125742 S43 M1 response 05aug2021

Pfizer Documents (PHMPT/FDA)

Pfizer Bla Submission

Pfizer 16 Plus Documents

24

Document text

COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 1TABLE OF CONTENTS
LIST OF TABLES ................................ ................................ ................................ ..................... 1
 (PFIZER CHESTERFIELD ) ................................ ...................... 3
QUERY 1 ................................ ................................ ................................ ................................ ...3
RESPONSE 1 ................................ ................................ ................................ ................... 3
QUERY 2 ................................ ................................ ................................ ................................ ...4
RESPONSE 2 ................................ ................................ ................................ ................... 4
DRUG SUBSTANCE (PFIZ ER A NDOVER-  AND )................................ ....8
QUERY 4 ................................ ................................ ................................ ................................ ...8
RESPONSE 4 b ................................ ................................ ................................ ................ 8
QUERY 5 ................................ ................................ ................................ ................................ ...9
RESPONSE 5 ................................ ................................ ................................ ................... 9
QUERY 6 ................................ ................................ ................................ ................................ .12
RESPONSE 6 ................................ ................................ ................................ ................. 12
DRUG PRODUCT ................................ ................................ ................................ ................... 13
QUERY 7 ................................ ................................ ................................ ................................ .13
RESPONSE 7 ................................ ................................ ................................ ................. 13
QUERY 8 ................................ ................................ ................................ ................................ .14
RESPONSE 8 ................................ ................................ ................................ ................. 14
QUERY 9 ................................ ................................ ................................ ................................ .15
RESPONSE 9 ................................ ................................ ................................ ................. 15
QUERY 10 ................................ ................................ ................................ ............................... 16
RESPONSE 10 ................................ ................................ ................................ ............... 16
QUERY 11 ................................ ................................ ................................ ............................... 18
FOLLOW -UP TO FDA’S 2 6 JUL Y 2021 IR RESPO NSE REGARDI NG 
MANUFACTURING AND EQ UIPMENT: QUERY 16E ................................ ................ 21
LIST OF TABLES
Table 1. List of Critical Equipment/Materials Used in Manufacturing of the  
............................... ................................ ................................ .................... 4
Table 2. Cleaning Validation Results Portable Tank ............................ 6
Table 3. Deviations ................................ ................................ ................................ ............... 7
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FDA-CBER-2021-5683-1149546
COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 2Table 4. Clean Hold Time Results ................................ ................................ ........... 9
Table 5. Clean Hold Time Results Andover ................................ ........................... 10
Table 6.  Tank Qualification Status ................................ ................................ ........... 18
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FDA-CBER-2021-5683-1149547
COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 3(PFIZER CHESTERFIELD)
QUERY 1
Please clarify  what critical utilities are used during the  process, and the 
microbial control for each critical utility  (e.g., or routine monitoring).
RESPONSE 1
are the onl y critical utilities used during the  
process.  
Literature References
None
SUPPORTING DOCUMENTATION
New or Replaced Supporting Documentation
None
Previously submitted supporting documentation
None
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FDA-CBER-2021-5683-1149548
COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 4QUERY 2
The list provided in Table 3.2.A.1 -1 does not include tubing, small parts, biological safet y 
cabinets, and laminar flow hoods. Please update Table 3.2.A.1 -1 to include all direct product 
contact equipment.
RESPONSE 2
Additional product -contact parts are listed in the table below.  Biological safet y cabinets and 
laminar flow hoods are not direct product contact and are not included in the table.  Table 
3.2.A.1- 1 in Section 3.2.A.1 Facilities and Equipment (Chesterfield) has been updated.  
Table 1. List of Critical Equipment/Materials Used in Manufacturing of the  
Equipment/ 
MaterialsProduct Contact/
UseSingle Use / 
Multiuse/ 
DedicatedMaterial of Construct
(MOC )Cleaned / 
Sterilized
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COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 5Literature References
None
SUPPORTING DOCUMENTATION
New or Replaced Supporting Documentation
3.2.A.1 Facilities and Equipment (Chesterfield) -Replaced
Previously submitted supporting documentation
None
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FDA-CBER-2021-5683-1149550
COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 6QUERY 3
Regarding equipment cleaning validation, please provide the following information:
a.Provide the cleaning validation results (or rationale for lack thereof) for the following 
equipment 
b.Specify  the maximum clean hold times and provide clean hold time validation results f or 
each equipment.
c.Specify  the equipment cleaning verification frequency  and the parameters to be tested 
(i.e., ) during routine production.
RESPONSE 3
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COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 7Literature References
None
SUPPORTING DOCUMENTATION
New or Replaced Supporting Documentation
Section 3.2.A.1 Facilities and Equipment Cleaning Validation Summary  (Chesterfield)-
Replaced
Previously submitted supporting documentation
None
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FDA-CBER-2021-5683-1149552
COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 8DRUG SUBSTANCE (PFIZ ER ANDOVER -  AND
QUERY 4
Regarding environmental monitoring, please provide the following information:
a.Please define “at rest” and “in operation”.
b.Please clarify  if the total air particulate limits are for “in operation” conditions.
RESPONSE 4 a
“At rest” describes the status of a facility  with all services functioning, standard processing 
equipment installed, and with no personnel or manufacturing activities being performed other 
than environmental monitoring.
“In operation” describes the status of a facility  with all services functioning, standard 
processing equipment installed, but includes routine personnel and production- related 
activities  being performed or simulated. A facility is considered to be in operation status 
from the time of the initial set -up to the start of final clean -up including  set -up and 
production operations.
RESPONSE 4 b
The total air particulate limits are applied for both at rest and in operation monitoring. A 
footnote was added to the Table 3.2.A.1 -4, in 3.2.A.1 Facilities and Equipment (Andover 
  and Table 3.2.A.1-6, in 3.2.A.1 Facilities and Equip ment (  for clarification.
Literature References
None
SUPPORTING DOCUMENTATION
3.2.A.1 Facilities and Equipment (Andover -Replaced
3.2.A.1 Facilities and Equipment ( -Replaced
Previously submitted supporting documentation
None
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COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 9QUERY 5
Please supply  the following information regarding the dirty  and clean hold times of direct 
product contact equipment:
a.Please clarify  if clean and dirty  hold times were performed during process validation, and 
please provide the number of replicates perfor med. 
b.Define the parameters tested at the end of the clean hold time to verify  the equipment 
remained clean (i.e., ).
RESPONSE 5
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COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 10
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BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 11Literature References
None
SUPPORTING DOCUMENTATION
New or Replaced Supporting Documentation
None
Previously submitted supporting documentation
None
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FDA-CBER-2021-5683-1149556
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BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 12QUERY 6
Please clarify  if the manufacturing areas and direct product contact equipment are product 
dedicated or campaign dedicated for BNT162b2 in both and , as there are the 
following inconsistencies:
a.In 3.2.A.1.1, you state,  
However, in 3.2.A.1.8.1, y ou indicate that the  
b.Table 3.2.A.1- 4 (  indicates that  
c.Table 3.2.A.1- 3 ( ) indicates that
 
 
RESPONSE 6
The response applies to query  6 a, b and c.
Literature References
None
SUPPORTING DOCUMENTATION
3.2.A.1 Facilities and Equipment (Andover -Replaced
3.2.A.1 Facilities and Equipment ( -Replaced
Previously submitted supporting documentation
None
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BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 13DRUG PRODUCT
QUERY 7
Please update Table P.3.1 with the specific anal ytical test methods for drug product release 
and stability  testing to be performed at each facility.
RESPONSE 7
Section 3.2.P.3.1 Manufacturer(s) is updated to include the anal ytical test methods performed 
at each facilit y for releas e and stability .  This information is also included within Section 
3.2.R Summary  of Analytical Procedures, Method Validation and Transfer Reports.
Literature References
None
SUPPORTING DOCUMENTATION
New or Replaced Supporting Documentation
3.2.P.3.1 Manufa cturer(s) , replaced
Previously submitted supporting documentation
3.2.R Summary  of Analytical Procedures, Method Validation and Transfer Reports
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FDA-CBER-2021-5683-1149558
COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 14QUERY 8
Please indicate what room and building the visual inspection line is located. Please 
explain when this inspection machine will be used for inspecting BNT162b2 filled vials 
manufactured on Filling Lines .
RESPONSE 8
Inspection L ine  is located in the  Building at Pfizer Puurs, room . The 
Inspection L ine is not intended for use under the commercial BLA and information is 
removed from the 3.2.A.1 Facilities and Equipment (Puurs). 
Literature References
None
SUPPORTING DOCUMENTATION
New or Replaced Supporting Documentation
3.2.A.1 Facilities and Equipment (Puurs) , replaced
Previously submitted supporting documentation
None
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COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 15QUERY 9
Regarding the container closure integrit y testing, please submit the  method 
validation protocol, summary  report and assay  performance pro cedure that is followed at 
Pfizer Puurs and Pfizer Kalamazoo.
RESPONSE 9
For Pfizer Kalamazoo, the anal ytical method transfer/validation report along with the 
analytical procedure covering the  method is found in Section 3.2.R Summary  
of Anal ytical Procedures, Method Validation and Transfer Reports.  The protocol used for 
Literature References
None
SUPPORTING DOCUMENTATION
New or Replaced Supporting Documentation
Previously submitted supporting documentation
3.2.R Summary  of Analytical Procedures, Method Validation and Transfer Reports
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COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 16QUERY 10
Please submit the  container closure integrit y test method validation protocol, 
summary  report and assay  performance procedure that is followed at Pfizer Puurs and Pfizer 
Kalamazoo. Please explain when this method will be used as you have two container closure 
integrit y methods for your drug product.
RESPONSE 10
Executed test method validation protocols for the  anal ysis test method are 
provided in lieu of the protocols and summary  reports (as all information is captured therein),
covering container closure combinations from both Pfizer Puurs ( USP-1207 Method 
Validation - Pfizer Puurs 2mL  vial Rev 2.4_Final Report ) and Pfizer Kalamazoo ( USP-
1207 Method Validation - Pfizer Kalamazoo 2mL  vial Rev 1.2_Final Report ).
Literature References
None
SUPPORTING DOCUMENTATION
New or Replaced Supporting Documentation
USP-1207 Method Validation Pfizer Puurs 2mL  vial Rev 2.4_Final Report , new
USP-1207 Method Validation Pfizer Kalamazoo 2mL  vial Rev 1.2_Final Report , new
3.2.P.3.1 Manufacturer(s) , replaced
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FDA-CBER-2021-5683-1149561
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BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 17Previously submitted supporting documentation
3.2.P.2.4 Container Closure Sy stem
3.2.P.2.5 Microbiological Attributes
3.2.P.3.5 Shipping Validation
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FDA-CBER-2021-5683-1149562
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BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 18QUERY 11
Regarding a recent Information Request response (Response to FDA 26 Jul 2021) STN 
125742/0.24, the Agency requires clarification to your Query  16a response regarding new 
equipment at Pfizer Kalamazoo. As stated in Table 5 of your 16a response, the 
  tanks are not y et qualified. Please provide the following 
information regarding these tanks:
QUERY 11a
Please provide the equipment numbers and when qualification is expected to be completed (if 
not previously completed).
RESPONSE 11a
Equipment (ie, tank) numbers and qualification status are provided in Table 6.Based on 
procedures, equipment cannot be used in the process until it is qualified.  
Table 6.  Tank Qualification Status
Tank Size Tank ID Number Qualification Status Anticipated Qualification 
Completion Date
Abbreviations:  NA = Not Applicable
The  tanks were not included in the BLA application and were submitted as an
amendment to the EUA/IND (SN0426 submitted on 28 Jul 2021) , which is currentl y under 
review b y CBER.
QUERY 11b
Please explain wheth er these tanks were used in the process validation runs included in 
support of y our BLA application. If not, please provide a justification to explain how the 
tanks are suitable for your process operation.
RESPONSE 11b
The  tanks were not used for the process validation runs included in the BLA 
application.
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FDA-CBER-2021-5683-1149563
COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 19QUERY 11c
Please address the discrepancy regarding the  tanks qualification status with y our recent 
IND amendment (SN0426), which you referenced in Table 5 of your response to Query 
16a. According to y our IND amendment, 2.3. Introduction to the Quality  Overa ll Summary  
Section 2.3.1.1 y ou claim these  tanks are qualified.
RESPONSE 11c
The  tanks have been submitted as an amendment to I ND19736 (SN0426 submitted on 
28 Jul 2021 ) and also included in Table 5 of response to Query  16a previously  submitt ed to 
STN 126742/0.24.  Query  16 indicated that it was in regard to the BNT162b2 major 
manufacturing equipment used at Pfizer Kalamazoo , therefore the  tanks that were 
recentl y submitted, were added to the table to be complete.
As a clarification relative to the Quality  Overall Summary  Section 2.3.1 .1 of IND 19736 
SN0426 which states that the tanks are  status is 
in reference to and in support of the  tanks are 
 although  of the tanks been full y qualified for use.  
The remaining  tanks will be qualified prior to being placed into service by
.
QUERY 11d
Please address whether these tanks have been used in the ma nufacture of EUA BNT162b2 
material prior to qualification.
RESPONSE 11d
None of the  tanks have been used to manufacture EUA BNT162b2 material.   
 of the  tanks has been qualified for use.  Change control records are 
utilized to document the qualification activities of each individual tank.  Tanks can be placed 
into service following approval of the amendment to I ND19736 (SN0426 submitted on 28 
Jul 2021 ) and after all change control activities have been completed.
QUERY 11e
Please provide summaries of y our cleaning and sterilization validations for the  tanks. 
If cleaning and/or sterilization validations are not complete, pl ease provide a timeframe that 
you expect to complete the respective validations. Please provide a summary  of your 
cleaning verification regime including acceptance criteria. 
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FDA-CBER-2021-5683-1149564
COVID -19 Vaccine (BNT162, PF -0730 2048)
BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 20RESPONSE 11e
The sterilization validation for the  tanks has been provided in the recent IND 19736 
amendment (SN0426).  An updated Section 3.2.P.3.5 Sterilization in Place (SI P) Validation 
[Kalamazoo] is also provided in this response. This updated document is fully  aligned with 
the content submitted in IND 19736 SN0426, includin g a revised scope of  tanks 
presented, which focuses only  on tanks that contact the sterile drug product.  I nformation has 
been removed for  
 and do not contact th e sterile drug product .
A cleaning assessment has been completed for the  tanks which determined that 
the tanks are covered b y existing cleaning validation.    The cleaning validation summary  for 
the  tanks are covered by  the data for the BN T162b2  Bulk Hold, and Sterile 
Tanks provided in 3.2.A.1 Facilities and Equipment Cleaning Validation Summary  –Pfizer, 
Kalamazoo.
QUERY 11f
Please provi de  BNT162b2 hold time validations for the  tanks 
including the microbi al challenge resul ts and criteria.
RESPONSE 11f
The hold time validations for the  tanks hav e not y et been completed.  The h old time 
validations will be completed b y .
Literature References
None
SUPPORTING DOCUMENTATION
New or Replaced Supp orting Documentation
3.2.P.3.5 Sterilization in Place (SI P) Validation [Kalamazoo], Replaced
Previously submitted supporting documentation
3.2.A.1 Facilities and Equipment Cleaning Validation Summary  –Pfizer, Kalamazoo
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FDA-CBER-2021-5683-1149565
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BLA 125742/0
Response to 05 Aug 2021 FDA IR-Facilities Questions
PFIZER CONFIDENTIAL
Page 21FOLLOW -UP TO FDA’S 26 JULY 2021 I RRESPONSE REGARDING
MANUFACTURING AND EQ UIPMENT : QUERY 16E
Regarding the recent Information Request response to the agency  on 26 Jul 2021 (Response 
to FDA 26 Jul 2021) STN 125742/0.24, to Query 16 e, the following Table 8 has been 
updated with additional i nformation for portable tank .  Portable tank 
has been removed from the table as it was incorrectl y added in the 
response to Query  16e.  Minor formatting corrections were also made to the table.
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PFIZER CONFIDENTIAL
Page 22Table 8.Drug Product Contact Equipment Summary
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Page 23Table 8.Drug Product Contact Equipment Summary
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Page 24Table 8.Drug Product Contact Equipment Summary
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