Document text
FM 5055B LOT #3 yJo
C-02133 *
FINGERPRINT TEST DATA REPORT
NAS8-36298 COPY # 21
TABLE OF CONTENTS
FILLER TESTING
NAS8- 36298
U.S. Polymeric O. E. 71188
TEST
1.
2 .
3.
3m.
3b.
4.
5.
6a.
6b.
7.
7a.
pi Her Lot, for NAS A Lot* 3
Carbon Content.
Ash Content
Atomic Absorption
Moisture Content
Ash Content
PH
Particle Size, S.E.M. procedure
TGA, *C at 50X Loss
TGA
Particle Size Distribution
Particle Size, Horiba
PAGE
. 1
. 1
. 1
. 1
. 1
,. 1
.. 1
.. 1
.. 2
.. 2
.. 2
CHARTS
TGA
Particle Size Distribution
6A
7A
6C
7C
uop
UStotymeric
Page 1 of 2
FILLER TESTING
NAS8-36298
U. S. POLYMERIC 0. E. 71108
Filler L ot, for NASA Lotf-3.
1. Carbon Content,
QAI-5560
2. Aah Content, X
PTM-71B
3. Atomic Absorption, ppm
CTM-53B
(Values are average of
2 determinations)
#3A-1
99. 40
NASA LOT#
0.000
0.000
AVG. 0. 000
NASA LOT#
#3A-1
3a. Moisture Content, X
CTM-53B
3b. Ash Content, X
CTM-53B
4. pH, Units
ASTM D1912
3. Particle Size, microns
S. E. M. procedure
(Average values are
of 20 determinations)
6a. TGA, *C at 30X Loss
CTM-51
.010
uSSS.
AVG. . 00B
NASA LOT# 3
.023
.023
AVG. . 023
NASA LOT#
4. 80
4.95
AVG. 4. 88
NASA LOT#
AVG.
Maximum
Minimum
Std. Dev
.31
.99
.20
.23
864
NASA LOT# 3 AVERAGE 858
SAMPLE
#3Az3.
99. 32
99. 44
3 AVERAGE
99. 39
0.000
0. 000
0. 000
0. 905
0. 000
0. 002
3 AVERAGE
0. 001
#3A-2
#3A-3
L0T#3
AYPt-
6.0
6. 0
6.0
1.0
2.0
1.8
2. 5
2.0
2. 3
0.0
0.0
0. 0
0.0
0.0
s.
9.5
10. 0
10. 2
.015
0. 000
.020
0. 000
.018
0. 000
3 AVERAGE
: .008
.000
.000
.010
.000
.005
.000
3 AVERAGE . 010
4.75
4.85
4i 99
4. 78
4.82
3 AVERAGE 4.83
.31
.42
.88
.85
. 18
. 15
.20
. 17
AVERAGE SIZE .48
660
850
MITOO MATERIALS DIVISION
700 E. DYER ROAD, SANTA ANA, CALIFORNIA 92707 • (714) 549-1101 • TWX (910) 595-1130 • FAX # (714) 549-2858-5-2437
Page 2 of 2
Filler Lot for N ASA Lot# 3
6b. TGA
CTK-51
7. Particle Size Diatribution
CTH-72
7a. Particle Size, Microns
CTM-72
See Charts 6A-6C
See Charts 7A-7C
f?A-JL
£3A"Z
.69
.94
.69
i_2±
.63
.86
AVB. . 92
.68
.68
NASA LOT#
3 AVERAGE
.89
U. S. Polymeric
^j| * -4 ^ • ( 0 “ ’
Hasid H. Quraishi, Manager
Quality Assurance Department
I
CHART 6A
tfl
WEIGHT
NO. HN7-01-J5-J0M
ORIGINAL PAGE IS
OF POOR QUALITY
CHART 6C
✓
ORIGINAL PAGE IS
OF POOR QUALITY
CHART 7 A
urn'h'
• DISTRIBUTION TUPLE (BV VOL.;
CHART 7 B
ORIGINAL PAGE IS
OF POOR QUALITY,
'•I
OKJOINAJ; PAGE IS
OF POOR QOAIITY
CHART 7C
TABLE OF
CONTENTS
—
RESIN
TESTING
NAS8-
36298
—
U.S. Polymeric 0. E. 711G8
31LD Resin Lot
^or NASA Lot# 3
—
TEST
PAGE
1
1.
Resin Solids
1
2.
Specific Gravity
1
—
3.
Brookfield Viscosity
1
4.
1
5.
Atomic Absorption
1
6.
Gas Chromatography
1
7.
1
8.
1
9.
1
1G.
2
11.
PH
2
—
12.
Phenol Content
2
13.
Chang's Index
2
14.
2
15.
CHARTS
Gas Chromatography
TGA
DSC
HPLC
RDS
NMR
6A
7A
8A
9A
IGA
14A
15A
6C
7C
8C
9C
1GC
14C
15C
Page 1 of 2
1. Resin Solids, X
PTM-7C
RESIN TESTING
HASS-36298
U. S.
Polymeric 0. E. 71108
♦3-l_
71. 8
71. 4
AVG.
71. 8
71.7
Lot# 3
71.6
71. 8
♦ 3-3
71. 3
72. 3
71.3
AVERAGE
71. 6
71. 5
2. Specific Gravity 8 25- C
PTN-29C
3. Viscosity, Brookfield, cps
PTN-14C
0 22. 8* C
4. Gel Time, mins sec
PTH-47B
5. Atomic Absorption, PP m
CTH-53B
Na
K
Ca
Mg
Li
AVG.
6. Volatile*' □•« Chromatography
CTH-55
7. TGA, X Weight Loss at 500 C
CTM-51 <AIR>
8. DSC, temperature *C
CTM-50A
1. 129
Lot4 3
1. 131
AVERAGE
1. 128
1. 129
1250
Lot4 3
1375 l 25 ®
AVERAGE 1292
3:40
Lot4 3
3s 38 3s 33
AVERAGE 3s 37
♦3-2
14
0
5
1
♦3-3
14
0
5
1
21
21
i nTl AVG
12 .®
0 . 0
5.0
1.0
See Charts 6A-6C
♦2-L
38.7
Lot4 3
♦ 3-3
38. 2
38. 5
See Chart 7A-7C
178 183 18 o
Lot4 3 AVERAGE 182
See Chart 8A-8C
9. HPLC
CTM-49A
10. GPC, Average solecular vt
CTM-49A
See Chart 9A-9C
1666
Lot4 3
1751
average
1838
1752
See Chart 10A-10C
«T00 MATER.AU 0IV.8.0N . . TWX (.«» * «* *
nAAn cant A ANA
( 714 ) 549 - 2858 - 5-2437
Page 2 of 2
11. pH, unite
CTK-1B
Qfi.D Re "' 1 n Lot f pr HASA L*Qt» ,3.
#3-1
8.5
Lot#
#3-2 i2z . 2
©. 5 ®*
3 AVERAGE 8.5
12. Phenol Content, X
CTH-55 Appendix 1
AVG.
12.22
12.57
12.39
Lot#
11.92 11.72
12. 18 LLi 7-2.
12.01 11.72
3 AVERAGE 12.04
13. Chang 's Index, ml.
CTM-5B
14. RDS, Minimum Viscosity, cps.
CTH-57A
#3-1
#3-2
#3-a
AVG.
24.8 24.6 25.2
Lot# 3 AVERAGE 24.9
VIsCjl
179
212
197
■C
107
115
107
110
See Charts 14A-14C
15. NHR
Vendor procedure
See Charts 15A-15C
U. S. Polymeric
Hamid M. Ouraishi,
Quality Assurance
Manager
Department
ORIGINAL PAGE IS
OF POOR QUALITY
typical gas chromatograph St
l-ur
OptHtOT-
Column
Length
Dia.
Liquid
•t. *
Support
Rest*
Cittier 8i
Rot one tor
lotoctor
Foltege
Sonsit.
CHART SP#
SAMPLE :
Size
Flo* V,
Kgdrogen & iO ** 1
Scavenge
Split j-
IT337
Column —
Solvent-—
Concn .— Uti
6ftS rHBnMATOGRAPHYJIWmia^ 1
TEST METHOD CTM-55
MEOH
ETHANOL
MECL2
ACETONE
1PA
THF
ACETONITRILE
CRESOL
MEK
furfural
toluene
CHLOROBENZENE
PHENOL
.6
1.18
1.28
1.45
1.83
3.08
3.2
4.03
4.08
15.03
17.98
19.6
22.08
w OS USES TO DILUTE ™ «S1« » lS '
CHART 6A
VERTICAL SCALE FhCTOF.
SAMPLE
MI SC
- TIME-
C=0 L 0'394l6H5/HL
LD 3-1
17 •• 40
iftTi* lr'%% 6
OPERATOR’
RUM TIME-
delay time
CHAM 0
30
0
00
. 00
mimutes
PK
MO
RET
TIME
PEAK
AREA
AREA
V.
B
L
2
4
5
6
7
8
Cl
10
€3
1.63
1 .88
3.33
5.58
5 . 86
€-35
6.58
9 1 1 £ 5
5 21 11
6 22.es
7 22.20
3625
1 15880
215000
3548900
11738
10483
4501
15*617
18886
35525
12068
13296
.091
2 . 876
5.374
88 .707
.293
. 262
112
’ 490
.272
.888
.302
•772
1
2
2
3
A
4
4
4
2
2
r,
c
1
PEAK
HT
433
11211
11219
86537
573
391
395
376
519
5295
1684
1675
0TflL WEB- 408*716
*}E e I?°hiSth1 »»
SAMPLE
MISC.
|i0 L 0994lGM5/^ L
TIME- 17=40
&"!■ 11'*%?
OPERATOR : -> Gt
. ttmp 70 00 MIMUTES
RUM TIME ~
DELAY TIME » • k,, °
CHAN = 0
p P ft K AREA S'
PK RET AEAK L
HO. TIME
1.63
1.88
3.33
5.58
5.98
6.58
18 11 ll
35 21-95
36 2208
37 22-20
4
5
6
7
8
10
1 15080
215000
3548900 © s
11738
10483
19617
10886
35525
12068
13296
.882
.385
887
294
263
.491
.273
.890
.302
333
2
2
3
4
4
4
2
2
c.
1
PEAK
HT .
11211
11219
86537
573
391
376
519
5295
1684
1675
TOTftL BRE«= 3962593
THRESHOLD- l ti
** real
- r i
time
CHROMATOGRAM ***
/
— final full scale M
=1000 . 00
ORIGINAL page is chart 6B
OF POOR QUALITY
I wEPTICflt SCALE FACTOR - IX
SAMPLE
M I S C ■
cU^elieFHS/HI.
time ■ is : 2:4 , .
CATE. 1
OPERATOR :
g, .iLj TIME , 30 00 MINUTES
oelaVtIme 0.00
CHAM ; 0
PK RET fiR f L
HO TIME hREH
£
6
7
8
9
10
11
23
33
40
41
€3
1 .70
30
10
58
98
3
5
5
5
€
11
18
21
40
88
25
'.95
. 08
42 22.20
1800
250880
3049400
10194
14229
241b
1389
35297
2731
34535
10788
1321 1
7
88
053 1
.318 2
991
.297
.415
.071
.040
030
.080
. . 008
.315
.386
4
7
w
4
4
3
1
2
2
1
PEAK
HT .
276
11092
04 633
409
996
96
98
1855
140
5148
1570
1686
34 26-648
total area=
i?r. E pr 0 «STHi i»
APEA^FE JEC T= I860
SAMPLE
Ml SC • :
!i0 LI ;'e!is«rtS/Hi-
TIME : 18 : 24
DATE 12^1 ® <.® e
OPERATOR :
RUN time=
delay time
CHAN : 0
30
0
00
00
minutes
PK
NO
6
7
8
9
23
40
41
42
RET
TIME
PEAK
AREA
AREA
t
L
1 .70
3 . 30
5.10
5.58
1 1 . 68
21 -95
22.ee
22 . 20
250680
3049400
10194
14229
35297
34535
10786
13211
2
7.33
89.207
298
.416
1 .0
1 .010
.316
. 386
3
4
3
33 3
2
2
1
total area=
threshold- 1
MIN FK. WIDTH-
AREA REJECT-
3418332
15
5000
PEAK
HT .
11092
64633
409
996
1855
5148
1570
1 686
original pace is
OF. POOR QUALITY
t
CHART 6C
*** REftL TIME
CHROMATOGRAM
FINAL FULL SCALE MV
= 1000 . oo
vertical scale factor. IX
SAMPLE •
Ml SC .
A 1 LD 3-3
C=0 • 10052
€MS/Mt
TIME 19=0«
date 12/10;&c-
OPERATOR : J6^
RUN TIME :
delay time-
CHAN • O
PK RET
HO. TIME
30.00 MINUTES
"e . 00
PEAK AREA B
AREA 5S L
PEAK
HT .
2
4
5
6
7
8
9
10
18
29
41
42
.63
1.63
I . 90
3 . 40
5 . 10
5.60
5.98
6.40
II. 73
16.38
21.93
22 . 05
5795
77409
241490
3546900
7286
7111
4081
3260
15339
1188
54630
317880
.135 2
1 . 808 2
5.639 2
82.826 3
. 170 4
. 166 4
.095 4
. 076 4
358 1
.028 2
1.276 2
7 . 423 3
TOTAL AREA-
threshold* i
MIN . PK .WIDTH*
AREA REJECT*
4282369
15
1000
579
10929
10997
85797
258
547
189
152
829
51
951"
12752
sample
M l SC . :
C=0 100526HS/HL
TIME- 1908
DATE : I2.'iu;e*
OPERATOR •• JL<^
RUN TIME:
DELAY TIME
CHAN : 0
30 . 00
0 . 00
PK
NO
RET
TIME
PEAK
AREA
MINUTES
AREA B
*/. L
PEAK
HT .
1 €3
1 .90
3.40
11.73
— . - r.T
77409
241490
3546900
15339
54630
317880
1 . 820 2
5.677 2
83.385 3
.361 1
1.284 2
7.473 3
AL AREA*
?ESHOLD= 1
j PK WIDTH*
rft REJECT*
4253648
15
10000
10929
10997
85797
829
8517
12752
CHART 7 A
original pace 1 ^
OF POOR QUA LlT •
oiSl
CD
tSs
a (\i
: • \
i a x
• o
t^ta
§= CD
O
0 men
h EO®‘
«-t *-• ©
ns
cn -• r*
DO* W
i a n
1 .<*>
fl *H «H <
ffl (M X X
« °
IS 5 . -
E N C +£ U'O
o »« 3 5 o a
(fltnaa . .
cm in
CM o
in a:
< *-•
L 3 <
LU *"
I UJ O
UJ I— CM
“ -I O
uj < a
J Z O)
Q_ •-
2: li-
en h- in
tr cm
<
(Bui) ^LjB I PM %
o ~ s
•o u 5
"o.
&
V
o
(M Q.
•* E
a
. H- I
vo
ai a
cd d
i-i O)
r* o
• •
in in
rH fN
~‘o
eo a
cm o
r-i CO
vo
< o
• •
o) in
cn o
to d
cn
VO
a
cn in
. -1 o
st"
d d
CHART 7 B
ORIGINAL PAGE IS
OF POOR QUALITY
. CD i
cm a
> CD -
CD
< a>
a cm
•
I Q Z
in a
<
a <
0^2
ou *
10 m
01
o
a
w
O
•CM O.
E
a
*- e
cm £
i cm a
m « •• .
S ^ <
CD *“•
a giro
h EGO'
«-• *h CD
cn s
oi ^ f*
□ MW
_J ri N
i . a >
«i o « <
o> -• z z
a. 5 o i
e n c -p 7 ^
O ** 3 o Q O
in <n a: a . .
O) in
«-• a
1 w 9
uj t— c\j
H- <
< a:
“jo
LU < O
J Z O)
CL
2 U.
in t- in
a: cm
<
(Bui) igSto* X
<nO
cn o
• •
co a
«-• O)
vo
CO o
• •
cn in
«-• r-»
vo
cn a
■ •
a a
to
•-« a
• •
cd in
■ •
in o
cn
VO
r» o
• •
cm in
t J a
va cm
O Q
• •
a a
•8 I
o ft
• n X
CHART 7C
giai8iSi«Sii^S558SSgSSSj585 gm:g§SSS8S888SS88S88g|8ggS8S5SS8 ^S85^^ ^y§j^^^
I— w— ■■”3
■UWHIWIHj
MlIKUIUIIII
Rmuniiimi
Kiumiiiiini
asa
EEaS
Siiiniinini!
P0<
ORIGINAL PAGE IS
OF POOR QUALITY
OF POOR
CHART 9A
)AT A FILE As PHEN036. HDR TAKEN 09-05-19B6 15:49:05
" '**"■**■'**’"**""**"**' "**" ' ” ' ^x.*.M.»*********************
.„.,..»«.*«.******«****«»** # * M *******‘‘**‘*Sper»tor Initials: OGZ *
USSr r;U9G^1^^0i 7 H.tho 2 ,PHEN0LIC Channel*: O^Viat^ N.P. *
LiT:^
, Instrument Type: BECKMAN HFL TH F /WATER , 2:1 BY WEIGHT .
* Solvent Description TE -1.S ML/MIN
Operating Conditions. ^ detector 1:
*■ DeteCtDr V r-s tr'TLJ— OSt. „ ^^.^M-M-********
report
* Mi sc. Information: # ^^^*L*************************^***?
** ************************** Ending Retention Time.
Starting Delay: 0.00
10.00
Ret
Time
1.80
2.07
Peak
Area
Area B
7. L
Peak
Ht.
Normalized Area/
y m Height
11 6498 73.6309 2
42437 26.3691 2
5085
4223
100.000
35.813
23.3
10 . 1
rnfal Area:
160935 Area Reject:
1000 One eample per 1,000 seC ‘
ORIGINATE PAGE IS
OF POOR QUALITY
CHART 9B
)A1 . FILE As MB561^HDR TAKEN 09“05“^986^4 .Lj^^ ^
}A -m FILE A-.PHEN035.HDR TAKEN uv
.k.****** area
-n- -K- -K- ■* t_ * ■*■ * '**'
„~************************************^^ l
: 'JSl' ot-os-I ie6 ’ 1 ie • ob 9 L th=d = PHENOL i c o PHE ^i. M.fl. *
* Inter-faces 4 10 Threshold: .01 ^.c**************************
;.“i^t^2*:::---i*****-™*-r**********c:t^*; „x r oBo ND A P «K c- ls .
: — ‘ WE,EHT :
. operating Condition,:^. ^ Detector 1 =
'ft\ irting Delays 0.00 .
_ kUr mz>i i 7pd Area/
Ret
Time
1 .78
2.05
Peak
Area
Area B
7. L
Peak
Ht.
Normalized Area/
y m Height
117907 74.0922 2
41228 25.907B 2
5029
4167
100.000
34.967
23.4
9.9
Total Areas
159135 Area Rejects
1000
One sample per 1.000 sec.
ORIGINAL PAGE IS
OF POOR QUALITY
AT A FILE A-.FHEN034.HDR
TAKEN 09-05-1986
15:07:23
ORIGINAL- PAGE IS
OF POOR QUALITY!
'"LL1.LL.LL.:: :
: Lte! e — :
MIC ro BDN da P ak c -.e ;
. -Instrument Type! BECKMAN HPUC^ /wflTER) Zs 1 BY WEIGHT
.• Operettn, KS- »• t
Starting Delay: 0.00
report
^Mt-*-*-*-**"*
3
V
Ret
Time
1.78
2.05
Peak
Area
Area B
% L
Peak
Ht.
Normal ized
7.
Area/
Height
118569
43673
73.0817 2
26.9184 2
5139
4294
100.000
36.833
23. 1
10.2
1000 One sample per
1.000 sec.
Total Area:
162242
Area Reject
6PC CALIBRATION PLOT
*** Cal ibration Data ***
Calibration Name:
Mi sc Information:
Fit Type: 3
Log Mol Wt «
2 « 5^3977
Coefficient
Ret Time
3.50
4.33
4.83
5.09
6.00
7.17
7.50
A + Bx ♦ Cx~2 ♦ Bx^3 24
B . 2.11561= C- '-****2
,f Determination* P:"
Molecular Weight
35000
15000
3600
2350
570
92
72
D« 3.606432E-02
Log Mol Wt
4.544
4. 176
3.556
3.371
2.756
1.964
1.857
CPC CALlBUftTlOW PLOT.
4.1 5.1 ‘I
Retention Ti«e or Volme
CHART 10A
VT FILE B:GPC 21
. HDR TAKEN OB-05- 19B6 17:26
*++*■*-*-*-■**-*■** GF-C
ORIGINAL PAGE IS
122 OE POOR QUALITY
L .-r ^mmm*"*"**"* 1- *
Operator Initials: GBF
DATA FILE: ®
Channel#: 0 Vial#. N.A.
*********************************************Operator Initials: BBF *
Ste ! 6 08 - 05 -I 9 B 6 li* 42 *^ 6 ”ycJe 2 l 21 Chinned. ''o^^vtal#: N.A. *
~ 0 p e ratin 9 D Cond.t» D n.. 25 -- /iftU Detector 1= *
Mist. Information: CA 1 :’®^^°»»»»*,*.»».*«»»»*******************do***
?w ********************** Ending Retention Time:
Starting Delay: rPCFHEN
vibration i lie. ibu tion Averages
secular Weight Diet 10.OO MW:
baseline TIMES: ^ ^ 10 . 00 MW:
! r !T S AreI- 256218
\. al Area. Jfc64>
»Iw= 284
M D *Mn= 5.8652
M ' M 4056
1451
Mv=
22295 to
22295 to
CHART 10B
ORIGINAL PAGE IS
~ OK POOR QUALITY
* F1LE B..BPC33 -HOR — 0B -° 5 -'^^ ********
******* - Gf=c R r*:*r»*****‘*i
*************************** Operator- In ^gp^23 -PTB *
****************£ 3 _2 C=2.68 DATA FILE* * vial#: N.A. *
. mp le Names 91LD 53 Me thod: Channel#- ° *
' |te: 08-05-1986 C ycle#: 2o ********************
- InstrUme -'ru 0 "«r”. P 3 t 5 c°F^RATe=2.onL/m« ior ls
Operating Cond ^' 0t 2 54NM/.1A U *********************
SsW-SrHr
3.85 to
3.85 to
251238
1751
322
5.4277
4258
1527
«
*
*
«=— '■-SI: iU Z.BS to 10.00 «
lecu*®' ~
seline TIMES:
ocess .TIMES:
ital Area:
/Mn=
MW:
MW:
22295 to
22295 to
2
2
Cum 7
* FILE EHGPC24
ORIGINAL PAGE IS
OF POOR QUALITY
. HDR TAKEN 0B-05-1 986 17:34:48
CHART IOC
-Nr -**-*--** C3F-C REPORT
*
*
*
*
*
**************** — * . i GB p
* fc**********-^^^" Operator Initials, oor
Sample Name: 91LD 3-3 ^-2.68 DATA FILE: B:GPC24 .FTS
• nate: 08-05-1986 12:29:oB Method. ^ Channel#: 0 Vial#: N.A.
’ ^tartin^Peak Width: 60 Thres ^°^* ® ************************************
,*********************^ Column Type: ULTRASTVRAGEL 500A *
Instrument Type: HFLC/BECKMAN THF *
f . CondTt i ons^ C T=35C°FL0WRATE=2. OML/MIN I
> Operating Conditions. 1 Detector 1:
Detector 0: 254NM/.1AU
Information: CAL I BRAT I ON /BFC
Mi sc
«Tf*******
^ibr^ion’me: GPCPHEN
_.c U l»r Weight Distribution ftvereges
Baseline TIMES:
> r >cess TIMES:
'i^_:al Area:
1w—
1r=
J< , Mn=
t -
■i“ 2
1v=
3.85 to
3.85 to
243393
1838
369
4.9751
4370
1608
10.00
10.00
MW:
MW:
Ending Retention Timie: 1 •
22295 to
22295 to
1.0E3
CHART 14A
o
<V > 3SI0d
*VJ3
eriment No* *
1% in, >rr — ^” 5 ^^'- Jpsaai - E ^
7i« ngWriTT ;®YNA«1P
rrT5T33 .v- ‘2J
leep Type *
)metry *
CURE _ ... ^
DI SK' t<'TL'AT£
RADIUS * _
GAP !
25*00
0.50
3tes s
r RAlN =507. * - —
EDUENCV -10RAD/SEC
ORIGINAL PAGE IS
OF POOR QUALITY
;^L5£.r\r ru w 1
__£ XA *-
•„ POISE
l.©07e+002
4.686e+O02
r^OISE -^— i 2000e-001 -.2, 7O0e+OOl
1 j753e+002 .-4 Jix| ' ?tS*0Oi— J7POOe-€QOe£2 .B00e+001___
4.6Q6e+O02 ^lT^?etW2^r9S0 e ^0ran J-JSqi 2.000e+000.-' 3^>0e+001 _i_
1 . 529e+.Q02 _. .1.7.4 836+002 3 . 3i~?^^Y^-3903e+OO 1-^3 .OOOe+OOO . 2O0e+O0l - y
1. S59e+O02 - 1.3126+502 ~l5L*£t ^;300eW-=^-_-
<?0e*002 ^4Yl4l6+002 ^ • -' 8fc£ ^*^:~rJ ^-Jvle+OOr 1 " - ®. ©OOe^OOO ~3 7500e+001 __
h — 1 rO48e+O02 -9.925e+O0 1 57 ^* 3*01 — -**
^ ^fti^^SeioOO ~8 - ©00^+000 -p* . lOOe+OOl -- __
&
I
5. 630e+001
^5.O41e+001
4.901e+001
4.273e+001
©.-©■l^e+w*:^? ^ « 9-?5e+0OO ©.©OOe+OOO.r -3 ** lOOe+OOl---
77t22e+001^*-450e+001 Z^^tnoi -^BBoe+OOD S. 000fi+x»00^.300e+001_ r
6.291e+OOi:::S.S9lB+DOI Z37BB6 b O -_7.s l.OOOe+OOl 4.500e+001
... — 'i^^OOO- i.iO0B«01--4.-7O0B+O01- :
&75e+001 4.900e+00i -;—
- 13
*.5BBe+001
4
4. 195e+001
5
3.8736+001
. 16
3. 532e+001
* 7
3. 20Be+001
' 8
2.9356+001
19
2. 697e+001
20
2. 559 e +001
9 21
- 2.’4^9e+OC>l
i. 259 e +000
^'^ile+OOl 2.524e+001_._
-|*9»6e-001 -2.4554-001 -4.B51e-000
iilsle-OOl 2-299.-001 - 4.427.-000
z* ''-2.0754-00 1_ _4 . 0 1 6.-000
1 .*200e+001:
1". 300 b + 001
1 ,400e+001
1 . SOOb+OOI
1 . 600e+00 1
~ i . 700 b+00 1
4.900e+001
5- lOOe+OOl
-5.400e+001
5.600B+001
S.BOOe+OOJl
~6. OOOfi+OOl
23
24
_25
26
27
28
2 -7
30
2. 1 76e+00 1
1.9906+001
2.O33e+O01
-i .-9966+001 -
- 1 . 940e+O01-
-1 ,895e+001
1 . 809e+001
1.684e+001
1 .564e+001
1 .Sioe^wi 1 * 43Be+0C> 1 - __
7 407e+0Ol — 1.344e+001 - -4 . 1 ->Be+0 .
203e+O0 1 1-1 50e+00 1
090e+00 1 1 • 050e+00 1
77E + UUU j- •owe: • wt. - — — . .*T
.-420K*e01:rf-0664.000=4£rf<>0e-Ofii
. ^ ooomiiViA - 2.-4006+001
-6s-600r+001-
3.-^6e+yw^^' vt ;7, T n.-.ri. i n m
! . 2504-001 - 2 . 6924—000 - 2. 1004-00 1 - +«£££*
A. 070e+00 1
, B22e+001
,667e+001
,525e+001
2. 2B2e+000
2 . 090e+000
1 . 9 1 2e+000
1 . 765e+000
1 . 51 0e+000
1 . 36BB+000
31
9 . 522b+000
9.1 506+000
6. 399e+000
© . 037-e+OOO
n!>o
7. 470e+O00
7. 2206+000
34
5. 769e+000
5 . 5B3e+000
35
5. 67Be+000
5. 498e+000
3-^3
-3. 1596+000
* 3. 134e+000
37
5.39Be+000
5 . 333e+000
38
4.775e+000
4 . 669e+000
-39
4.6796+000
4 . 642e+000
40
4.2766+000
4. 182e+000
41
2.7£>7e+000
^2 77546+000
42
1 . 7876+000
1 .631e+OCO
43
2. 1 9Se+000_
?. 1356+000
2 ©92e+000 - 2 . luuen'u 1 — ^
1*725^-000 -2. 200.-00 1 J.O004-00T-
2 * 495e— 000 - ■2.3004—001 3-.20O4-O0r-
2 . 400e+001
2.500B+001
2. -600B+001
2. 700e+001
2. B00e+001
2. 900 b+001
2.6354-000 1.1954-000 3-0004-001__- -
2.4304+000 —I.Oj-4-OOC -■ 20( wo01 9.000.-001 — *
''l-t B !ono 7 ' i -,7-ooi 3 " 3004—001 =.2004-001
! -^tooo- f. ‘^‘^s^SS^4:SS:^fe
3.B57e-t>01 ->.96-e vi. -4 z.nrie.+noi 9.700e+001
B. 3474-001 6.7734-00 -0004-00 ^ .
9. 992.-001 _S. 9S54-001_ i '™**™- , 1 olC-4-00^ ^
1 . 030e+002
©.2B6e+00C>
,6.946e+000
5. 7706+000
5. 0o7e+000
>Be+000
3.5316+000
2 . 9566+000
r> . fc35e+000
7. 400e+001
7 . 600e+001. _
7 . B00e+001 - frr
©. OOOe+OOl
8 . 2006+001 —
B. 4006+001 -
6. 600e+001
44
45
46
47
48
49
50
2.6356+000
2. 138e+000_
2. 367e+000
2. 131e+000
2. 789e+000
4. 053e+000
5. 206e+O00
57B60e-001
B~. 925e— 001
_2.753e-001
7.296e-00l
JS r 1 46-0 0 1
2.7B2e-001
5. 196e— 002
7. 212e-001
2. 13Be+000
2. 254e+000
2 . 032e+000 6 . 39Be— 00 1
*7 . S39e+O00 ' 1 . 1546+000
5 . B65e— 00 1 3.B00e+0C>l
rr -taa«»-OoY 3. 900e+001 -
4' 4724-001 - -4:0004-001— 1 .-0504-002
^2*244.-001 4 . 100.-001 > -070.-002
2*7594-001 - 4 . 2004-OQA_2-1 ■ 09s>4*5£li.
3*309e-C*0lZ 4.300e-001 1 . 110.-OO2.
4.400e+001. 1 . 130e+o0^
4. 500e+001 1.150e+002
4.600e+001 4-1706+002
“3 .' © 49 e +0O0 ’
A . 692e+i*CK'
1.2716+000
2. 255e+000
_2 . 6B3e— 00 1 .
2. 970e— 001
2.6756-001
" 3 . 499e-O01
-5.0866+001
6.5266-001.
4.700e+001 -1.190e+002
4 .©OOe+OOl r. ^ I Ob+002
4. 9006+001" 1 . 2306+002
ORIGINAL PAGE_TS
OF POOR QUALITY
:-r; - -v* r~;
_ a _
FINGERPRINT viscosity profile
CHART 1AB
2.0E2
• TIT .. — .
FI SPRINT VI SCOSITX^ROF U-E SILO,***™.
10."" „ETA* -
POJSE -
_ 1.750e+002
-2 1.643**002
3 1'. 486**002
1.-307**002
-5 1 . 152e+<X»2
1 .OOSe+002
B.867e+001
"V.7iie+001
6. B30e*001
6. 164e+001
5. 460e+001
4.943**001
4.357**001
4. 0B4e+001
3.825**001
3. 460e+001
3. 154e+001
2.914e+001
2.6S7e+001
2.537e+001
_2. 422**001
2. 33Se+001
2. 207**001
2.007e+001
1 .B97e+001
1.696e+001
1 . 521**001
1 . 444e+001
ETA
EXfl *l_
_ -UpDlSE 13RAMS-CM -“V- - ^^ N *
' & 214**001 -;2. 197**001 J2X>OOe— 001_ -
*r— 929e+001 “"2^063*® 01 _ _JTrOOOe*O00- -3
-^09el00 000.^0 3
---
y.y.-i — r m — - 6 OOOe-tvw rr »
- 3.049^0, ***%£ . toSrXo :
£..B46e+000 1.000**001 4
r%T 199e+OO0
jtorque
6
F
3
’ 9
'»
1
12
1 3
4
t 5
16
7
_B
19
"*0
!1
^!2
-27
?4
-25
26
27
28
7°
30
•“i /» o -
1. 1 lBe+001
31 9.736e+000
“32 1.107e+001
33 1.03Be+001
34 9.424e*000
_35 7 . 320**000
36 4.630e*000
37 5.220e+000
3B 5.032e+000
~ 39 4 . 606e+000
40 4.843**000
.41 3.51 0e+000
-42 2.902**000
43 2. 663e+000
44 2.271 e+000
45 2. 235e*000
46 2.124**000
47 2.549**000
48 3.300**000
r -49 4.442e+000
50 6.473**000
POISE
1 . 69Be+002
I . 595**002
J . 439**002
1.261**002
i . 1 Ole *002
9.513e+001
_B. 240**001 -
_7.047e+001_
6. 1 12e*001 -
-5. 40Be+001
4. 642e*001
4. 103**001
3 . 4B6e+001
3. 195e*001
2. 922e+001
2. 609e+001
2. 377e*001
2. 206e+001
2. 077e+001
2. 040e+001
1^ 963e*001
1 . 943e+001
l.B95e*001
1 . 755e+00J
1 . 690e*001
1 . 557e*001
1 .426e+001
1 .344e*001
1 . 173**001
1 . 063**001
9 . 302**000
l . 070**001 -
9.901**000
9.057**000
7. 20Be*000
4 . 559**000
5 . 203e*000
4 . 930e+000
A . 4B4e*000
4 . 770e*000
3.502**000
2. B53e*000
2.543**000
2. 147e+000
1 . 835**000
1 . 3B3e*000
2. 370e*000
2. B33e*000
3.945e*000
6.061**000
2.95Be+001
2. B75e+001
2.755e+001
2.613**001
2.543e*001
2. 46Be*001
2. 272e+001
2.072**001
1 . 904e+001
1V705**C>01
1 . 59 1 e*00 1
A m V ~
1.100e+001 4
. l 77 C T VVV *
z,. 462B+000 Tl .200e+001
5 . 120e+000 1 ,300e+001
4 .795**000
4.340e*000
3. 951 e+000_
3 . 651 e+000
3 ; 369e+000
3.241e+000
1 . Zt'r len'vi w . — ^
1 ^4 1 9e+00 1—3 .-037 e+OOO
1 .300**00 1 2 .930**000
1 . 130**001
9 . 736e*000
B. 606**000
6. 724e*000
5.293**000
5. 284e+000
4.278**000
3. 477e+000
2.879**000
2. 823**000
3.117**000
2 . 495e*000
1 . 276e+OOG
_. 767**000
2. 515e*000
2.360**000
2. 127e*000
1 . 910e+000
l.B 12 e +000
1 . 567e+000
1 . 404e*000
1 . 222e*000
390e*000
1 . 302e*000
1.1 B3e*000
9. 191 e— 00 1
A • . -
-B.-OBOe-OOl -*5.©07e-O01
4. 206e— 001 6. 553* -001
1 . 00Be+000
1 .052**000
B. 349e— 001
-2. 337*— 001
5.302e-001
7.924e^001 _
7.41 3e— 00 1
1.27fce+000
1 . 612**000
9. 395e— 001
1.691 e+000
2. 042e+000
2.272**000
6. 31 le-001
1 . 400**001
4.500e+001
1 . 600e+00 1
1 . 700e+00 1
lTB00e+001
1 . 900e+001
rSzO00**O01
-2. 100e*00 1 6
2 - 200e+00 1 — -.7
“2 .300**001 7
2.400e+001 -
2. 500e+001
2 . 600e*00 1
2 . 700e+00 1
2. B00e+001
2 . 900e+00 1
3 . 000**001
-3. -100e*00 1 ~ -&
3. 200e+001 9
3. 300e+001
3.400e+001
3.300e+001
3. 600e+001
700e*p01
o = v ' r * ° M
779 e — 00 1 _ 3 . B 00 e+o 0 1 — 1
6. 074e— 001 3.900e+001 1
4 , 402 e— 001 4.000*+001 1
3 . 638*— 00 1 4.1 00**00 1
3.339*-OOLZj^-2Q0b*C>01
4.300e+001
4 . 400e+001
4 . 500e+001
4.600**001
4 . 700**00 1
4. BOOe+OOl
ZJ.U v ^ w __ .
B . 1 29e— 001 . 4- 900**00 1
2. B45e-001
2. BO le-001
2. 659e— 001
3. 196e— 001
4. 142e— 001
5.573e— 001
- TEMP
DEG. C
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100e+001
200e+001_.
. 400e+001~ '
'.-fcOOe+001"' ■'
.B00e+001
’,-000e+00I^f_
.-200e+001
.300**001
. 500e+00 1
700**001
. 900e+001 "
J7'l 00**00 1
5.300e+001
3.500**001
5. 700e+001
5. 900**001
6. 100e+001
'6 ."300**001-
6.500e+001
r^.-T'OOe+OOl - ^
900**001
,-OOOe+OOl “
v 200e+001
. 400**001
. 600**001
BOOe+OOl
. 000e+001
200**001
. 400**001
. 600e*001
. 800**00 1
. 000e+001
200**001
. 400**001
. 600e+00i
. BOOe+OOl
. Q00e+002
. 020e+002
. 040e+002
. 060 e +002
. 070e+002
_D90**002
_ . 1 10e+002
1 . I30e*002
1 . 150e+002
1 . 1 70e*002
1.1 9 | 0*+^ m - , 2
1 . 2 l 0 e +002
1 . 230**002
-7.
7.
7.
B.
8.
8.
B,
9,
.9.
9.
9.
.1
ORIGINAL PAGE IS
OF POOR QUALITY
ITY PROFILE 91LD RESIN NASA L0T3-3
CHART mC
4
4
<
4
4
(V ) 351 Od
♦V13
" V ■ vi. rrr-' ~ E£ ^_;
iZ j*nd Ta^^ : r^ 3 ^ s ^ y _ 3
fSSg^tl^e ,^YWMIC
^p T ype • CURE^ :1: v-^_ r
netry -• --©ISK-fc «--ATE
RADIUS s _-_
- — GAP " !
15.00
-0.50
ces s ._. .
RAIN =50% ‘
QUENCV =10 RAD/SEC
ORIGINAL PAGE IS
OF POOR. QUALITY
?.431e^0Ca ^^ £ ^^ Oe:| . o01 „
3 ;*68e+<*>l^^;*^gE§nLLSe^^ 4.4OC>e+O01
B. lOSetOOl: — *~2 -fc28e+001 - 1 .^07e+<>C oVnnOe+OOO
Loiee^l ,iL*oor-9.81*e*<>0<' *-^'!tool 4.700.-<-001
7! B19e + 00r-^7- 22B.-00 J— *• t , s . 84 Be*000^ 4 .OOO.^ 1 - * ^, 0e+0 0 1 ^ .
i/io4e*oo-r-^.-3J2^ooj *. 754e+001 _ wtb^oc© *-=Xtooi 3.300—001
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2 1 057e+001 l.e29^001„;J.4^e^o 2 . 3 76e+000 2.400e-001 ^ 600e * O Ql
l # 891e+001 l,726e + 775e+000^ 2* 214e^000 4 +{iQ&+001 7^800e*^001
1.763e.00> 1.620-00 |‘ 77 ^00 2.012-000 2^"*Sol g. ^o^ool- -
1.601—001 1-5^°°; “; e71e .OOO 1.779e.OOO l-Z-^^j e . 20 o— OOl
1.4l7e+001 l.^w'le - on^e+QQQ l*564e+00- .. ■ * ori ^_ + noi 8.400e+001 _.
1.24be+001 1 * « i7eloC»l 3.399e+000 V' 4 ^e+000 ^' O00e +O0l B.600e+001
1.1 6Be+00 1 1.1 l 7e 0 R23e+000 1.296e+000 ^r8<K»e+^l
1.032e+001 9.92^e+000 “ 00 ^ i06e+OOO - 00 1 -9.000e+001 ~
-9 . 434e+000 9 '^ e ^'r, l*691e+000 l.OOSe+OOO ^‘^ooe+OOl 9.200e+001_
7 .995e+000 7.81 e _*I l 1 343e+000 B.844e-o01_ • I 00e+ 001 9.400e+0Dl
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• 4. 942e+000 4.BB7e+ o’-goBe-OOl 5.449e-001 aoOb+001 9-B00e+001
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J 4 . 037 e+OOO 3.BB5e+000 1-™ZJ 001 ^ . :
3 3 . 1 B 1 e+000 ,>.04oe lBBe-001 3.294e-0Ql • ■ 9OOe+P 01 1.040e+002
’ : VJ£%\ 4g*+h
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4 2.343e+000 2.251e+00o 000 2 .fc36e-001 p01 i. i50e+002
* ?-SS l:«- l:S^i .
7 ^'eS7e-000 ■ 2.674e.00C S.035e-0C1 4 4,0^002
50 44769B+000 4.63 le+000 l. _ . . _. _^- ■-- £^r. [_ r S^r:^ : - .
ORIGINAL PAGE IS _.
OF POOR-QUALITY
. *M : **». "
FINGERPRINT viscosity |
profile ? ivp;«esin;nasa i-0T$-.3
ETA'--
POISE
_^ETAVj^=
"JH POISE -
^r^7e-PC‘l
_JL-TOROUE. ~r,r - s’
ZERAM5-EM - ...-=-
4 rQ97*~<rtJZ-P- m ~
- TIME «MP„
"... MIN* .r -. DE6 ’i
rbOOe+C>p • »?•♦««
1. 27Oe+O02
\
TABLE OF CONTENTS
FABRIC TESTING
NAS8-36296
U.S. Polymeric 0. E. 71108
CCAz2 Fabric- for NASA Lot* _3
TEST
la. Breaking Strength, WARP. • • • • •
lb. Breaking Strength, FILL
PAGE,
1
1
1
2a. Carbon Assay. •••••*
2
2b. Hydrogen Assay
2
2c. Nitrogen Assay •
2
3. Visual Inspection
2
4 . Specific Gravity
3
3
3
7a. Atomic Absorption
4
7b. Moisture Content
4
7c. Ash Content
. A
6a. Filament diameter, WARP
4
8b. Filament diameter, FILL. • * ♦
4
9a. Thread Count, WARP
5
9b. Thread Count, FILL.
5
1Q»b. Areal weight * * *
10b. Volatiles.
10c. Weight Change on Acetone Wash,
CHARTS
Visual Inspection
TGA
3A - 3F
6A - &L
Page 1 of 6
IKI1J FABRIC TESTIHG
U&RJymerie NASB-36298
U.S. POLYMERIC O. E. 71108
Fab r <r ’- * or MASA 1°^* —
la. Breaking Strength, lba/in, WARP pICK 31~
ASTH D1682 CENTER 32
plain 32.
avg. 33 * 3
PICK
CENTER
PLAIN
AVG.
A3-2E
32
30
21
31.0
#3-3S
39
38
42.
40.3
CENTER
plain
AVG.
f3-5S
36
30
3Z.
34. 3
f 3-5E.
47
38
42.
44.3
lb. Broking Strength, lb./ln, FILL
ASTK D1682
PICK
CENTER
PLAIN
AVG.
PICK
CENTER
PLAIN
AVG.
«3-2E
32
28
22.
29.7
#3-3S
37
28
30
31.7
PICK
CENTER
PLAIN
AVG.
13-52.
18
19
13.
18.7
#3-5E.
32
34
33
33.0
Carbon Aaaay,
HDQAI 5560
PICK
CENTER
PLAIN
AVG.
#3-2E.
96.7
96.8
£6.5,
96. 67
PICK
CENTER
PLAIN
AVG.
f3-3S
96.6
96. 8
?6.£-
96.67
»3-3E
38
39
32.
37.7
•3-6S.
42
33
31
35. 3
• 3- IS.
14
19
12 .
17.0
•3-3E.
34
27
27
29.3
*3-6S
52
44
11
45.7
»3-lS
96.8
96. 0
97. _L
96. 63
#3-3E
97. 3
97.2
?6. 8
97. 10
♦3-1E i
30 :
32 :
31
31. 0
•3-4S,
34
31
36
33. 7
#3-6E
45
37
34.
38. 7
f3-l£
31
31
31
31. 0
#3-4S
29
30
24.
27. 7
•3-6E
43
42
42.
42. 3
#3-lE
96. 5
97. 1
97. 2.
96. 93
•3-4S,
97. 2
96. 9
96. iL
) 96. 97
#3-2S_
38
32
35
35.0
*3-4E
38
35
38
37.0
• 3-2S
30
27
28
28. 3
•3-4E
27
34
34
31.7
IOT3
31. 6
30. 3
29. 7
30. 5
— • TWX ‘ > ' 0 ’ 6&, ’ 3 ° ' F “ ' <m>
Page
2 of 6
2«. Carbon Assay,
MDQAI 5560
T 4 Fabric,
(CONTINUED)
mr High LotJL
2b. Hydrogen Assay,
MDQAI 5560
2c. Nitrogen Assay, *
MDQAI 5560
3. Visual Inspection
QCi-102
4. Specific Gravity, Units
PTM-64
.kote. d “*
See Charts 3A-3F
43-1S.
2.9910
2. 9886
2. 9062,
AVG. 2. 962
1 3-l£.
2.7440
2.5514
6228
2.639
Page 3 of 6
4 . Specific Gravity, Units
PTM-84
AVG.
rt-3 F^hrle f or HASA_ l»o*f L-3-
(COHTIKUED)
*3-25
2. 4989
2 . 6106
2. 5835
2.564
AVG. 2.774
5.
pH, Unite
CTM-24B
AVG.
AVG.
6. TOA, -C .t sex «**» M L °**
CTM-51 (AIR)
7
SET
.55
up §X
~ ’
3-1S
647
3-2S
647
3-3E
644
3-4E
651
3-5E
652
3-6E
649
AVG.
648
*3-35
7.2
7. 1
7.15
# 3-65
6.0
ft. 0
6.00
*3-35
2. 3014
2. 1918
J 2 . 2203
2.238
#3-3E
2. 7607
2. 7008
2. 7294
2.730
*3-45
2.6102
2.6347
£. 5935
2.613
#3-55
3. 0945
2. 9334
J2. 9026
2.977
f3-6S
2.6413
2. 5773
5808
2.600
f 3-6E
2.6548
2. 4646
2- 5079
2.542
#3-15.
*3-15
7.5
7.2
7.4
Z_tJ2
AVG.
7.45
7. 20
*3-45
2. 6355
2.7418
2.7169
2. 698
|.HT3 AVG
2.7094
2.6861
?. 6872
2.694
cft UP €2
IE 593
3
3-2E
3-3S
3-4S
3-5S
3-6S
590
585
587
585
568
AVG.
588
irte 6 A- 6 L
#3- IS
*3-15
*3^25
325
26
7a. Atomic Absorption, PP«
Ha
395
357
39
10
58
0
464
CTM-53B
K
Ca
Hg
40
11
40
5
38
0
Li
AVG.
0
486
394
Na
K
Ca
KQ
Li
AVG.
f 3-25
318
30
5
36
__®
389
*3-35
325
26
10
96
0
457
*3-35
375
29
9
52
465
#3-4S
400
24
7
91
0
522
• 3-45
362
35
8
40
0
465
Page
4 of 6
J (CONTINUED)
Atomic Absorption, PP
CTM-53B «3-5S £2
Na
K
Ca
Wg
Li
AVG.
7b. Moisture Content, X
CTM-53B
S3-5S
446
40
2
42
©
530
7c. Ash Content, X
CTM-53B
S3-5E
333
34
11
52
0
430
#3-lS
#3-lE
#3-2S
#3-2E
#3-3S
#3z3E-
#3-lS
#3-lE
#3-2S
#3-2E
#3-3S
#3-3E_
#3-6g.
395
23
12
60
0
490
7.188
6.762
7.021
7 . 001
6.846
6.724
Lot# 3
.115
.095
.089
. 114
. 135
,710 -
f3-6E
362
23
2
45
0
432
#3-4S
#3-4E
#3-5S
#3-5E
#3-6S
S3-6E —
average
#3-4S
#3-4E
#3-5S
#3-5E
#3-6S
#3z6£_
71W
Lot# 3 AVERAGE
SB Filament diameter, «icron AVERAGE
S.E.M. procedure Hinimum
(diameters are an averag Maximum
10 measurements ) std . Dev
§ 2 z. 4 §-
AVERAGE 11* ^
Minimum 1®* 4®
Maximum l1 *®^
Std. Dev 0. 53
ab Fll..ent dl.«t.r, -Icron., FILL.
S-E.H proc.--r. .
< r f *ic t :.:.ur:..nt.>
9.. Thr..- Count# P*r inch#
PTM-SA
#3- IS
10.82
10. 00
11. 85
0.53
f3-5S
10. 48
8.80
11.60
1.02
*3-2S
11.08
10. 00
14. 00
1.28
#3-6S
12. 38
9 . 00
15. 95
2 . 02
] nT3 AVG
367.8
30 . 8
7.7
54. 2
O
460.3
6.811
6.491
6.609
6.618
6.741
6. 428
6.770
. 155
.234
.222
. 109
. 105
. 070
. 138
#3z2S
10.76
9. 40
12.00
0. 89
i2z±§-
AVERAGE 12. 73
Minimum H- ^®
Maximum 15. 85
Std. Dev 1*2®
#3- IS.
52
53
53
52
53
52.6
#3-lE
52
52
52
52
52.
52. ®
#3^2g.
52
52
52
53
53
52. 4
Page 5 of 6
Thread Count, per inch
PTW-5A
for NASA lot*.
WARP (CONTINUED)
AVG.
AVG.
1 3- -2E
52
52
53
53
53
52.6
f3-5S
52
52
52
52
22
52.0
#3-35
52
52
52
52
S3.
52.2
#3-45
52
52
51
52
22
51. 6
9b. Thread Count,
PTM-5A
per inch, FILL
#3-55
54
#3-65
53
#3-6E
53
53
53
54
53
52
53
52 .
53
53
52
52.6
52
52.6
£3.
53. 2
#3-15
#3-lE
49
49
49
49
49
46
49
49
49
49
AVG.
49.0
46. 6
AVG.
AVG.
t 2z2 &
50
49
50
50
43
49.6
#3-55
49
49
50
49
50
49.4
f3-3S.
50
49
49
49
49
49.2
#3-35
49
49
49
49
£0
49.2
#3-45
49
49
49
49
49
49.0
#3-5E
#3-6S
#3-65
47
49
49
48
49
49
48
49
50
49
49
49
4B
48.8
49
49.0
43
49.2
10a. Areal aeight a
PTM-3A
. r.c.lv.d, g./4«4 LEpT
CENTER
RIGHT
AVG.
#3-15
2.991
3. 006
3. 001
3. 000
LEFT
CENTER
RIGHT
AVG.
#3-35
3.069
3.036
3.065
3.056
#3-35
3. 166
3.062
3 . 149
3.132
49.2
Page 6 of 6
, ^ n */4x4 (COHTINUED)
1». *r..l «l9 h t - r.dved, 9 »'<*
PTM-3A — — J,#3 - K,p -
LEFT
CENTER
RIGHT
AVG.
10b. Volatiles
PTM-3A
is received, X
LEFT
CENTER
RIGHT
AVG.
LEFT
CENTER
RIGHT
AVG.
f3-2&
6.42
6. 13
p.54
6.03
f3-5S
6.91
6.78
7 . 11 .
6. 93
10c. Weight Change on Acetone Wash, X
PTH -3 A CENTER
RIGHT
AVG.
f3-3£
- 3 . 11
-2.83
-2.29
-2.74
LEFT
CENTER
RIGHT
AVG.
LEFT
CENTER
RIGHT
AVG.
^.r>T3 AVG
3. 064
3.036
3.057
3. 052
-.19
U. S. Polymeric
\ HT3 AVG.
- 1.16
-1.18
-1.15
A
M-
u.nid M. Ouraishi, Manager
ORIGIN/.' ?A'GE IS
OF POOR QUALITY
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TABLE OF CONTENTS
PREPREG TESTING
NAS8-36298
U.S. Polymeric 0. E. 71108
FM 5055B HASA LOT* 3 U.S.P. LOT* C02133
TEST
PAGE
. . 1
la»
Resin Content, Soxhlet
.. 2
lb.
Filler Content Soxhlet
.. 2
lC.
Cloth Content Soxhlet
.. 3
2.
3.
4.
5.
6.
7a.
7b.
7c.
a.
9.
10.
Volatile Content *
Flow * *
Reein Content., Dry y ‘ '
Tack
Gel Time
Atomic Absorption
Moisture Content. ********
. . 3
.. 4
.. 4
.. 4
.. 5
. . 5
5
Ash Content ! ! ! '. '. ! !
Infrared (IRZB) Baseline
. • w
.. 6
.. 6
.. 6
... 6
11.
12.
13a.
13b.
13c.
Environmental History. • *
Specific Gravity . . .
Tensile Strength *
Tensile Modulus
Tensile Elongation
,.. 7
, . . 7
... 8
. . . 8
... 9
14a.
14b.
15a.
15b.
16.
17.
Flexural Strength *
Flexural Modulus. # # #
Compressive Strength. ...•••
Compressive Modulus # # # f
Double Shear Strength
Barcol Hardness
... 9
. . . 10
. . . 11
. . .11
. . . 12
. . . 12
ia.
19.
20.
Residual Volatiles *
Resin Content, Pyrolysis
Acetone Extraction
. . . 12
. . . 13
. . . 13
21a.
21b.
CTE, with ply
CTE, crossply
. . . 14
DSC
Infrared (IRZB)
CTE
Baseline.
6A -
9A -
10A -
21A -
8N
9N
10N
21N
CHARTS
Udp
USRjfymeric m
Page 1 of 14
prepreg TESTING
HASS-36298
U.S. POLYMERIC O. E. 71108
PH 5055B_NASA_kQI#
p. LOT# C 02133
1*. Resin Content,
CTH-6D
ROLL# 3
START
33. 5
32. 0
32. 9.
AVG. 32. 8
R0LL#6
END _
35.8
33. 5
35. 5
AVG. 34. 9
Soxhlet, X
AVG.
R0LL#3
ROLL#4
pND
START
33.8
33. 9
33.9
32. 4
33.9
32.0
33. 9
32.8
R0LL#7
R0LL#7
START
END
35. 9
33. 1
33. 4
32. 2
35. 9
32.2
35. 1
32. 5
R0LL#1
ftTART
35.4
35. 1
32.7
34. 4
ROLL# 1
END _
33.6
34.4
34.7
34. 2
R0LL#2
START,
35. 9
36. 3
35. £
35.9
R0LL#2
END
R0LL#4
END _
33. 5
35.2
33-3-
34.0
ROLL# 5
?TART_
33. 8
32.7
35. _3.
33.9
R0LL#5
END
R0LL#8
SXABI_
roll#s
END
R0LL#9
?tart__
R0LL#9
END
NASA LOT# 3 AVERAGE 34. 1
HfTCO MATERIALS DIVISION
700 E. DYER ROAD, SANTA ANA. CALIFORNIA
92707 • (714)
549-1101 • TWX (910) 595-1130 •
FAX # (714) 549-2858-5-2437
Page
2 of 14
:m S055B,
NASA_LQT#_3_
l P-
Filler Content*
CTH-6D
AVG.
R0LL#6
f-ND —
AVG.
Soxhlet, X
R0LL#3
END
AVG.
R0LL#1
fTART_
R0LL#4
END
OT* f-S2l33
ROLL.fl
f.ND -
14. 1
14.5
14._&
14. 4
ROLL# 5
«yTART_
ROLLfS
^tart —
ROLLfS
f.ND -
ROLLfS
PHD
R0LL#2
F.ND
ROLL# 3
f TART —
ROLLfS
F.ND _
HASA LOT# 3 AVERAGE 14.3
lc. Cloth Content,
CTH-6D
AVG.
AVG.
Soxhlet,
ROLLfS
F.ND _
ROLL# 3
£Nfi
ROLL# 2
END
ROLLfS
f TART ,
ROLLfS
END _
ROLLfS
f TART_
ROLLfS
END-
MASA LOT# 3
AVERAGE 51.5
Page 3
fh S855 n HASA LOT# 3_
n.s.p. i nT<
2. Volat.il-® Content, *
PTH-17B
AVG.
R0LL#3
START _
3.7
3.5
2 * 2 .
3.6
R0LL#6
END
4. 4
3.9
2 * 3 .
4. 1
R0LL#3
EHD _
3.6
3. 5
2 * 3 .
3. 6
R0LL#7
START
4.6
3. 8
2 * 3 .
4. 1
AVG.
RDLL#4
START _
3.9
3. 4
4.8
3.8
R0LL#7
£HD _
3.9
3.8
2 * 2 .
3.8
R0LL#1
ftTART_
4.3
4. 1
4. 8
4.4
R0LL#4
EHD _
3. 9
3.7
3^8
3.8
R0LL*1
EHD _
3.8
3.6
3^6
3.7
ROLL* 5
START _
4.8
3.7
3. 8
3.8
R0LL#8 ROLL# 8
pTART EHfi
R0LL#2
ftTART
4.3
3. 9
±3.
4. 1
R0LL#5
END
4.2
3.5
3.5
3.7
R0LL#2
EHD _
3.9
3. 8
2*3
3.8
R0LL#6
START
3. 8
3.6
3.6
3.7
R0LL#9 R0LL#9
START EHfi
NASA LOT#
AVERAGE 3. 8
3. Floe, X
PTK-19G
AVG.
R0LL#3
pTART _
11.7
15.8
14. 1
13.6
R0LL#6
EHD
17.7
17.8
17.5
17.7
R0LL#3
pHD _
19.7
16.2
17. 8
17.6
R0LL#7
ftTART
19.4
17.2
16.8
17. 8
AVG.
R0LL#4
ffTART_
11. 4
18. 5
12. 8
11.3
R0LL#7
f-ND
18. 5
19.7
19.5
19. 2
R0LL#1
START _
19. 5
17.8
18. 1
18. 5
RQLL#4
END _
11.7
12.3
li.e
11.9
roll#i
EHD _
16. 3
15. 4
16.7
16. 1
ROLL# 5
START_
13. 3
13.6
14.8
13.6
ROLL#8 R0LL#8
pTART EMfi
ROLL# 2
START
18. 9
17. 5
16.9
17.8
ROLL# 5
EHD
14. 3
14.3
13.8
14. 1
R0LL#2
END _
15. 6
11. 3
j4.8
13. 9
NASA LOT#
Page
4 of
i
rM sa55 P NASA LOT »_
ii, tt r, mu cfizm
«. Resin Content# Dry Reels, *
PTH-16F, Type II
AVG.
R0LL#3
pTART _
33. 9
33. 5
?3. 6
33. 7
R0LL#6
EHD _
35. 9
32. 9
35. 6
34. 9
R0LL#3
£HD _
33. 6
32. 6
32. 6
32. 9
R0LL#7
pTART
36. 3
32.7
35.7
34. 9
AVG.
RDLL#4
pTART _
35.6
31. 9
?7. o
34. B
R0LL#7
£HD -
33.6
32. 3
?2.9
32. 9
ROLLtl
pTART
36. S
35. 4
?6. 5
36. 1
R0LL#4
£HD
34. 1
31. 7
?4.6
33. 5
ROLL# 1
EHD
34.6
33.7
24aJ.
34.4
ROLL# 5
START _
35.7
32.0
?5.7
34. 5
ROLL#& ROLL# 8
pTART EH2
R0LL#2
pTART
36. B
34. 2
36. 1
35.7
R0LL#5
EHD __
35.0
33. 5
34. 5
34. 3
R0LL#9
5TART_
R0LL#2
EHD
34. 5
34. 1
33. 5
34.0
HASA LOT# 3 AVERAGE 34.3
5. TACK, lbe
PTH-80
6. Gel Time, Seconds
PTM-20E
roll#i-s
roll#i-e
R0LL#2-S
R0LL#2-E
R0LL#3-S
R0LL#3-E
R0LL#4-S
R0LL#4-E
pnLL»5-_E
HASA LOT#
roll#i-s
R0LL#1“E
R0LL#2-S
R0LL#2-E
R0LL#3-S
R0LL#3-E
R0LL#4-S
R0LL#4“E
POLL#5-S
63
95
61
3B
55
SO
44
32
49
NASA LOT#
R0LL#5-E
R0LL#6-S
R0LL#6-E
R0LL#7-S
R0LL#7-E
roll#b-s
roll#b-e
R0LL#9-S
ROLL#9-_E
3 AVERAGE
R0LL#5-E
R0LL#6-S
R0LL#6-E
R0LL#7-S
R0LL#7**E
roll#b-s
R0LL#8-E
R0LL#9-S
pm -L#9~E — .
^ 3 AVERAGE
Page 5 of 14
>133
Atomic Absorption,
CTM-53B
ppm
Ns
K
Ca
Hg
LI
TOTAL
Hs
K
Ca
Hg
Ll
R0LL#3
EHD
309
15
3
R0LL#4
START _
399
17
3
ROLLfl
START _
344
19
2
2
0
367
R0LL#4
EHD
456
14
2
ROLLfl
iMP
438
17
2
2
0
459
ROLLfS
START _
454
15
2
2
ROLL# 2
START
436
20
2
2
0
460
ROLLfS
END _
382
18
2
2
ROLL# 2
END _
428
20
2
3
0
453
ROLL# 6
START
500
20
2
1
ROLL# 3
START
276
16
2
2
0
296
ROLL# 6
END
494
21
2
3
TOTAL
Na
K
Ca
Mg
Ll
1
X
Ok
0
0
0
0
MJ
< a
328
1 0
420
473
473
404
523
jakI
ROLL# 7
START
R0LL#7
END
ROLLfS
START
ROLLfS
END
ROLL49
START
R0LLf9
END
LOT# 3
AVG.
410
533
288
* " 1
—
18
22
18
--
2
2
2
0
2
2
0
559
310
432
TOTAL
7b. Moisture Content, X
CTK-53B
7c. Ash Content,
CTM-53B
R0LL#1-S
ROLLfl -E
ROLL# 2~S
R0LL#2-E
R0LL#3-S
R0LL#3-E
ROLL# 4-S
ROLL# 4-E
>OLLf 5-_T
roll#i-s
ROLLfl-E
ROLL# 2-S
R0LL#2-E
ROLL# 3-S
ROLL# 3~E
ROLL# 4-S
R0LL#4-E
RQLLfS-
5 . 22
5. 19
5. 13
5.48
5.05
4.99
5.06
4. 86
5. i:
16
, 11
.07
. 12
.21
. 12
. 15
. 19
18
NASA LOT#
ROLL# 5-E
ROLL# 6-S
ROLL# 6-E
ROLL# 7-S
ROLL# 7-E
ROLLfS -S
ROLL# 8-E
ROLL# 9-S
ROLL# 9~E_
3 AVERAGE
ROLL# 5-E
ROLL# 6-S
R0LL#6-E
ROLL# 7-S
R0LLf7-E
ROLLfS -S
ROLL# 8-E
ROLL# 9-S
ROLL# 9-J
3 AVERAGE
5. 03
5. 24
5. 42
5. 34
5.21
17
20
31
26
.23
p§ge 6 of
8 TGA, * »«i9 ht l0 *’’ * l S0ia ‘ C
CTK-51 <Nitrog*n>
R0LL#1-S
R0LL#1-E
R0LL#2-S
R0LL#2-E
R0LL#3-S
R0LL#3-E
R0LL#4-S
R0LL#4-E
?m-L»5-S_
10.9
9.7
9.6
9.4
9. 1
9.5
10.4
9.5
10 . 1
R0LL#5-E
R0LL#6-S
R0LL#6-E
R0LL#7-S
R0LL#7-E
R0LL#8-S
R0LL#6-E
R0LL#9-S
pm L»9-E_
3 AVERAGE
5. 9
8.9
10 . 1
10. 3
11. 1
9. DSC , *C
CTM-50A
roll#i-s
R0LL#1-E
R0LL#2-S
R0LL#2-E
R0LL#3-S
R0LL#3-E
RQLL#4-S
R0LL#4-E
R0LL#5-S
R0LL#5-E
R0LL#6-S
R0LL#6-E
R0LL#7-S
R0LL#7-E
R0LL#8-S
R0LL#8-E
R0LL#9-S
p ni.l.#9-E
NASA LOT# 3 AVERAGE
See chert 9A-9N
See chert 8A-8N
gypST t cmpfr atuRE-
T * e AA
180
'175
177
179
176
174
179
178
178
179
179
178
178
178
178
10 .
Infrered
CTM-21C
( IRZB) Beeeline
roll#i-s
roll#i-e
R0LL#2-S
R0LL#2-E
R0LL#3-S
R0LL#3-E
R0LL#4-S
R0LL#4-E
pnLL»5-S_
1.
1.
1.
1
1
1
1
1
13
13
13
07
pr.rQN P TEMPERATUR .E
233
235
232
236
237
234
237
237
238
236
235
234
235
235
235
R0LL#5-E
R0LL#6-S
R0LL#6-E
R0LL#7-S
R0LL#7“E
R0LL#8-S
R0LL#6-E
R0LL#9-S
pnt r L»9-E_
3 AVERAGE
1.
1.
1.
1
1
08
11
10
, 15
. 14
See
chert 10A-10N
Envlroneentel Hletory
D . t . "• r, “'* ct p"yithyl.« r big l -*P port * d
p.ck.g* in. *° l £. rd j, 0 « rd e.rton
12 June 1986 in
Dete ehippeds
Page
7 of 14
, r L0T * 3-
Bpedflc Gr.vlty, Cured, Unit.
ASTW D792
AVG.
AVG.
R0LL#3
START_
1. 483
1. 483
1-483.
1. 483
R0LL#6
EHD __
1. 488
1.486
It 187
1.486
R0LL#3
EHD _
AVG.
R0LL#4
START
13a. Tensile Strength, kei,
FTMS 406-1011
WARP
R0LL#7
£ND _
1.483
1. 480
1.476
1. 480
R0LL#4
END
1.473
1.481
1-453
1.469
R0LL#8
PTART-
AVG.
ROLL# 3
EHD _
25. 40
24. 10
22 . 68
22. 19
?4.05
23.68
ROLL# 1
£ND
1.464
I. 462
J. 409
1.445
R0LL#2
*5TART
1. 484
1. 483
j. 481
1. 483
R0LL#2
pND
1. 398
1. 446
|. 418
1.421
R0LL#5
start
R0LL#5
EHD
R0LL#6
START
1 AAA
R0LL*8
EM2
R0LL#9
START _
R0LL#9
Ei4D
NASA LOT# 3
AVG.
R0LL#6
EHD _
21. 96
21. 61
20 . 01
22. 19
?2.55
21.71
AVG.
R0LL#4
START —
21. 52
22. 45
22. 54
21.75
23. 00
22. 25
R0LL#7
f.ND _
21.24
20. 45
21 . 13
18.53
gl.Slu
20. 57
R0LL#4
END __
19. 34
21 . 16
21.48
20.97
21 . 32
20. 65
ROLL# 6
START _
AVERAGE 1. 473
ROLL# 5
^TART_
20. 36
20. 19
19.93
21.02
21 -.25
20. 65
R0LL#8
EHD
NASA LOT# 3
AVERAGE 21.21
Page B of 14
rw 5055B,
lot* J — iin . p lOTf cMi aa.
13b. Tenallb HoduluH, ael, WARP
FTMS 406-1011
AVC.
RQLL#6
EMD __
AVG.
R0LL#2
^TART _
3. 0®
2 . 86
2 . 98
3 . 12
2. 87
2. 97
R0LL#5
EHD _
2. 96
R0LL#2
EMD _
R0LL#9
START
R0LL#9
END
NASA LOT# 3 AVERAGE 3.04
13c. Tensile Elongation, X,
FTMS 406-l®ll
R0LL#3
START _
.92
1.05
.97
1.05
12 .
1.02
R0LL#3
EHD,
40
33
1. 18
1 . 20
LOl L
1.26
WARP
AVG.
R0LL#4
STARTs
1.09
1.17
1. 16
1 . 12
UA4
1. 14
ROLL#4
EHD
R0LL41
EHD _
.98
1.05
1.01
1.01
-,21
.99
ROLL#S
START —
.08
11
1.04
1. 13
LO 5
1 . 10
1.
1.
R0LL#2
£TART_
1.04
1.02
. 97
R0LL#5
EHD _
1 . 11
R0LL#2
EHD
AVG
Page 9 ^
14a.
ROLL# 6
R0LL#7
END
ftTART
1.13
1.03
1.17
1. 14
1.09
1. 14
.96
1.13
^.15
LO*
AVG. 1-1®
1. 12
Flexurel Strength# hal
FTMS 406-
1031
ROLL# 8 R0LL#6 F0LL#9
pTART END glABX-
R0LL#9
END
HASA LOT# 3 AVERAGE l.®9
ROLL#l
ftTART —
36.08
35.98
36.75
36.95
ROLL#l
END _
36.71
34.90
33.06
41.06
AVG.
AVG.
£7. 68
36. 69
42.95
37.73
ROLL# 3
§TART
R0LL#3
END
RQLL#4
START
R0LL#4
END
35. 38
33.44
33.79
32.90
34.07
33. 91
ROLL# 5
{■START
31. 74
35. 36
34.27
33. 85
37. 60
36. 29
35. 47
40.63
44.99
40.27
39. 47
40. 14
41. 10
34. 48
35. 69
32. 21
32. 70
?4. 42
33. 90
35. 62
36. 83
39. 58
36. 80
36. 51
R0LL#2
START _
33. 49
27. 46
33. 09
34. 58
34. 37
32. 60
RQLL#5
END
R0LL#2
END _
40. 68
36. 14
39. 13
39. 00
36. 58
38. 30
AVG.
R0LL#6
END
30. 63
34. 28
37. 18
38. 38
33. 43
34. 78
R0LL#8
ftTART _
ROLL# 8
END
R0LL#9
£TART _
R0LL#9
END __
HAS* LOT. 3 AVERAGE 35. 1®
14b. Fl.xur.l Hodulu., ML SARP
FTMS 406-1031
R0LL#1
{START —
2.68
2.50
2. 84
2.99
&-5B
R0LL#1
END
2.82
2.80
2. 89
2.73
3. 11
R0LL#2
f-ND _
2. 69
2.68
2.81
2. 84
AVG
Page
10 of 14
■1 r . WB MA SA L0T«_3 ILr I* I" 1 * «® ?ia3 -
, MnrfuluB «.l, WAR p ‘CONTINUED)
14b. Flexural Moaulua,
FTWS 406-1031
AVG.
ROLL# 3
START _
2 . 84
2.68
2.57
2.72
2.90
2.74
RQLL#6
END __
2 . 86
2.73
2.64
2. 82
2.47
2.70
ROLL# 3
END _
2. 92
2. 81
2.84
2.70
2.83
2.82
RQLL#7
ftTART
2.75
2.87
2.71
2. 32
?.69
2.67
RQLL#4
pTART _
2.60
2.42
2.66
2.47
2.74
2.58
R0LL#7
END __
1.93
2.57
2. 94
2.75
?.64
2.61
ROLL# 4
pND
2.43
2.78
2.76
2.59
2. 58
2.63
ROLL# 8
£TART__
ROLL# 5
START —
3.06
3. 17
3.09
3.35
3.27
3. 19
ROLL# 8
END _
ROLL# 5
|END
2. 82
2. 98
2 . 21
2.32
2. 72
2.61
RQLL#9
START _
R0LL#6
START_
2.31
2. 61
2. 54
2.73
2.71
2.58
R0LL#9
END _
15.. Co»pr...iv. Str.ngth, k.l, N* RP
FTMS 406-1021
R0LL#3
START _
60. 25
52. 48
43.92
59. 52
61. 08
55. 45
R0LL#6
END _
56. 89
49. 98
54. 63
49.56
S6. 00
53. 41
R0LL#3
END
51. 89
52. 59
64.72
63.44
62. 13
58.95
R0LL#7
£TART
56. 95
62. 3®
52. 83
56. 31
54. 49
56. 58
MAS* LOT# 3 AVERAGE 2. 72
R0LL#4
START
48.83
60.64
54. 38
66 . 11
67.95
59.58
R0LL#7
END _
54. 21
56. 45
59. 29
54.85
54.60
55. 88
ROLL# 1
START
62.60
61.55
59.06
60.74
57. 41
60. 27
ROLL# 4
END
59. 23
63.44
61. 55
60.69
53.50
59.68
R0LL#8
START _
ROLL#l
£ND _
48.73
64.07
63.42
64. 43
sa. 27
59.78
ROLL# 5
START_
51. 62
58. 09
53. 18
54.76
48 . 54
53. 24
R0LL#8
END _
R0LL#2
START _
51.96
61. 36
57. 80
63. 24
fr2.74
59. 42
R0LL#5
END __
52. 12
56. ®5
50.77
61. 83
59 . 22
56. 00
R0LL#9
SIASI—
R0LL#2
END __
59. 70
62.56
58. 95
57. 13
55. 63
58.79
NASA LOT# 3
AVERAGE 56.98
Page
11 of 14
ISb.
16
c r'* ctc;n HAS* LOT* JL
:o.pr...iv., Kodulu., -1. W * BP
FTHS 406-1021
n S.P. inT< c &
VC.
R0LL#6
END.
VG.
auble Shear Strength, kal
FTHS 406-10414
AVG.
roll#i
pND
3. 07
3. 12
3.06
3.09
3. 06
3.06
R0LL#2
«?tart
R0LL#2
END
3. 00
3.07
3. 13
3. 19
?.38
3. 15
3.22
3. 09
2. 96
3.04
3. 08
ROLL# 5
Sf ART
R0LL#5
END
R0LL#6
START
3. 14
3.23
3. 03
3. 04
?.03
3. 09
3. 42
3.38
3. 46
3.31
37
3. 39
3. 07
3. 32
3.05
3. 09
?.02
3. 11
R0LL#8
£ND
R0LL#9
ETART_
ROLL# 9
END
—
--
— —
NASA LOT# 3 AVERAGE 3.13
AVG.
R0LL#3
END _
4.66
3. 51
4.72
4.77
105
4.40
ROLL# 4
END
(CONTINUED)
Double Shear Strength, kal
FTNS 406"!®^^
t VG.
R0LL#7
R0LL#7
£TART
pND
5.69
5.56
5.66
4.75
4. 13
4.59
4.64
4.79
4. 19
?.53
4.66
5.04
ROLL# 8
ftTART_
ROLL# 8
END _
ROLL# 9
START _
R0LL#9
END
HAS* lot# 3 AVERAGE 5. »®
Barcol Hardness,
ASTM D-2583
(Average of 1®
determination* >
Units
R0LL#1-S
roll#i-e
R0LL#2-S
R0LL#2-E
R0LL#3-S
R0LL#3-E
ROLL# 4 -S
R0LL#4-E
R0LL#5-E
R0LL#6-S
R0LL#6-E
R0LL#7-S
RQLL#7-E
R0LL#8-S
R0LL#8-E
R0LL#9-S
pni.L#9-E_
74.6
73.7
73. 3
74. 0
73.®
Residual Volatile*® *
PTN-98
AVG.
AVG.
Remin Content, Pyrolysi*® *
CTN-14B
32.31
32. 61
22*99
AVG
Pgge 13 of 14
19.
Corit.nt, Pyroly.l.. * .COKTINUED,
CTM-14B
R0LL#4
END _
32. 82
33. 11
31.7a
32.55
ROLL# 5
END
R0LL#6
END _
AVG.
R0LL#7
j^TART
35.86
36.49
36.73
36.36
R0LL#7
END _
34. 04
34. 49
94.25
34.26
R0LL#8
£TART_
ROLL# 8
END
ROLL# 5
START _
33. 35
34.98
?4. 57
34. 98
R0LL#9
£TART
ROLL# 6
END _
35. 07
34. 38
35.74.
35.06
ROLL# 9
£ND
NASA LOT# 3 AVERAGE 34.04
20. Acetone Extraction, X
CTM-18A
AVG.
AVG.
R0LL#3
END _
.33
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Page 14 of 14
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\
Hamid H.
Quality
Quraishi, Manager
Assurance Departmen
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