maintenance
Regular maintenance of your system maintains the value of it. We recommend that you close a
service contract with your service company. You then have the certainty of a high operational
safety and reliability.
NOTE!
To ensure that your system will work reliably for a long time, it must be checked, serviced and
cared for at regular time intervals in accordance with these Operating Instructions.
For this reason, the Operating Instructions must be readily available to operating and mainte-
nance staff at all times, and be carefully followed.
Any maintenance work should become necessary during the validity of the guarantee, this is
only to be carried out by a service professional which is expressly authorized to do such work.
The staff who are trained on and operate the system are committed to carry out daily/weekly
checks.
The maintenance work specified on the maintenance record supplied with these Operating In-
structions should to be carried out weekly.
CAUTION!
The cleaning and disinfection of your system is performed for reasons of hygiene and has no
effect on the technical condition of the system.
The system must only be cleaned and disinfected when algae or slime are detected inside it, or
at least once yearly.
the system off at the mains switch to make it currentless and ensuring that it will not be
inadvertently turned back on. Such work is only to be carried out by qualified electri-
cians
Checks or maintenance work on electrical equipment are only to be made after turning
50
Thermo Thermo Scientific Barnstead GenPure with xCAD
SEE Ultrapure water system
13.1 Maintenance intervals
Consumable materials are to be replaced at the intervals given in the following Table or when
there is a drop in performance:
Material Flow chart no. | Article no. Interval*
Filter cartridge F1 09.2005 12 Months
Sterilefiltercapsule F2 09.1003 12 Months
Ultrafiltration membrane F3 50133980 24 Months
*Please keep in mind that the life of your consumables is directly dependent on the quality of
the feed water and the amount of water used daily. The interval is contingent on the feedwater
quality so that a shorter one may be necessary.
51
Thermo Thermo Scientific Barnstead GenPure with xCAD
i ili cles Ultrapure water system
13.2 Replacing the filter cartridge
(i)
The filter cartridge is to be replaced when the maximum limiting value
that you have set for the ultra pure water is exceeded or when the "New
Filter cartridge" message is shown in the display.
Proceed as follows to replace the filter cartridge:
52
1.
2.
10.
11.
12.
13.
Shut off the supply of feedwater.
Press the press button on the xCAD for water dispensing until no more water
emerges and push it again to stop dispensing.
Switch the system off.
Remove the cartridge cover.
Take off the quick-conects from the feed and ultra pure water sides of the filter car-
tridge and close the connectors with the stoppers you have saved.
Draw the spent filter cartridge out from the guide and push the new filter cartridge in.
Remove the stoppers from the new filter cartridge and save them.
Fit the quick connects to the filter cartridge so that they audibly click into position.
Replace the cartridge cover.
Open the supply of feedwater.
Switch the system on.
Dispense and discard at least 5 litres of water.
To set the operating time counter of the filter cartridge back to zero, enter the serial
number that is given on the filter cartridge as is described in "Filter cartridge operating
time counter" section.
Caution: To do this, the system must be unlocked, as is decribed in the "Unlocking
the system" section.
Switch the system to the "Rinsing" operating mode to vent air out of it.
Thermo Thermo Scientific Barnstead GenPure with xCAD
SETAS Ultrapure water system
13.3 Disinfection
Disinfection should be regularly carried out, at the latest when the filter
cartridge is replaced.
To disinfect the system you require a Disinfection cartridge, article no. 09.2201.
Use cleaning solutions as follows:
MICRO-Chlor Granulate, 1 box, article no. 09.2202 (Europe only)
Cleaning Solution, 1 syringe, article no. CMX 25 (US-market only).
with Micro-Chlor disinfectant to avoid possible health hazards!
À Please observe the information given in the safety data sheet supplied
Proceed as follows to disinfect your system:
1. Switch the GenPure system off.
2. Shut off the supply of feedwater to the system and open the dispensing valve so that
pressure in the system is completely released.
3. Remove the filter cartridge (as under "Changing the filter cartridge" in the Operating
Instructions for the system).
4. _ Unscrew the stopper from the disinfectant cartridge, fill the cartridge with water then
empty the contents of a box respectively a syringe of the cleaning solution into the wa-
ter.
Important! For effective disinfection the cartridge must be completely filled
with water.
5. | Screw the stopper back on the disinfectant cartridge and connect the cartridge in the
system (as under "Changing the filter cartridge" in the Operating Instructions for the
system).
6. Re-open the feedwater supply.
7. | Switch the system on and select the "Disinfection" prompt in the menu. The disinfec-
tion programme is finished after approx. 30 minutes.
8. Switch the system off.
9. Shut off the supply of feedwater to the system.
10. Remove the disinfectant cartridge (as under "Changing the filter cartridge" in the Op-
erating Instructions for the system).
11. | Connect the new filter cartridge in the system (as under "Changing the filter cartridge"
in the Operating Instructions for the system).
Before dispensing water from the system, let water run out for approx.
15 minutes. The system is then ready for use.
53
Thermo Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
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54
Thermo Thermo Scientific Barnstead GenPure with xCAD
SEE Ultrapure water system
14. Waste disposal
When the packaging is no longer needed it can be disposed of as household waste.
Systems are in conformity with EEC Guideline 2002/95/EC
The system is not to be thrown away as household waste but must be properly disposed of. It
can be returned to the manufacturer for safe disposal according to EEC Guideline 2002/96/EC.
We therefore request our customers in Germany and other member States in the European
Economic Area to contact our local service centre or our headquarters:
Thermo Electron LED GmbH
Stockland 3
D-56412 Niederelbert, Germany
WEEE-Reg.-no.: DE 12471402
In countries outside of the European Economic Area, please contact your local authorities or
waste disposal company.
55
15. Trouble shooting
The system does not start
Thermo Scientific Barnstead GenPure with xCAD
No supply of power
Ultrapure water system
Provide power
Dispensing not possible
Feedwater tap is closed
Feedwater and rinse water
connections mixed up
Feedwater pressure
< 0.1 bar
Open feedwater tap
Correct the connections
Increase feedwater pressure
Resistance < 18.2 MOxcm
System has a UF-module
(higher conductivity
possible)
lon exchange capacity
exhausted
Replace filter cartridge
with a new one
System control no longer
reacts
Improper operation
Unplug the mains plug for
5 seconds
Water flows out
Leaky hose connection
Feedwater pressure > 6 bar
Check and seal the hose
connection
Install a pressure reducer
Dispensed water flow rate is
too low
UF-Module blocked
Pre-pressure too low
Internal pressure too low
Replace UF-module
Increase pre-pressure
Readjust pressure reducer
Wrong time or date
Time zone
Summer/winter time
Reset time and date
Wrong language
Wrong language set
Correct language setting
Fault message:
"Limit value feed"
56
Feedwater conductivity
too high
Limiting value set too low
Check the pretreatment
Check and suit the limiting
value
Fault message:
"Lim. val.pure w."
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
Filter cartridge exhausted
Limiting value set too low
System has a UF-module
(higher conductivity
possible)
Replace with new filter
cartridge (art.-no.: 09.2005)
Check and suit the limiting
value
Fault message:
"UV-time"
UV-Lamp operating time
has been exceeded
Replace the UV-lamp
(art.-no. 09.2002) and reset
the operating time counter
(see 12.1.4)
Fault message:
"UV-intensity"
UV-Lamp intensity no
longer sufficient
UV-Sensor dirtied
Limiting value set too low
Replace and measure in
a new UV-lamp
Clean UV-sensor
Check and suit the limiting
value
Fault message:
"max. Temperature"
The temperature in the
system is too high
Interval pump time too long
Limiting value set too low
Feedwater temperature
too high
Reduce temperature by
running water off
Reduce interval pump time
Check and suit the limiting
value
Reduce feedwater
temperature
Fault message:
"Measuring cell LF1"
Fault message:
"Measuring cell LF2"
Measuring cell cable break
System control defect
Conductivity of ultra pure
water ouside measuring
range
Measuring cell cable break
System control defect
Feedwater conductivity
ouside measuring range
Replace measuring cell
Replace system control
see "Conductivity
< 18.2 MOxcm"
Replace measuring cell
Replace system control
see “Limit value. feed“
Fault message:
"Measuring cell LF3"
Fault message:
"Measuring cell Temp.
Measuring cell cable break
System control defect
Measuring cell cable break
System control defect
Replace measuring cell
Replace system control
Replace measuring cell
Replace system control
Fault message:
"New Filter cartridge"
Filter cartridge operating
time has expired
Replace with new filter
cartridge (art.-no.: 09.2005)
57
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
16. Replacement parts and consumables
16.1 GenPure
10 f - ©
OR | 12
T i 11 J
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No. | R+I no. | Article desigantion Article no.
1 A-F1 Filter cartridge 09.2005
2 A-UV1 Replacement UV-lamp 09.2002
3 A-P1 Pressure booster pump 19.0050
4 |A-F3 Ultrafiltration module (optional) 50133980
5 |V4 Rinsing solenoid valve 50131190
6 V1 Pressure reducer 50133985
7 FIS400 | Flowmeter 15.0100
8 QIA300 | Conductivity measuring cell, feedwater 16.0126
9 Adapter board 16.0364
10 Microprocessor-system control, interface 50131346
11 Booster for UV-lamp (optional) 22.0088
12 |QIA303 | Conductivity measuring cell, ultra pure water 50133992
TIA500 | Conductivity measuring cell, temperature sensor
13 | V2 Check valve 15.0009
14 |QIA301 | UV-Intensity sensor (optional) 16.0222
15 |V5 Check valve 15.0019
16 Fuseholder for glas tube fuse, 5x20mm 50133979
Glas tube fuse, 5x20mm, 3.15 A, slow 50131758
Table top power pack, 24V DC (not showns) 50134196
Ui)
58
We ask for your understanding that the guarantee that we give becomes
invalidated when replacement parts, accessories or consumables from
other manufacturers are used in or for the system, as we have no influ-
ence on their appropriateness, composition or quality.
Thermo Scientific Barnstead GenPure with xCAD
Ultrapure water system
16.2 xCAD
19
18
|
|
|
|
|
|
Z anal
I? ( |
e=
No. | R+I no. | Article designation Article no.
17 Microprocessor-system control 26.0025
18 |A-F2 Sterile filter capsule, 0,2 um 09.1003
19 Press button 16.0370
20 |V3 Solenoid valve 15.0101
Extension cable SUB-D, 25 pin, GenPure/xCAD 16.0375
59
Thermo Thermo Scientific Barnstead GenPure with xCAD
eee Ultrapure water system
17. Consumables and accessories
Article designation Article no.
lon exchanger system DI 1500 02.1500
Disinfection agent, MICRO-Chlor (pack of 12 cans, Europe only) 09.2202
Cleaning Solution, 1 syringe (US-market only) CMX25
Disinfection cartridge 09.2201
Printer 09.2207
Qualification documents IQ, OQ IOQDOCE50133918
The address to contact when your system requires service:
Overview of Thermo Scientific International Sales Organization
Postal address USA:
Thermo Scientific
275 Aiken Road
Asheville, NC 28804
USA
Enquiries from USA/ Canada
Sales: +1 866 984 3766
Service: +1 800 438 4851
Enquiries from Latin America
Sales: +1 866 984 3766
Service: +1 866 984 3766
Enquiries from Asia
China
Sales: +86 10 8419 3588
Service: Toll free 8008105118
Support Mobile 4006505118 or +86 10 8419 3588
India
Sales: +91 22 6716 2200
Service: Toll free 1 800 22 8374 or +91 22 6716 2200
Japan
Sales: +81 45 453 9220
Service: +81 45 453 9224
Enquiries from the Rest of Asia/ Australia/ New Zealand
Sales: +852 2885 4613
Service: +65 6872 9720
Enquiries from Countries not listed / Rest of EMEA
Sales: +49 6184 90 6940 or +33 2 2803 2000
Service: +49 6184 90 6940
Enquiries from Europe
Austria
Sales: +43 1801 40 0
Service: +43 1801 40 0
60
Thermo Thermo Scientific Barnstead GenPure with xCAD
Belgium
Sales: +32 53 73 4241
Service: +32 53 73 4241
Finland/ Nordic/ Baltic countries
Sales: +358 9 329 100
Service: +358 9 329 100
France
Sales: +33 2 2803 2180
Service: +33 825 800 119
Germany:
Postal Address Germany:
Thermo Electron LED GmbH
Robert-Bosch-Strake 1
D - 63505 Langenselbold
Phone
Sales: Toll free 0800 1 536 376
or +49 6184 90 6940
Service: Toll free 0800 1 112110
or +49 6184 90 6940
E-Mail: [email protected]
Italy
Sales: +39 02 95059 341
Service: +39 02 95059 250
Netherlands
Sales: +31 76 579 5555
Service: +31 76 579 5639
Russa/ CIS
Sales: +7 812 703 4215
Service: +7 812 703 4215
Spain/ Portugal
Sales: +34 93 223 0918
Service: +34 93 223 0918
Switzerland
Sales: +41 44 454 1212
Service: +41 44 454 1212
UK/ Ireland
Service: +44 870 609 9203
Sales: +44 870 609 9203
Ultrapure water system
61
Thermo Thermo Scientific Barnstead GenPure with xCAD
Se Ultrapure water system
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62
Thermo Thermo Scientific Barnstead GenPure with xCAD
AAEE Ultrapure water system
19. Maintenance record
(Correct keeping of this maintenance record is a condition of the guarantee)
Customer address: Location:
System type:
Serial no.:
Year made:
Feedwater | Ultra pure Ultra pure UV- UV-lamp
resistance | water water intensity operating
resistance | volume flow time,
[MOxcm] [MOxcm] [L/h] [%] [h]
Last change |Last Last change | Remarks Signature
of filter cleaning / of
cartridge disinfection | pretreatment
Any false entry is considered to constitute a falsification of documents.
The following points are to be observed to safeguard the quality of the system:
> 1x Weekly, enter measured values.
The pretreatment must be checked and replaced at regular intervals to ensure the
optimal ultra pure water quality.
63
Thermo Thermo Scientific Barnstead GenPure with xCAD
Se re Ultrapure water system
Contact I nformation Thermo Scientific
North America:
USA/Canada +1 866 984 3766 (866-9-THERMO)
Europe:
Austria +43 1 801 40 0, Belgium +32 53 73 42 41, France +33 2 2803 2180,
Germany national toll free 08001-536 376,
Germany international +49 6184 90 6940, Italy +39 02 95059 448,
Netherlands +31 76 579 55 55, Nordic/Baltic/CIS countries +358 9 329 10200,
Russia +7 812 703 42 15, Spain/Portugal +34 93 223 09 18,
Switzerland +41 44 454 12 12, UK/Ireland +44 870 609 9203
Asia:
Australia +61 39757 4300, China +86 21 6865 4588 or +86 10 8419 3588,
India toll free 1800 22 8374, India +91 22 6716 2200,
Japan +81 45 453 9220, New Zealand +64 9 980 6700,
Other Asian countries +852 2885 4613
Countries not listed: +49 6184 90 6940
© 2011 Thermo Fisher Scientific Inc. All rights reserved. All trademarks are the property of Thermo Fish-
er Scientific Inc. and its subsidiaries. Specifications, terms and pricing
are subject to change. Not all products are available in all countries. Please consult your local sales
representative for details.
64