Document text
U.S. POLYMERIC
HITCO MATERIALS DIVISION
uop
U «S Polymeric ■
(FASA-CEt
I iitQbi :
-1794 I?)
IB 5634
CAT A
143 F
CSC L 11B
G3/27
H89- 1 3604
Onclas
0140168
FM 583*1 LOT #2
D-09275
FINGERPRINT TEST DATA REPORT
NAS8-36298
COPY # 9
uop
rrc zxjl— v, B
U&Fbfymeric
Page 1 of 2
1. Carbon Content,
QAI-5560
2. Ash Content,
PTM-71B
3. Atomic Absorption, ppm
CTM-53B
(Values are average of
2 determinations)
FILLER TESTIHG
NAS8-36298
U. S. POLYMERIC 0. E. 71108
Filler Lot for NASA Lot# 2
SAMPLE
3a. Moisture Content,
CTM-53B
3b. Ash Content,
CTM-53B
4. pH, Units
ASTM D1512
5. Particle Size, microns
S. E. M. procedure
(Average values are
of 20 determinations)
Sa. TGA, *C at 50% Loss
CTM-51
#2A-1
#2A-2
#2A-3
99. 31
99. 18
99. 40
NASA LOT#
2
AVERAGE
99. 30
0.0
0. 0
0. 0
0.0
0. 0
0. 0
AVG.
0.0
0. 0
0.0
NASA LOT#
2
AVERAGE
0. 0
#2A-1
#2A-2
#2A-3
L0T#2
AVG- _
Na
7.0
7.5
9.0
7. 8
K
1. 5
1.0
2. 5
1.7
Ca
2. S
1. 5
2. 0
2. 0
Mg
0.0
0.0
0. 0
0. 0
Li
0.0
0. 0
0. 0
TOTAL
11.0
10.0 13.3
11. 5
.041
.034
.039
, 03JL
t?45
AVG.
. 036
. 027
. 042
NASA LOT#
2
AVERAGE
.035
0. 003
0. 000
0. 013
e.Qge
e.025
0. 000
AVG.
0. 003
0.013
0. 008
NASA LOT#
2
AVERAGE
0. 008
4.60
4. 40
4. 50
4.60
AVG.
4.60
4. 30
4. 60
NASA LOT#
2
AVERAGE
4. 57
AVG.
.36
. 37
. 52
Maximum
.90
1. 25
1. 17
Minimum
.23
. 20
. 25
Std. Dev
.22
.28
. 24
NASA
LOT# 2
AVERAGE SIZE . 55
842
850
857
NASA LOT#
2
AVERAGE
850
HITCO MATERIALS DIVISION
700 E. DYER ROAD. SANTA ANA, CALIFORNIA 92707 • (714) 549-1101 • TWX (910) 595-1130 • FAX # (714) 549-2858-5-2437
Page 2 of 2
6b.
7.
7a
Filler Lot for NASA Lot* 2
TGA See Charts 6A-6C
CTH-51
Particle Size Distribution See Charts 7A-7C
CTM-72
Particle Size, microns #2A-1
#2A-2
i2Az
CTM-72
.97
.95
.65
1. 08
*32,
AVG. . 86
1.82
. 94
NASA LOT#
2 AVERAGE
.94
U. S. Polyseric
Hasid M. Quraishi, Manager
Quality Assurance Departaent
CHART NO. RNJ-Ol-JS-JOM _ <*»«
CHART 6A
ORIGINAL PAGE IS
OF POOR QUALITY
I
W - WKIOTf CEAKUK TC - THKMX.'OOVtJi
CHART NO. RNR-OI-73-JOM
ORIGINAL P AGE IS
OP POOR QUALITY
CHART 6C
weight
» DISTRIBUTION TABLE (BV VOL.)
CHART 7 A
•Ji-JCxNAL PAGE IS
Oft POOR QUALITY
4^
CHART 7B
ORIGINAL PAGE IS
OF. POOR QUALITY.
ORIGINAL PAGE IS
OF POOR QUALITY CHART 7C
£-9C*+1 i I C'V<1J°1
TABLE OF CONTENTS
TEST
1.
2 .
3.
4.
5.
6 .
7.
8.
9.
10 .
11 .
12 .
13.
14.
15.
RESIN TESTING
NAS8-36298
U. S. Polymeric O.E. 71108
91 LD Resin Lot for NASA Lot# 2
Resin Solids
Specific Gravity. . . .
Brookfield Viscosity
Gel Time
Atomic Absorption. . .
Gas Chromatography. .
TGA
DSC
HPLC
GPC
PH
Phenol Content.
Chang's Index
RDS
NMR
PAGE
. 1
. 1
. 1
. 1
. 1
. 1
. 1
. 1
. 1
. 1
. 2
. 2
. 2
. 2
. 2
CHARTS
Gas Chromatography
TGA
DSC. .
HPLC
GPC
RDS
6A
7A
8A
9A
10A
6C
7C
ec
9C
10C
14C
15C
NMR
14A
15A
Page 1 of 2
US Fbiymehc
RESIN TESTING
NASS -36298
U. S. Polymeric 0. E. 71108
91LD Resin Lot for NASA Lot» 2
1. Resin Solids, X
PTK-7C
AVG.
2. Specific Gravity 9 25* C
PTM-29C
3. Viscosity, Brookfield, cps. 0 22. 8* C
PTH-14C
4. Gel Time, min: sec
PTM-47B
5. Atomic Absorption, ppm £2;
CTM-53B Na 4
K 0
Ca 3
Mg 1
Li _0
AVG. 8
6. Volatiles, Gas Chromatography
CTM-55
7. TGA, X Weight Loss at 500* C
CTH-51 (AIR)
8. DSC, temperature *C
CTM-50A
9. HPLC
CTM-49A
10. GPC, Average molecular *t.
CTM-49A
#2-1
#2-2
#2-3
70. 8
70. 4
71. 7
70. 8
70. 2
71. 2
71. 9
72. 0
70. 5
71. 2
70. 9
71. 1
Lot#
2
AVERAGE
71. 1
1. 141
1. 140
1. 139
Lot#
2
AVERAGE
1. 140
1250
1250
1500
Lot#
2
AVERAGE
1333
3:30
3:38
3:34
Lot#
2
AVERAGE
3:34
#2-2
#2-3
LOTI AVG
4
8
5. 3
0
0
0. 0
2
2
2. 3
1
1
1. 0
1
0
0. 3
8
11
9. 0
See Charts 6A-6C
#2-1
#2-2
#2-3
39. 5
40. 1
39. 4
Lot#
2
AVERAGE
39. 7
See Chart 7A-7C
183
191
183
Lot#
2
AVERAGE
188
See Chart 8A-8C
See Chart 9A-9C
1718
1801
1598
Lot#
2
AVERAGE
1706
See Chart 10A-10C
~ A HITCO MATERIALS DIVISION
700 E. DYER ROAD, SANTA ANA, CALIFORNIA 92707 • (714) 549-1101 • TWX (910) 595-1130 • FAX # (714) 549-2858-5-2437
Page 2 of 2
91LD Resin Lot for HASA Lot» 2
11. pH, unite
CTM-1B
12. Phenol Content, X
CTM-55 Appendix 1
13. Chang's Index, ml.
CTM-5B
14. RDS, Minimum Viscosity, cps.
CTM-57A
15. NMR
Vendor procedure
#2-1
#2-2
#2-3
a. s
8. 3
a. 4
Lot#
2
AVERAGE
8. 4
10. 04
11. 09
11.74
9. 83
10. 80
11. 88
AVG.
9. 94
10. 94
11. 81
Lot#
2
AVERAGE
10. 90
24. 2
24. a
25. 2
Lot#
2
AVERAGE
24. 7
Min. Vise.
■C
#2-1
278
107
#2-2
249
111
#2-3
239
113
AVG.
255
110
See Charts 14A-14C
See Charts 15A-15C
U. S. Polymeric
Hamid M. Ouraishi, Manager
Quality Assurance Department
TYPICAL GAS CHROMATOGRAPH SET-UP
ORIGINAL PAGE E5
OF POOR QUALITY
Operator.
Column
Length «
Die
Liquid Phase
*t. % cz
Support.
Mesh
Carrier Gas
Rotameter
nuisoic ici .1 1 ■> ■■
Inlet Pres$_£2£psig
Rite. 3*£2. — il/Bin
CHART SPE
SAMPLE
Size _
EED r-
Bate.
•etecto
Vo I tage
Sens i t
Floe Rite*, tl/sin--!
Hydrogen pQ. Ai r Zpg
Scavenge
Split
Temperature, # C — _ —
Bet. a Za&L In j . pU£3
Coluin initiii m?
Final jaLLQ.
Rate .
Solvent _
Concn.
m
mu
' mr $A
GAS CHROMATOGRAPHY STANDARD SOLVENT
TEST METHOD CTM-55
STANDARD SOLVENT/MONOMER RETENTION TIME (MINS.)
MEOH
ETHANOL
MECL2
ACETONE
1PA
THF
ACETONITRILE
CRESOL
MEK
FURFURAL
TOLUENE
CHLOROBENZENE
PHENOL
.6
1.18
1.28
1.A5
1.83
3.08
3.2
A. 03
A. 08
15.03
17.98
19.6
22.08
NOTE: THF WAS USED TO DILUTE THE RESIN SAMPLES.
ORIGINAL PAGE IS
OF POOR QUALITY
CHART 6A
VERTICAL SCALE FACTOR 1
*** F.EAL TIME CHROMATOGRAM *1-*
ru_
INAL FULL SCALE MV =1000.00
SAMPLE' SI LD 2-1
1 1 SC . • C=0 101701 GrtS/HL
T I ME : 11 49
TATE 1 2-1 0-8 S
jRERATOR : JGZ
RUH TIME- 30.00 MINUTES
JELAY TIME 0-00
SHAN = 0
P|: RET PEAK AREA B PEAK
Vo. TIME AREA XL HT
2 .65 1709 .075 2
=, i.?0 204140 8.56$ 2
£ 7 05 2010900 84.397 3
7 5 55 1537 .065 4
IS 11.90 2214 .093 2
39 22 05 162080 6 . 802 1
TOTAL AREA= 2382661
THRESHOLD* 1
MIN FT WIDTH* 15
9REA REJECT* 1000
235
11953
84306
127
96
8700
19 -
SAMPLE: 9i LO 2-1
M I SC . C = 0 1 0 1 78 1 €HS/HL
TIME : 1149
DATE 12 '10 '06
OPERATOR : JGZ
RUN TIME 30.00 MINUTES
DELAY TIME 0.00
CHAN : 0
PR RET PEAK AREA B PEAL
NO. TIME AREA ’• L HT .
*, 1.70 204 140 8.58 6 2 1 1 953
6 3 05 2010900 84 594 3 ®430t>
39 22.05 162080 6 SIS 1 S70O
TOTAL AREA* 2377120
THRESHOLD* 1
MIN PK. WIDTH* 15
AREA REJECT* 2300
ORIGINAL PAGE :S
OF POOR QUALITY
CHART 6B
*:* REAL TIME CHROMATOGRAM 4*4
L \
FI HAL FULL SCALE MV = 1 000 00
VERTICAL SCALE FACTOR : 1 X
I
I
i
SAMPLE 1 91 LD 2-2
MI SC C = O. 10137 €HS/HL
SAMPLE^ &j ld 2-2 ^ ...
M I SC C= 0 . 1 0 1 3 . 6 HS/HL
T I ME IE 17
DATE: 12 -' 10/83
OPERATOR : JGZ
pi IH T I ME : 30 .00 MI NUT ES
DELAY TIME 0 00
CHAN : 0
PK PET PEAK AREA Es REAL
HO TIME AREA >. L KT .
TIME: 1 C 17
DATE 1 £ / 1 0 ■' 8 3
OPERATOR : JGZ
PUH TIME: 30.00 MINUTES
DELAY TIME: 0 00
CHAN : 0
PK RET PEAK AREA 8
NO TIME AREA *• L
2
. 38
4
1 .43
5
1 70
2 93
3 45
8
5 ' 55
9
3 03
1 0
3 58
18
11.75
25
IS 45
34
21 . 98
35
22 15
1 S 3 4
1354
135890
1 1 92800
41333
5352
9425
9398
10301
1194
104430
1 97270
. 095 3
39.335 3
2.415 4
.342 4
551 4
.549 4
.319 1
. 070 2
3 . 103 2
143
207
10131
72100
585
354
249
139
547
3 9
10015
9916
5 1.70 135890 8.129 2
3 2.93 1 192300 71.350 3
7 3.95 41333 2 472 4
34 21 Aft 104430 3.249 2
35 22.15 197270 11.800 3
TOTAL AREA= 1371753
THRESHOLD' 1
MIN P» WIDTH' 15 -
AREA REJECT' 11000
TOTAL AREA' 1711710
THRESHOLD' 1
MIN PL. WIDTH' 15
AREA REJECT' 1000
real:
HT
10131
72100
585
10015
9913
ORIGINAL PAGE IS
OF. POOR QUALITY
CHART 6C
*.*t REAL TIME CHROMAT C'GRAM ***
u
FINAL FULL SCALE MU *1600.66
:.nhr L £ *1 LD 2-3
M I SC . C = 6 . 161 26 L
T I HE 16 = 58
DATE 1 2 ' 1 ‘3S 6
OPERATOR = JGZ
RIJN TIME : 36.06 MINUTES
DELRV TIME 6.00
CHAN : 6
PI-
NO
RET
TIME
PEAK
AREA
AREA
• _■
&
L
PEAK
HT .
2
. 63
4204
. 123
-y
435
4
1 . 45
1258
. 037
*2
129
5
1 . 69
81276
2 . 362
2
11465
i>
1 83
1 96320
5 . 753
2
11447
7
3 26
289976©
64 . 980
3
65372
e
5 60
2293
067
4
251
Cl
6 63
1464
043
4
69
IS
1 1 . 83
6140
. 180
3
248
35
22 03
54263
1 . 590
2
9873
40
22 15
1 65306
4 . 844
3
9887
TOTAL AREA* 3412211
THRESHOLD* 1
MIN FK. WIDTH* 13
AREA REJECT* 1000
VERTICAL SCALE FACTOR IX
i
i
SAMPLE = 91 LD 2-3
MI SC. C=0 10126 €HS/ML
T IME ; 16 58
DATE 12 10 '86
OPERATOR = JGZ
RUN T I ME : 30.60 MINUTES
DELAY TIME 6.6©
CHAN ©
PK
NO
RET
TIME
PERK
AREA
AREA
7.
E:
L
PEAK
HT .
5
1 €6
81270
2 39 3
w
11465
6
1 . 63
196320
5 .’ 779
2
11447
7
3.28
2899700
85.364
*
65372
39
22 . 03
54263
1 . 597
9873
40
22. 15
1 65300
4 . 666
9867
TOTAL AREA* 3396853
THRESHOLD* 1
MIN. PK WIDTH* 15
AREA REJECT* 6266
ORIGINAL PAGE IS
OR POOR QUALITY
CHART 7A
CHART 7 B
ORIGINAL PAGE IS
CHART 7 C
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CHART 9A
V A FILE A: PHEND39. HDR TAKEN 09-05-1986 16:56:50
AREIA PERCENT
REPORT *•»(-******
****************************************************************************
__ . . _ _ * _ . __ n— -4 + nr Tni t 1 al C! .7 fn 7 *
Operator Initials: JGZ
DATA FILE: A: PHEN039 . PTS
Channel#: 0 Vial#: N.A.
«■ Sample Name: 91LD,2-1 ,C-6. 85
* nate: 09-05-19B6 16:56:50 Method: PHENOLIC
f nterface: 4 Cycle#: 39
<■ starting Peak Width: 10 Threshold: .01
* Instrument Type: BECKMAN HPLC Column Type: MICR0B0NDAPAK
* Solvent Description: THF/WATER, 2:1 BY WEIGHT
* Operating Conditions: R.T., FL0WRATE=1.5 ML/MIN
* Detector 0: 220NM/.5AU Detector 1:
* Mi sc. Information: LENGTH=25
<-**-**-
Starting Delay: 0.00 Ending Retention Time: 10
Mo.
Ret
Time
Peak
Area
Area
•/.
B
L
Peak
Ht.
Normalized Area/
y. Height
4
1.7B
2.05
120482
39804
75. 1672
24.8328
2
2
5050
4045
100.000 23.9
33 . 037 9 . 8
Tt al Area:
160286
Area Reject:
1000 One sample per
1 . 000 sec .
>
X
CM
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CHART 9B
FILE A: PHENQ3B. HDR TAKEN 09-05- 19B6 16:40:05
AREA PERCENT
report
+(--**r-Kr-*--**--**--**r-**r
f* ***********************
«■ „ample Name: 91 LD , 2— 2 , C=6. 77
*****
Operator Initials: JGZ *
DATA FILE: A: PHEN038 . PTS *
Channel#: 0 Vial#: N.A. *
*
Date: 09-05-1986 16:40:05 Method: PHENOLIC
<■ nter-face: 4 Cycle#: 08
J tarting Peak Width: 10 Threshold: .01
. Instrument Types BECKMAN HPLC AT1= £ o1 C ^
* Solvent Description: THF/WATER, 2:1 BY WEIGH
» Operating Conditions: R.T., FL0WRATE=1.5 ML/M1N
«. Detector 0: 220NM/.5AU Detector It
* Mi sc. In-formation: LENGTH=25
* -i **********************
Starting Delay: 0.00
*
*
*
****
PI
No.
Ret'
T i me
Peak
Area
Area B
7. L
Peak
Ht.
Normalized Area/
y m Height
1 . 7B
121012
74.9964 2
5109
100.000
23.7
4
2.05
40345
25.0036 2
4092
33.340
9.9
w.al
Area:
161357
Area Reject:
1 000 One
sample per
1 . 000 sec .
DATA FILE-PHEN03B FROM 0. 00 MIN. TO 10.00 MIN. LOW SCALE- 3.320 Mv. HIGH SCALE- 10.656 Mv
91 LD, 2—2, C-6. 77 MG/ML. 0/5/06. JGZ
SO *2
BL'l
ORIGINAL PAGE IS
OF POOR QUALITY
CHART 9C
r r . tl aTpJenSaO.FTS at line 4620
, , F^E a“hEN037.HDR TAKEN 09-05-19B4 14.04:07
„„ fercemt report
. -tt- -x- -*f- -*tr -*<- -**- AREA f- ^
************************************** Operator Initials: JGZ *
c imple Name: 9 1 LD , 2-3 , C-6. 7 c-urwni ic DATA FILE: A: PHEN037 . F'TS *
I ite: 09-05-1986 16:04:07 Met h od : PHENOL I C D ^ nn . 1#| 0 vial#: N.A. *
charting Peak Width: 10 Threshold: ###### *****************************
*: ,..*.*........*...***♦*********** Co , u „ n Type . M1CR0B0NDAPAK C-1B *
inetrument Type: BECKMAN HPLC 2:1 BY WEIGHT
[ns tr U eent THE/WATER 2= l -V WEIGHT
Operating Conditions: R.T., BLOWRA -- £
Detector 0: 220 NM/.jAU
Mi sc. Information: LENGTH=25 „ a^^*.**.*
,t -ting Delay:
0.00
'k Ret
jo Time
Peak
Area
Area B
7. L
Peak
Ht.
2 1.78
2.05
121706
40052
75.2396 2
24.7604 2
5098
4076
Total Area:
161758
Area Reject:
Ending Retention Time: 10.00
Normalized Area/
y m Height
100.000
32.909
23.9
9 . B
1000 One sample per 1.000 sec,
ORIGIN Ai PA'OE TS
OF POOR QUALITY
I
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GPC CALIBRATION PLOT
*** Calibration Data ***
Calibration Name:
Mi sc Information:
Fit Type: 3
Log Mol Wt * A
A* 2.533977
Coefficient of
Ret Time
+ Bx ♦ Cx~2 +
B* 2.115315
Determi nation
Molecular
Vx^3
C* -.5646324
0.9902
Weight
D= 3. 606432E-02
Log Mol Wt
3.50
4.33
4.83
5. 09
6 . 00
7. 17
7.50
35000
15000
3600
2350
570
92
72
4.544
4. 176
3.556
3.371
2.756
1.964
1.857
ORIGINAL PAGE IS
OF POOR QUALITY
CHART 10A
A FILE B: GPC28 . HDR TAKEN 08-05-1986 17:13:56
GPC REPORT *+ **.++**■■*■■*■ ■*-•*■
*****************************************************************************
Sample Name: 91LD 2-1 =2.68 ^FTS *
Dale: 08-05-1986 14:05:42 Method: DATA FILE: B.GFC^B .F S
Inter-face: 5 Cycle#: 28 Channel#: 0 Vial#: N.A. *
Starting Peak Width: 60 Threshold: » *************************
* Instrument Type: HPLC/ BECKMAN Column Type: ULTR AST YF: ABEL 500A *
* Solvent Description: THF
* Operating Conditions: T=35C FLDWRATE=2. OML/MIN
* Detector Os
* Misc. Information:
*********************
Starting Delay: 0.00
C libration -file: GF'CF'HEN
Molecular Weight Distribution Averages
Detector Is
CAL I BRAT ION/ GPC
t ****** ***********
Endinq Retention Time: 10.00
Baseline TIMES:
F' Dcess .JIMES:
T tal Area:
Mw=
M- =
M /Mn =
Mz =
3.85 to
3.85 to
196902
1718
370
4.6439
4134
1501
10.00
10 . 00
MW:
MW:
2229J
2229S
to
to
ORIGINAL PAG F, IS
OK POOR QUALITY
CHART 10B
>*■' 3 FILE B: GPC22 . HDR TAKEN 08— 05-1986 17:1 8:^7
GPC
(■
□ample Name: 91LD 2—2 C=2.£>8
Date: 08-05-1986 11:58:33 Method:
nterface: 5 Cycle#: ^2
tarHnn Peak Width: 60 Threshold:
Operator Initials: GBF
DATA FILE: B:GPC22 .PTS
Channel#: 0 Vial#: N.A.
Column Type:
*
*
*
*
*******
00 A *
*
*
Instrument Type: HPLC/BECKMAN
Solvent Description: THF
Operating Conditions: T=35C FL0WRATE=2. OML/MIN
Detector 0: 254NM/.1AU Detector #
Mi sc. Information: CAL I BRAT I ON/GPC ## ************************
Ending Retention Time: lu.uu
1 :
M*
Starting Delay:
2s ibration file
•1c ecular Weight
Baseline TIMES:
- , r r> CE55 TIMES:
Tc al Area:
Mw-
Mn=
Mi" Mn=
Mi -
0 . 00
: GPCPHEN
Di str i but i on
3.85 to
3.85 to
240471
1801
368
4.8945
4352
1573
Averages
10 . 00
10 . 00
MW:
MW:
22295
22295
to
to
2
r>
CHART IOC
GPC REPORT -**--*- -*e-*e*e-**-*e-*e
*■
*
*
*
*
*
*
*
*
*
*
*
HMMH
Sample Name: 91LD 2—3 C=2.68
Date: 0B-05-19B6 11:28:37 Method:GPC
Inter-face: 5 Cycle#: 20
Starting Peal Width: 60 Threshold:
. *********************************** -1
Instrument Type: HPLC/BECkMAN
Solvent Description: THF
Oper ati nq Conditions: T = j5C FLDWRATE-
~ Detector 0: 254NM/.1AU
Mi sc. Information: CAL I BRAT I DN/GPC
t *********************'* ***** 1
*********■***♦-***
Operator Initials: GBF *
DATA FILE: A:GPC20.PTS *
Channel#: 0 Vial#: N.A. *
.01
r **********
Column Type: ULTRASTYRAGEL 500A *
*
2. OML/MIN
Detector 1:
*
*
Starting Delay: 0.00
Calibration -file: GPCPHEN
M lecular Weight Distribution Averages
B-seline TIMES:
Process TIMES:
T tal Area:
M =
Mn=
M-/Mn=
M =
Mv-=
>.85 to
3.85 to
271362
1598
260
6. 1449
3922
1389
10.00
10 . 00
MW:
MW:
h*************
Ending Retention Time: 10.00
22295 to
22295 to
; per i n,fc*nt No
;f!heometric£ RECAP JLI
. s 12 -Sax&ple Nd. 1
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FI NGERPRINT VIBCOSITI PROFILE 91LD RESIN NASA L0T2-1
ot tftor x CP - — - rr*_— - -
at** and JTime x Tuesday, Augu*M:--4^P s -1906 — “13:4^:46
jerating Mode : DYNAMIC
*n T/pe s CURE
^ometry : DISK ?< PLATE
RAD I UE : 25.00
GAP : 0.50
3-1 :-s :
v f\r-lIN =r50V.
RE3UENCY =10RAD/SEC
ORIGIN AE PAGE TS
OF POOR QUALITY
}3A FINGERPRINT VISCDSITI I^ROFILE^VJLD RESIN JslASA -LDT2-1
-• -
• — ■
—
rTAjc CT i
FTA"
JTOKQUE
-IIME
TEMP -
- X. J V-?. —
- POISE r^POISE
7 . 552e+000 7. 303e-*-000
■ .-POISE v—
-L. 925e+QOO
GRAMS -CM . ;
9 . 4B3e— 001
: rr MIN. -
S.OOOe+OOl-
-DEE. C
1 . 2-40e-*-00
ORIGINAL PAGE IS
OF POOR QUALITY
2 —
CHART 1MB
I I I K I I 1
xperi ment No. : 13 Sample No. s 1
i l e:
ASA FINGERPRINT VISCOSITY PROFILE -91LD -RES IN -NASA L0T2-2
■f tor t CR _ _ ~1.~ -
ate and Time : - T uesday August 1 9 ,1 986” -^¥4 : 59s OB - -
p< -at i ng Tlode s DYNAMIC ~ 7 ‘ " ~ ""
Type r CURE - -- ' • 1 : — . - -
eometry : DISK & PLATE _
RADIUS : 25.00
GAP : 0.50
o‘ ?5 :
~i UN =507.
REOUENCY =!ORAD/SEC
ORIGINAL PAGE IS
OF POOR QUALITY
iS . FINGERPRINT VISCOSITY-PROFILE -*?1LD-R£SIN NASA LOT2-2
ETA* X
ED I BE
-L.243e+002 _3
1.124e+C>02 1
1 . 050e+002 «
9.511e+001 — 1
8 . 337e+00 1 .... '
7. 3i9e+O01 ^-4
^.374e+001 -4
El. BB6e+D01 ~
- - 5 . - 277 »+ 001 ~ -1
4.B47e+O01
4.413e+001
4 . C>70e+001
3 . 753e+00 1
3 . 4B9e+001
3.2296+001
2. 959e+001
2.796e+001
2. 69 ie+OOl
2.517e+001
2.4136+001*
2.235e+001
2. OB5e+001
- -1 . 926e+003 -
1 . 769e+001
1 . 60 i 6+00 1
1 .447e+001
1.317e+001
1 . 150e+001
1 . 019e+001
9. 266e+O00
8 . 599e+000
: 9 . 007e+000
; E.291e+00O
, 5. 992e+000
; 3.1 43e+000
, 3.942e+000
r 4.2816+000
l “4 . '9156+000
? 4 . 494e+000
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1 3.2926+000
2 2 . B 1 O e+000
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5 3. 037 e+000.
6 3 .42 1 e+000
7 3.175e+000
£ 3.242e+000
9 4 . 047e+000
O 5.702e+000
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_1 . 142e+002_.
1 . 044e+002 r -_-
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3.7B4e+OOi-
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1 1.4436+001
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1 1.21 8e+00 1
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4.9 1 6e+00 1
-A. 1766+001
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~T. 563 e+ 0 WT
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~ TIME -
— -MIN. .
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3 . 989e+000 1 . 443e+000
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2. 773e+000
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3.214e+000
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1 . 1636+000 2. 900e+001
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2. 7C»0e+001 B. OOOe+OOl
2 ! BOOe+OOl 6 . 200e+001
1. 130e+000
1 . 040e+000
1. 361 e+000 . 7.»517e— 001
7.494e-001 3.946e-001
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3. 200e+001
3.300e+001
3, 400e+001
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9. 200e+00I
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B. 3Ele-001 4. 946e— 001
1.1526+000 5 . 37 4e -OOl
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6.690e-001 5.640e-001
7 . 30Be— 00 1 4.7B0e-001
2."622e-001 —4 .131 6-<’01
4.544e-O01 2.524e-001
3.422b— 001 3. 120e— OOl
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_ 1 . 230 e +002
1.126e+00C» 7. 15Qe— OOl -4.900e+001
ORIGINAL PAGE IS
OF POOR QUALITY
Nnafi FI NGERPR TNT SCQS I T Y *PRDFI 1 .E ^lLD^RESXN^AS A AQT 2 - 2 ^^
ETA* ETA'' ETA" TOROUE
POISE POISE POISE GRAMS CM
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TIME TEMP
MIN. DEG. C
. G Due +00-1 .1 . r? 50£+00-2
ORIGINAL PAGE IS
OE POOR QUALITY
O
NASA FINGERPRINT VISCOSITY
CHART 1AC
(V)
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asiod
*V13
Rheometr i cs RECAP II
>; per i men t No. : 14 Sample -No. : 1
iA^A FINGERPRINT VISCOSITY PROFILE 9 1 LD RESIN NASA LOT2-3
i^r-aior : CRISTINA P
ate and Time : Tuesday, August 19, 1986 — 16:16:38
ipv -ating Mode : DYNAMIC
.w- ?p Type : CURE . _ — -
■eometry : BISK & PLATE
RADIUS «r..4 25.00 -• — — -**“• - ' ----- — -----
GAP i 0.50 —
origtnat: page is
OF POOR -QUALITY
ORIGINAL PAGE IS _____
OF, POOR^ QUALITY -
h BA FINGERPRINT V I SCD5IT V T^RUFILE"? lrbfRESI AS A
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268e+002
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1.266e+00:
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4.992e+001
4.-5216+001
1 . 196e+002-- 4.216e+001
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3.397e+001
- 3. 296e+00l_
3. 128e+66l
2. 9B2e+OC>l
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1 . 696e+001
1.68Be+001
1.591 b+ 001
1 « 446e+001
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3 _ 422e+0.01 2. B67e+001=j
2-964e+00i _2. 7356+001
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6. 926e+000
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-4. 1 656+000
3.7186+000
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1. 901e+001
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1 . 7266+001
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i.»_200e+001
_1.300e+00_l_
1. ‘4006+001
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3.26Be+000 l,7OGe+0Ol
1 . 829e+001 1 . 254e+001
1.7786+001 T .0616+001
1 . 656e+001
1 . 597e+001
1 . 449e+001
1. 367e+001
1.2266+001
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8. 917e+000
7.383e+000
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5.297e+000
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X
\|C A FINGERPRINT VISCOSITY PROFILE 91LO RESIN -NASA -LOT2-3 -
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TABLE OF CONTENTS
FABRIC TESTING
NASB-36298
TEST
la.
lb.
U. S. Polymeric
SWB-8 Fabric lor
Breaking Strength, WARP
Breaking Strength, FILL
0. E.
NASA
ft ft ft • 1
7iiae
Lot# 2
PAGE
. 1
1
2a.
2
2b.
2
2c.
2
3.
Visual Inspection.
2
4.
Speciiic uraviiy . .....*•*
_ u
3
5 •
•rr a
3
6.
3
7a.
Atomic Absorption
4
7b.
Moisture Content. ..••••>•
4
7c.
8b.
Filament diameter, WARP. -
a a ft a
4
fib.
Filament diameter, FILL. .
a a • a
4
5
9a.
Thread Count, wak“
t a a •
9b.
Thread Count, r ill. • • • • •
» a a •
5
10a.
Areal weight.
4 4 4 _ X ^ 1 sa. _ _ _
a • a a
10b.
10c.
Weight Change on Acetone
Wash. . . *
6
CHARTS
- 3M
Visual Inspection
TGA
3A
6A
6M
Page 1 of 6
U3p
USRJymeric
FABRIC TESTING
NAS8-36298
U. S. POLYMERIC O. E. 71108
2a. Carbon Assay,
MDQAI 5S60
PICK
CENTER
PLAIN
AVG.
:±ng Strength, lbo/in, WARP
#2-1
1 D1682
PICK
61
CENTER
55
PLAIN
25 .
AVG.
63. 7
#2-4
#2-5
#2-6
#2-7
PICK
16
27
63
48
CENTER
69
84
65
87
PLAIN
76
77
&6
88
AVG.
53. 7
62. 7
64. 7
74. 3
#2-10
#2-11
#2-12
#2-13
PICK
24
59
71
38
CENTER
71
92
103
64
PLAIN
23
43
82
28
AVG.
39. 3
64. 7
as. 3
43. 3
cing Strength, lba/inch, FILL
#2-1
1 D1682
PICK
72
CENTER
83
PLAIN
67
AVG.
74. 0
#2-4
#2-5
#2-6
#2-7
PICK
92
28
71
102
CENTER
71
77
39
48
PLAIN
61
47
70
- 22 .
AVG.
74. 7
50. 7
60.0
59. 0
#2-10
#2-11
*2-12
#2-13
PICK
73
63
30
55
CENTER
20
83
58
51
PLAIN
£8
85
&8
45
AVG.
50. 3
83. 7
58. 7
50. 3
* 2-1
99. 2
99. 6
99. 0
99. 27
PICK
CENTER
PLAIN
AVG.
*2-4
99. 1
99. 8
99. 9
99. 60
#2-5
99. 2
99. 7
99. 0
99. 30
# 2-6
99. 9
99. 6
99. 9
99. 80
#2-7
99. 7
99. 8
99. 4
99. 63
HITCO MATERIALS DIVISION
L 700 E. DYER ROAD, SANTA ANA, CALIFORNIA 92707 • (714) 549-1101 • TWX (910) 595-1130 • FAX
#2-2
#2-3
42
92
44
98
60
27
48. 7
72. 3
#2-8
#2-9
25
12
14
41
48
73
29. 0
42
LOT2
AVG
44. 5
68. 2
58. 9
57. 2
#2-2
#2-3
59
77
66
63
63
73
63. 3
71. 0
#2-8
#2-9
25
53
22
46
55
22. 0
51. 3
LPT2 AVG
63. 1
55. 9
58. 5
59. 2
#2-2
#2-3
99. 6
99. 8
99. 8
99. 6
98. 9
99. 9
99. 43
99. 77
#2-8
#2-9
99. 7
99. 7
99. 7
99. 8
99. 9
99. 9
99. 77
99. 80
# (714) 549-2858-5-2437
Page 2 of 6
2a. Carbon Assay,
HDQAI 5560
PICK
CENTER
PLAIN
AVG.
2b. Hydrogen Assay, X
MDQAI 5560
CMR-fl Fabric for Lot» 2
X (CONTINUED)
#2-10
#2-11
#2-12
99. 9
99. 9
99. 4
99. 6
99. 5
99. 6
99. 2
99. 4
£9. 6
99. 57
99. 60
99.60
LPT2 AVG
99. 62
99.71
99. 53
99. 62
PICK
CENTER
PLAIN
AVG.
#2-1
#2-2
#2-3
. 03
. 02
.01
.03
.01
.01
. 02
. 02
t 01
.027
. 017
. 010
PICK
CENTER
PLAIN
AVG.
#2-4
#2-5
#2-6
a 02
.01
.02
a 01
<.01
.02
01
<.01
. 01
. 013
EST . ©04
.017
PICK
CENTER
PLAIN
AVG. EST . 004 EST
# 2-10
<.01
<. 01
. 01
# 2-11
.01
<. 01
<. 01
©01 EST .001 EST .001
#2-13
<.01
<.01
<. 01
2c. Nitrogen Assay,
HDQAI 5560
004 EST .007 EST .©01
PICK
CENTER
PLAIN
AVG.
LPT2 AVG
. 010
. 007
. 007
. 006
PICK
CENTER
PLAIN
AVG.
PICK
CENTER
PLAIN
AVG.
#2-1
#2-2
#2-3
.22
. 19
. 11
.21
. 23
.09
.09
. 17
.09
. 17
. 16
. 12
#2-7
#2-6
#2-9
. 1
. 1
. 04
.06
#2-13
. 1
. 1
. 02
.073
.2
.2
. 1
. 167
. 3
. 2
±J-
. 2
LPT2 AVG
. 14
. 14
. 10
. 127
3. Visual Inspection
QCi-102
4. Specific Gravity, Units
PTM-64
See Charts 3A-3H
PICK
CENTER
PLAIN
AVG.
# 2-1
1.7376
1.7742
1. 9094
1 . A07
7. 041
Page 3 of 6
^WB-fl Fabric for NAS A Lot* — 2
Unite (CONTINUED)
4. Specific Gravity,
PTH-84
PICK
CENTER
PLAIN
AVG.
PICK
CENTER
PLAIN
AVG.
5. pH, UnitB
CTH-24B
AVG.
AVG.
6. TGA, -C at 50X
CTH-51 (AIR)
Na
K
Ca
Mg
Li
AVG.
• 2-4
#2-5
2. 1453
2. 1458
2. 1874
2. 7238
2. 1789
2. 2718
2. 171
2. 38®
#2-1®
#2-11
1. 6823
1.7784
1 . 8®32
1.7732
1.7129
1.7895
1.733
1.780
#2-4
#2-5
8. 0
6.2
8. 3
6. 15
6. 2
6. 2
#2-1®
#2-11
6. 2
6. 6
6. 2
8. 2
6. 5
6. 55
Weight Loss
#2-4
#2-5
3
5
2
2
25
16
0
1
e
0
30
24
#2-6
#2-7
2. 2223
2. 0307
2. 1354
2. 0625
2. 1337
2. 1014
2. 164
2.065
#2-12
#2-13
1 . 5362
1.6062
1. 6435
1.7198
1.7164
1.7572
1.632
1.694
#2-1
6. 6
6.3
AVG.
6.45
#2-6
#2-7
6.4
6. 0
6.®
6.4
6. 0
#2-12
#2-13
6.®
6.8
6 .®
6.9
6.0
6.85
SET UP#
1
#2-2
939
#2-4
926
#2-5
934
#2-7
913
#2-9
879
#2-11
876
#2-13
905
AVG.
910
See Chart 6A-6M
#2-1
Na
3
K
1
Ca
31
Mg
0
Li
0
AVG.
35
#2-6
#2-7
6
4
1
1
13
15
1
0
0
0
21
20
#2-8
#2-9
2. 1896
1. 7857
2. 1918
1. 8273
2. 1909
1.7342
2. 191
1.782
LOT2 AVG
1.9146
1.9969
1. 9689
1.960
#2-2
#2-3
4. 2
6. 1
4. 2
6. 2
4. 2
6. 15
#2-8
#2-9
6.4
6.9
6.4
7.0
6. 4
6.95
LOT2 AVG
6. 18
6. 2®
6. 19
SET UP#
2
#2-1
867
#2-3
881
#2-6
834
#2-8
825
#2-1®
833
#2-12
782
AVG.
"837
#2-2
#2-3
4
6
1
1
32
16
0
1
0
0
37
24
#2-8
#2-9
9
11
1
1
77
101
1
1
0
0
88
114
7a. Atomic Absorption, ppm
CTM-53B
Page 4 of 6
SWB-fl Fabric for NASA L ot# 2
7a. Atomic Absorption, ppm (CONTINUED)
CTM-53B
* 2-10 * 2-11
Na 7 6
K 1 1
Ca £2 54
Mg 0 ©
Li _0 _©.
AVG. 70 £1
7b. Moisture Content, X
CTM-53B
7c. Ash Content,
CTM-53B
8a. Filament diameter, microns, WARP
S. E. M. procedure
(diameters are an average of
10 measurements)
*2-4
#2-5
AVERAGE
9. 58
10. 03
Minimum
7. 95
8. 75
Maximum
11. 25
12.45
Std. Dev
1. 15
1. 21
*2-10
*2-11
AVERAGE
9. as
9. 55
Minimum
7. 75
8. 55
Maximum
12. 00
10. 55
Std. Dev
1. 28
0. ££
8b. Filament diameter, microns, FILL
S. E. M. procedure
(diameters are an average of
10 measurements)
#2-12
#2-13
LOT2 AVG
4
4
5. 5
1
1
1.2
29
30
38. 5
0
1
0. 5
0
0
0. 0
34
36
45. 7
#2-1
.020
#2-8
. 000
#2-2
.025
#2-9
. 010
#2-3
.020
#2-10
. 015
#2-4
.015
#2-11
.010
#2-5
. 005
#2-12
.005
#2-fi
.015
#2-13
. 005
#2-7
. 005
Lo-t# 2
AVERAGE
. 011
#2-1
.020
#2-8
. 080
#2-2
.035
#2-9
. 059
#2-3
.020
#2-10
. 070
#2-4
. 020
#2-11
. 055
#2-5
.010
#2-12
.005
#2-£
.035
#2-13
. 029
#2-7
. 030
Lot# 2
AVERAGE
. 036
#2-*
#2-2
#2-3
AVERAGE
9. 12
9. 60
9. £4
Minimum
8. 25
8. 00
8. 95
Maximum
9.75
10. 90
10. 30
Std. Dev 0. 52
0. 94
0. 43
#2-£
#2-7
#2-8
#2-9
9. 36
9. £5
9. 28
9. 74
8. 00
8.05
8. 00
8. 35
10.60
11. 50
11. 00
10. 45
0. 89
0. 97
0. 90
0. 56
#2-12
*2-13
LOT2 AVG
9. 18
10. 11
9. 59
8. 10
8. 25
7.75
10. 05
12. 05
12. 45
0. £4
1. 25
0. 92
* 2-1
AVERAGE 10. 00
Minimum 9. 00
Maximum 13. 50
Std. Dev 1. 34
Page 5 of 6
9a.
9b.
10a
swb-6
Fabric
for NASA Lot# 2
Thread Count,
per inch.
WARP
#2-1
#2-2
#2-3
PTM-5A
41
44
40
41
43
40
40
45
40
41
44
41
41
44
40
AVG.
40 . a
44
40. 2
#2-4
#2-5
#2-6
#2-7
#2-8
#2-9
44
43
40
39
36
40
44
43
40
38
36
40
43
42
40
39
36
41
43
43
40
39
36
41
AVG.
44
43. 6
42
42. 6
40
40
38
36. 6
35
35. 8
41
40. 6
#2-10
#2-11
#2-12
#2-13
L0T2 AVG
35
40
42
35
39. 9
35
39
42
34
39. 6
36
39
41
35
39. a
35
39
41
34
39. a
35
40
40
34
39. 5
AVG.
35. 2
39. 4
41. 2
34. 4
39. 7
Thread Count,
per Inch,
, FILL
#2-1
#2-2
#2-3
PTK-5A
36
38
35
36
38
36
38
38
35
38
38
36
36
38
36
AVG.
38. 0
38. 0
35. 6
#2-4
#2-5
#2-6
#2-7
#2-8
#2-9
36
39
38
39
37
37
36
36
38
39
39
37
39
36
37
39
39
38
39
36
37
39
38
37
29
26
27
38
40
38
AVG.
36. 6
38. 2
37. 4
38. 6
38. 6
37. 4
#2-10
#2-11
#2-12
#2-13
L0T2 AVG
39
41
39
39
38. 2
36
41
39
39
38. 3
39
41
39
38
38. 3
36
42
39
39
38. 3
38
1L
29
39
38. 4
AVG.
38. 4
41. 2
39. 0
38. 8
38. 3
. Areal Weight
as received, gm/4x4
#2-1
#2-2
#2-3
PTM-3A
LEFT
3. 416
3. 516
3. 214
CENTER
3. 234
3. 510
3. 196
RIGHT
3. 327
3. 722
3. 375
AVG.
3. 326
3. 583
3. 262
Page & of 6
SWB-B Fabric for NASA Lot# .2.
10a. Areal Weight as received, gm/4x4
PTM-3A
LEFT
CENTER
RIGHT
AVG.
#2-4
3. 607
3. 533
3. 636
3. 592
#2-5
3. 640
3. 569
3. 762
3. 657
#2-6
3. 464
3. 366
3. 377
3. 402
#2-7
3.606
3. 566
3.710
3.694
#2-6
3. 246
2.970
3. 079
3. 096
#2-9
3. 145
2.933
3. 284
3. 121
LEFT
CENTER
RIGHT
AVG.
#2-10
3. 275
3. 159
3. 015
3. 150
#2-11
3. 562
3.263
3. 477
3.434
#2-12
3.567
2.759
3.379
3.242
#2-13
3.056
3. 149
2.648
3. 016
LOT2 AVG
3. 426
3. 247
3. 384
3. 352
10b.
Volatiles as
PTH-3A
received.
X
AVG.
#2-1
. 50
.43
. 30
.41
#2-2
.46
. 40
. 36
. 41
#2-3
. 59
. 47
.47
. 51
AVG.
#2-4
. 56
. 34
. 36
. 43
#2-5
.49
. 45
. 37
. 44
#2-6
.52
.33
. 30
. 38
#2-7
.47
.34
. 36
. 40
#2-8
.62
.40
. 39
. 47
#2-9
. 13
. 46
. 55
. 36
AVG.
#2-10
.24
. 44
. 60
.43
#2-11
.25
. 40
.46
. 37
#2-12
.33
.47
. 53
.45
#2-13
.36
.44
. 49
.43
LOT2
.43
.41
.43
.42
AVG
10c.
Weight change on Acetone vash,
PTM-3A
X
LEFT
CENTER
RIGHT
AVG.
#2-1
.06
-. 16
-.09
#2-2
. 11
.03
-. 05
.03
#2-3
. 13
-. 16
-. 15
-. 06
LEFT
CENTER
#2-4
.00
-. 17
-. 11
-.09
#2-5
. 03
-. 11
rr jfe
-.06
#2-6
-.03
-. 18
-fga
-. 10
#2-7
.00
-. 14
-. 11
#2-8
. 00
-.20
-. 13
#2-9
-. 51
-.21
-.06
RIGHT
AVG.
-.08
-. 11
-.26
LEFT
CENTER
RIGHT
AVG.
#2-10
-. 15
-. 13
. 00
-.09
#2-11
-. 11
-. 16
-. 14
-. 15
#2-12
-.22
-.25
-. 15
-.21
#2-13
-. 30
-.26
-.07
-.21
L0T2
-.08
-. 16
l-.LL
-. 12
AVG
U.S. Polymeric
. jl ' U.
(0
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Quality
. Quraishi, Manager
Assurance Department
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CHART 6D
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CHART 6F
CHART 6G
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original page rs
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CHART 61
ORIGINAL PAGE IS
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CHART 6J
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CHART NO 066-7300
CHART NO Q5K 7JQO
TABLE OF CONTENTS
PREPREG TESTING
NAS8-36298
U. S. Polymeric O.E. 71108
FM 5834 NASA LOT# 2 U.S.P. LOT* D09275
TEST
PAGE
1b. Resin Content, Soxhlet. . .
lb. Filler Content, Soxhlet. .
lc. Cloth Content, Soxhlet. . .
2. Volatile Content
3 .
4. Resin Content, Dry Basis.
5. Tack
6. Gel Time
7a. Atomic Absorption
7b. Moisture Content
7c. Ash Content
8. TGA
9. DSC
10. Infrared (IRZB) Baseline.
11. Environmental History....
12. Specific Gravity
13a. Tensile Strength
13b. Tensile Modulus
13c. Tensile Elongation
14a. Flexural Strength
14b. Flexural Modulus
15a. Compressive Strength. . . .
15b. Compressive Modulus
16. Double Shear Strength. . .
17. Barcol Hardness
18. Residual Volatiles
19. Resin Content, Pyrolysis
20. Acetone Extraction
21a. CTE, with ply
21b. CTE, crossply
1
1
1
1
1
2
2
2
2
2
3
3
3
3
3
3
4
4
4
4
5
5
5
5
5
8
6
6
6
6
TGA
DSC
Infrared (IRZB) Baseline.
CTE
8A - 6G
9A - 9G
10A - 10G
21 A - 21G
CHARTS
Page 1 of 6
u$p
USFbfymeric ®
FH 5834
PREPREG TESTING
NAS8-36298
U. S. POLYMERIC O. E. 71108
NASA LOT* 2 U. S. P. LOT» D09275
Resin Content,
CTM-6D
Soxhlet,
X
ROLLfl
ROLL# 2
ROLL# 3
START
START
START
37. 5
36. 0
35. 1
39. 6
36. 3
35.4
37. 1
35. 2
35. 2
AVG. 38. 1
35. 8
35. 2
lb. Filler Content, Soxhlet, X
CTM-6D
15. 6
15. 0
14. 6
16. 5
15. 1
14.7
*5.4
Hi-5
14.7
15. 8
14.9
14.7
ROLL# 4
ROLL# 5
R0LL#6
R0LL#7
START
START
START
START
36. 3
37. 9
38. 0
37. 2
35. 8
37. 3
37. 4
37. 7
35. 6
39. 3
38. 2
37. 8
35. 9
38. 2
37. 9
37. 6
NASA LOT#
2 AVERAGE
36. 9
15. 1
15. 8
15. 8
15. 5
14.9
15. 5
15. 6
15.7
14.8
16.4
15.9
15. 7
14a 9
15. 9
15. 8
15. 6
NASA LOT#
2 AVERAGE
15. 4
lc. Cloth Content,
CTM-6D
Soxhlet, X
46.9 49.0
43.9 48.6
47. 5 50. 3
AVG. 46.1 49.3
50. 3
49. 9
50. 1
50. 1
48. 6
46. 3
46. 2
47. 3
49. 3
47. 2
47. 0
46. 6
49. 6
44. 3
45. 9
46. 6
49. 2
45. 9
46.4
46. 8
NASA LOT#
2 AVERAGE
47. 7
2 .
Volatile Content, X
PTM-17B
4. 5
5. 4
5. 4
5. 5
5. 1
4. 3
5.7
5. 5
5. 8
5. 4
4. 3
AVG. 4.4
5. 4
5. 5
?L_2-
5.4
5.4
5. 6
5.4
NASA LOT#
5.6
6. 1
5. 5
5. 5
5. 8
5. 5
5. 8
AVERAGE
5. 3
3. Flow, X
PTM-19G
11.0
11.7
12. 9
AVG. 11.9
18.8 13.5
20.3 17.6
19. 8 17.0
19.6 16. 0
18.4 19.1
19.5 20.0
20. 4 18. 0
19.4 19.0
NASA LOT#
17. 2
19.
Cl
17. 9
20.
2
18. 9
19.
_8
18. 0
19.
7
AVERAGE
17.
7
/
HITCO MATERIALS DIVISION
700 E. DYER ROAD, SANTA ANA,
CALIFORNIA 92707 • (714) 549-1101 • TWX (910) 595-1130
FAX # (714) 549-2858-5-2437
Page 2 of 6
FW 5fl34 NASA LOT* 2 U. S. P. LOT# D09275
4. Resin Content, Dry Basie, X
PTM-16F, Type II
ROLLfl
START
38. 3
38. 8
38. 9
AVG. 38.7
R0LL#2
START
38. 7
41. 0
36. 6
38. 8
RDLL#3
START
41. 5
41.6
39. 4
40. 8
ROLL# 4
START
37.7
40. 1
34. 5
37. 4
R0LL#5
START
42. 4
41. 6
41. 3
41. 6
NASA LOT# 2
R0LL#6
START
36. 0
36. 4
39. 4
38. 6
AVERAGE
R0LL#7
START
43. 3
42. 7
41.8
42. 6
39. 8
5. Tack, lbs
PTM-80
60
44
36
40
48
NASA L0T#2
35 42
AVERAGE 44
£. Gel Time, Seconds
PTM-20E
87
66
70
62
73
NASA LOT# 2
65
AVERAGE
63
70
7a. Atomic Absorption, ppm
CTM-53B
Na
RQLL#1
START
8
K
2
Ca
18
wg
2
Li
0
TOTAL
30
Na
R0LL#5
START
6
K
2
Ca
16
Mg
1
Li
0
TOTAL
25
7b. Moisture Content, X
CTM-53B
R0LL#1 R0LL#2 R0LL#3
START START START
3.11 2. B5 3.44
R0LL#2
ROLL# 3
RQLL#4
START
START
START
7
13
6
2
1
1
17
16
15
2
1
1
0
0
0
28
31
23
ROLL# 6
ROLL# 7
LOT# 2
START
START
AVG.
10
5
6
1
1
1
35
58
25
1
2
1
0
0
0
47
66
36
RQLL#4
RQLL#5
RQLL#6
R0LL#7
START
START
START
START
2.97
3. 13
3. 77
2. 83
NASA LOT# 2
AVERAGE
3. 16
Page 3 of 6
FM 5634
LOT* 2 M-«-P- LOT* D092 Z5
7c. Ash Content, X
CTM-53B
R0LL#1 ROLL# 2 R0LL#3
START START START
.04 .04 • ® 3
R0LL#4 R0LL#5 R0LL#6
START START STAR JL
.04 “ .04 *02
NASA LOT# 2 AVERAGE .03
R0LL#7
START
. 04
8. TGA, % Weight Loss at 500* C
CTM-51 (Nitrogen)
7. 1
4.9
7.6
6.4 6.9 7 * 9 6 ’?
NASA LOT# 2 AVERAGE 6.6
See Chart 6A-BG
DSC, • C
CTM-50A
ROLL# 1 ~S
R0LL#2-S
R0LL#3-S
R0LL#4-S
RQLL#5-S
R0LL#6-S
*OLL#7-S_
NASA LOT# 2
FTRST T EMPERATURE.
182
182
182
182
161
183
180
AVERAGE
See Chart 9A-9G
10. Infrared (IRZB) Baseline
CTM-21C
ROLL# 1
START
1. 08
R0LL#2 R0LL#3
START START
1.09 1.09
Environmental History
SF.CQHP TEMPE RATURE
240
243
241
243
241
239
243
241
ROLL# 4 ROLL# 5
START START
1.07 l*® 7
NASA LOT# 2
ROLL#6 R0LL#7
START START
1.05 1.08
AVERAGE 1.08
See Chart 10A-10G
Date manufactureds 28 May 1986
Packaged in: Polyethylene bag
■upported in
cardboard carton
8 July 1986 in
40* F truck
Date shipped :
12. Specific Gravity, Cured,
ASTM D 792
Unite
^ 1.516
1. 513
1. 511
AVG. 1.513
1.513
1. 527
1.526
1.522
1. 500
1.501
1.499
1. 500
. 515
.523
. 522
1. 509
1.509
1. 504
1.496
1. 485
1.493
1.491
A * 520 NASA* LOT# 2 * AVERAGE 1.5® 9
Page 4 of 6
FH 5B34 NASA LOT# 2
13a. Tensile Strength, ksi, WARP
FTMS 406-1011
ROLL#l
ROLL# 2
R0LL#3
START
START
START
22. 67
24. 71
29.95
25. 17
21. 16
30. 46
24. 65
25. 99
25. 90
24. 40
22. 63
27.55
23. 67
23. 47
27. 46
AVG. 24. 15
23. 64
28. 27
Tensile Modulus, msi.
WARP
FTMS 406-1011
4. 59
4. 86
4. 57
5.66
5. 38
5. 18
4.74
4.84
4.99
4. 93
5. 06
4.92
5. 02
4. 60
5. 34
AVG. 4.99
4.99
5. 00
Tensile Elongation, %,
WARP
FTMS
406-1011
. 50
. 62
. 66
_ _
. 53
. 65
. 60
.65
. 58
. 54
. 55
.64
. 54
.58
.60
AVG.
. 55
. 59
. 63
14a. Flexural Strength, ksi, WARP
FTMS 406-1031
33. 69
36. 63
41.72
36. 59
40. 45
AVG. 38. 26
37.60 47.66
36. 59 <3* 56
36.87 45.62
32. 49 45. 90
31. 68 . 44. 35
35.49 45.46
II g.P. LOT# D09275
R0LL#4
R0LL#5
RQLL#6
R0LL#7
START
START
START
START
27. 64
22. 61
29. 66
26. 65
26. 27
22. 37
29. 89
27. 54
25. 46
20. 25
26. 63
24. 87
22. 55
22. 68
31. 79
27. 13
26. 04
21.06
29. 72
25. 13
25. 60
21. 64
29. 98
26. 70
NASA LOT#
2 AVERAGE
25. 74
5. 34
3. 95
6. 17
4.20
5.45
4.43
5.36
4.36
4.91
4. 16
5.45
4. 22
NASA LOT#
.60
. 66
.53
.64
. 54
. 53
.51
.64
.59
. 62
.55
.62
NASA LOT#
5.79
5. 61
5. 48
5. 26
- -
5. 40
6. 15
5. 80
6. 02
5. 38
5. 86
5. 49
AVERAGE
5. 14
. 55
.64
. 60
. 63
— _
. 57
. 53
. 60
. 57
. 55
. 56
. 60
AVERAGE
. 59
37.41 36.21
37.06 33.17
40. 61 37 * 20
39. 15 32. 90
34. 60 37. 91
37.77 35.66
NASA LOT# 2
43.37 39.23
42.09 41.73
44.55 41.66
44.63 42.03
43. 66 41. 59
43. 66 41 . 29
AVERAGE 39. 69
Page 5 of 6
FH 5834 NASA LOT# 2
ii.g.P. LOT* D09275
14 b. Flexural Modulus, msi, WARP
FTMS 406-1031
RQLL#1
ROLL# 2
ROLL# 3
START
START
START
4. 32
4. 28
6. 06
4. 16
4. 60
5. 58
4. 08
4. 72
5. 68
4. 38
3. 82
6. 04
4. 38
4. 32
4.88
4. 26
4.39
5. 65
R0LL#4
ROLL# 5
START
START
4. 46
4. 32
4. 44
3.70
4. 50
4.06
4. 40
3.96
4.42
4. 24
4.44
4. 06
NASA LOT#
RQLL#6
R0LL#7
START
START
4. 94
4.76
4. 82
4. 66
5. 22
4. 32
5. 28
4. 88
5. 02
4. 68
5. 06
4. 66
AVERAGE
4. 65
15a. Compressive Strength,
FTMS 406-1021
26.50 24.68
22.75 24.65
24.73 24.14
25. 37 23. 31
25. 15 ?3» 19
AVG. 24.90 24.03
ksi, WARP
27. 59
26. 66
27. 22
26. 15
27. 42
27. 05
25. 71 26. 56
26.63 23.95
25. 94 26. 89
26.68 24.98
25.47 ?7. 17.
26.12 25.91
NASA LOT#
29. 07
28. 84
27. 76
26. 08
27. 90
27. 60
28. 33
30. 12
£8. 73
26. 51
28. 36
28. 27
AVERAGE
26. 38
15b. Compressive Modulus, msi, WARP
FTMS 406-1021
5.12 4.96
4.44 4.59
5.04 4.22
5.09 4.50
5. 16 4.46
AVG. 4.97 4.55
5. 07
4.56
5. 02
4.67
4. 61
4. 82
5.25 4.86
5.26 4.54
4.97 5.02
5.32 4.79
4.89 4. 69
5.14 4.78
NASA LOT#
5. 23
4. 63
4. 50
4. 52
4.62
4. 69
4.75
4. 92
4. 91
4. 66
4. 80
4. 77
AVERAGE
4. 63
16. Double Shear Strength, ksi
FTMS 406-1041A
3. 55
3. 42
3. 26
3. 42
3. 36
AVG. 3.40
2.98 3.21
3. 33 3. 60
3.09 3.85
3.21 3.35
3. 62 3. 54
3.25 3.51
3. 66 3- 33
3. 62 3. 33
3.48 3. 35
3. 49 3. 37
3.93 3.52
3. 64 3. 33
NASA LOT#
3. 08
3. 62
3. 48
3. 21
3. 31
3. 43
3. 57
3. 94
3. 15
3. 52
3. 32
3. 54
AVERAGE
3. 44
17 , Barcol Hardness, Units
ASTM D-2583
(Average of 10 determinations)
£9. 5 68. 8 70. 5
70.4
69. 7
NASA LOT#
70.8 72.4
2 AVERAGE 70.3
Page 6 of 6
FH 5034 NASA L0T» 2 U. S. P. LOT# D09275
18. Residual Volatiles, X
PTM-98
ROLL# 1
START
2. 32
2. 35
2. 38
AVG. 2. 34
19. Resin Content,
CTM-14B
39. 44
37. 60
39. 39
AVG. 38.81
R0LL#2
R0LL#3
START
START
2. 34
2. 62
2. 28
2. 63
2. 37
2. 60
2. 33
2.62
Pyrolysis
, x
35.
74
35.
92
35.
74
34.
23
36.
82
36.
54
36.
10
35.
56
ROLL# 4 ROLL# 5
START START
2.35 2.49
2.28 2.77
2. 34 2. 73
2. 33 2.66
NASA LOT#
36. 23 38. 50
37.24 37.34
37.69 34. 35
37.05 36.73
NASA LOT#
R0LL#6 R0LL#7
START START
2. 39 2. 49
2.41 2.37
2. 46 2. 45
2.42 2.44
2 AVERAGE 2.45
40.14 36.08
38.56 34.60
39. 48 34. 36
39. 40 35. 01
2 AVERAGE 36.95
20. Acetone Extraction, X
CTH-18A
21a.
-. 15
. 81
. 59
.69
1.98
. 00
55
1. 19
-.46
. 16
1. 36
-. 16
-. 62
. 38
. 72
.54
. 40
. 66
. 16
3. 66
-. 22
AVG.
. 58
. 30
. 38
.98
.66
1.01
13
NASA LOT# 2
AVERAGE
• 54
CTE,
ln/ln *F,
with PLY
PTM-61B
-.27
1. 07
AVG. .40
.75 -.26
. 48 -.51
.62 -.39
.58 1.09
. 61 . 66
.60 .98
NASA LOT# 2
.10 -6.92
. 77 . 78
.44 -3.07
AVERAGE -.06
21b CTE, in/in
PTM-61B
13. 44
9. 80
AVG. 11.62
F, Cross PLY
11.31 11.20
11. 06 11. 20
11.19 11.20
13.79 13.12
12. 96 12. 75
13.38 12.94
NASA LOT#
See Chart
15.62 14.38
15. 75 14. 09
15.69 14.24
2 AVERAGE 12. 89
21A-21G
U. S. Polyseric
u.
Hamid M. Guraishi, Manager
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